Use-test

In this section results will be presented using test samples to determine the accuracy of our approach. Further on an example is shown using the system to analyse casting defects. For the experiments moderate projective magnifications between 1.1 and 1.4 were chosen. The test samples used to determine the accuracy of calibration, 3D defect position and volume estimation consist of several holes representing internal defects of different but known size and shape. 

The accuracy of the presented methods was verified using test pipes with various diameters and wall thickness of which the wall thickness was measured independently using a slide-rule. Both on film and on the monitor the wall thickness could be determined within an accuracy of ca. 0.2 - 0.3 mm. 

Particles magnetic is one of the most useful testing techniques in industry. It allows the detection of surfacic and sub-surfacic defects. The main difficulty of this technique is to optimize the control conditions allowing an easiest interpretation of the results which necessite a great experience of the operator. 

This reaction is a useful test for a sulphite or for moist sulphur dioxide, which turns dichromate paper (filter paper soaked in potassium dichromate) from yellow to green. 

For a cobalt(ll) salt, the precipitation of the blue->pitik cobalt(II) hydroxide by alkali, or precipitation of black cobalt(II) sulphide by hydrogen sulphide provide useful tests the hydroxide is soluble in excess alkali and is oxidised by air to the brown CoO(OH) . 

The reactions of aqueous solutions of nickel(II) salts with hydroxide ions, with excess ammonia, with sulphide ion and with dimethyl-glyoxime (see above) all provide useful tests for nickel(II) ions. 

The reaction of Cd (aq) with sulphide ion, to give yellow CdS, and with hydroxide ion to give the white CdfOHlj, soluble in ammonia, provide two useful tests. 

An additional useful test is to distil the acid or its sodium salt with soda lime. Heat 0.5 g. of the acid or its sodium salt with 0 2 g. of soda lime in an ignition tube to make certain that there is no explosion. Then grind together 0-5 g. of the acid with 3 g. of soda hme, place the mixture in a Pyrex test-tube and cover it with an equal bulk of soda hme. Fit a wide dehvery tube dipping into an empty test-tube. Clamp the tube near the mouth. Heat the soda lime first and then the mixture gradually to a dull-red heat. Examine the product this may consist of aromatic hydrocarbons or derivatives, e.g., phenol from sahcyUc acid, anisole from anisic acid, toluene from toluic acid, etc. 

Nitrogen and sulphur present. Just acidify 2-3 ml. of the fusion solution with dilute nitric acid, and evaporate to half the original volume in order to expel hydrogen cyanide and/or hydrogen sulphide which may be present. Dilute with an equal volume of water. If only one halogen is present, proceed as in tests (i) or (iii). If one or more halogens may be present, use tests (ii), (iii) or (iv). 

Nondestmctive evaluation, also termed nondestmctive testing or nondestmctive inspection, is extensively used in weld testing (14). Nondestmctive tests do no impair the serviceabiUty of the material or component under stress. The most widely used tests for evaluation of welds are Hquid penetrant, magnetic particle, ultrasonics, and radiography. Acoustic-emission tests are increasingly used. Nondestmctive tests detect and characterize, in terms of size, shape, and location, the various types of weld discontinuities that can occur. 

The experimental procedures depend to a large extent on the use to which the explosive is to be put. Comparison is often made to proven explosives of known performance. Many of the most commonly used tests in the various categories of concern are as follows ... 

In the most frequently used test the sample is placed between two electrodes and the voltage is increased from zero at a uniform rate until breakdown occurs. When an insulated wine is available, the voltage can be placed between the inner conductor and a conductive medium, such as an outside metallic shield or even water. 

Quahty control testing of siUcones utilizes a combination of physical and chemical measurements to ensure satisfactory product performance and processibihty. Eor example, in addition to the usual physical properties of cured elastomers, the plasticity of heat-cured mbber and the extmsion rate of TVR elastomers under standard conditions are important to the customer. Where the siUcone appHcation involves surface activity, a use test is frequently the only rehable indicator of performance. Eor example, the performance of an antifoaming agent can be tested by measuring the foam reduction when the sihcone emulsion is added to an agitated standard detergent solution. The product data sheets and technical bulletins from commercial siUcone producers can be consulted for more information. 

Viscosity. Although traditionally of Httle importance in the evaluation of vegetable and insect waxes, viscosity is an important test for mineral and synthetic waxes. One of the most frequently used tests, ASTM D88, is used to measure the time in seconds required for a specified quantity of wax at a specified temperature to flow by gravity through an orifice of specified dimensions. This viscosity is expressed in Saybolt Universal Seconds (SUS) at the temperature of the test. The SI unit for kinematic viscosity is mm /s (=cSt). 

Tests Simulating Use Conditions. Several simulation tests involving wear and use testing have been developed. The first and only one to be adopted as a standard in the United States is AATCC Test Method 134-1975 for measuring the electrostatic propensity of carpets (60). In this test a person wearing standard neoprene and leather sole shoes and carrying a probe connected to an electrometer walks on a carpet for 30 to 60 s until the measured body voltage builds up to a maximum. 

Source references for frequentiy used test procedures for determining properties of activated carbon are shown in Table 4. A primary source is the Jinnual Book ofyimerican Societyfor Testing and Materials (ASTM) Standards (61). Other usehil sources of standards and test procedures include manufacturers of activated carbon products, the American Water Works Association (AWWA) (33,34), and the Department of Defense (54). 

Formulation of effective corrosion-resistant coatings is made difficult by the lack of a laboratory test that can provide rehable predictions of field performance. The most widely used test is exposure in a salt fog chamber. It has been shown repeatedly, however, that the results of such tests do not correlate with actual performance (125). Outdoor exposure of panels can provide useful data, especially in locations where salt spray occurs, but predictions of performance are not always satisfactory (126). 

Particle-Size Distribution This is defined as the relative percentage by weight of grains of each of the different size fractious represented in the sample. It is one of the most important factors in evaluating a screening operation and is best determined by a complete size analysis using testing sieves. 

Further it is planned to use tests - organisms of various trophie levels to eaiTy out systematie reseai ehes on eompaiison of results of an estimation of quality of natural waters to the help of the different generalized pai ameters. 

Therefore the problem of development of express, inexpensive and simple in use test-methods for determination of volatile amines is of present day interest. 

Started to rise from the reaction, causing the vessel bottom head to fail at the weld seam. The force from the escaping gases propelled the tank into the ceiling and overhead structural steel. A small fire erupted which was quickly brought under control by the automatic sprinkler system. Even though the chemists had reviewed the chemistry and did not anticipate any problems, use testing could have identified this problem in the laboratory rather than the plant. 

Establish procedures for testing and verification of catalyst activity and identification including use testing. Include procedure to monitor shelf life of catalyst to maintain activity... 

Is all measuring equipment used, tested and calibrated for accuracy at regular intervals ... 

Most water analysis results are rather easily interpreted. However, two simple and useful tests need explanation. These are the P and M alkalinity. The water is titrated with N/30 HCl to the phenolphthalein end point at pH 8.3. This is called the P alkalinity. Similar titration to the methyl orange end point at pH 4.3 is called the M alkalinity. They are reported as ppm CaCO,. 

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