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Inorganic materials sodium sulfate

A 3-1., three-necked flask fitted with a mechanical stirrer, a dropping funnel, and a thermometer is then charged with an aqueous solution of 2.2 moles of calcium hypochlorite [Hypochlorous acid, calcium salt] (Note 3), and the piperidine acetate prepared above is placed in the dropping funnel. The hypochlorite solution is stirred and cooled to 0° to — 5° with a methanol-ice bath, and the piperidine acetate is added dropwise over a period of 1.25 hours while the temperature is maintained below 0°. After a further 15 minutes of stirring, equal portions of the mixture are placed in two 2-1. separatory funnels and extracted three times with a total of about 1300 ml. of ether. The ether extract is placed in a 2-1. flask and dried over anhydrous sodium sulfate in a cold room at 4° overnight. After filtration to remove inorganic material, the bulk of the ether is removed by boiling on a water bath maintained below 60° (Note 4). [Pg.118]

Inorganic residue is rinsed with diethyl ether. The combined ethereal extracts are added to the filtered solution and the mixture is concentrated to ca. 10 mL by evaporation of the solvent under reduced pressure. The residue is treated with a saturated solution of potassium chloride (KCI) (50 mL), extracted with dichloromethane (3 x 50 mL), and the combined extracts are dried over anhydrous sodium sulfate (Note 21). Removal of volatile material under reduced pressure gives an oil that is flash Chromatographed (silica, diethyl ether - petroleum ether 1 1) to afford 1.77 g (62%) of 2-0-benzyl-3,4-isopropylidene-D-erythrose (Note 22). [Pg.166]

Table 4 shows the typical ranges of black liquor constituents and characteristics of Kraft evaporator condensates. The composition of liquors may vary significantly, depending upon the type of raw material used. Inorganic constiments in black liquor are sodium hydroxide, sodium sulfate, sodium thiosulfate, sodium sulfide, sodium carbonate, and sodium chloride [11]. [Pg.461]

Chemical treatment of natural waters. Both directly and indirectly, the general problem of purification and treatment of natural waters is related to the chemical and physical properties of the normal and acid salts of carbonic acid. The common impurities in natural waters consist of suspended solid organic and inorganic materials and of certain dissolved salts, particularly the acid carbonates, chlorides, and sulfates of sodium, calcium, and magnesium. The solid matter may be removed by filtration, the presence of limited quantities of sodium salts is not objectionable, and the calcium and magnesium salts are eliminated only through appropriate chemical treatment. The ions that are most... [Pg.625]

The column is packed with the required amount of a sorbent and loaded with the sample extract. Elution of the analytes is effected with a suitable solvent, leaving the interfering compounds on the column. The packing material may be an inorganic substance such as Florisil (basic magnesium silicate) or one of many commercially available SPE stationary phases. The eluate may be further concentrated if necessary. A Florisil column is shown in Figure 1.9. Anhydrous sodium sulfate is used to dry the sample [8],... [Pg.24]

In the presynthetic surfactant era, soap was built (and still is) with alkaline salts such as soda ash, silicates, orthophosphates, and borates. These materials buffer the wash solution to a high pH and prevent soap protonation thus, the soap remains effective. Another type of builder is the neutral inorganic salt such as sodium chloride and sodium sulfate. These materials may improve detergency by increasing the ionic strength and altering the CMC of anionic surfactants. [Pg.3131]

The production of wood pulp and paper is a primary industry in the sense of its utilization of wood as its chief raw material. Pulp and paper is also a secondary industry in the sense that it consumes large quantities of bulk inorganic chemicals such as chlorine, sodium hydroxide, sodium sulfate, etc., produced by the primary (commodity) chemical industry. This business area consumes close to 10% of the inorganic chemicals produced in the countries in which it is dominant. Thus, it not only contributes directly to the economy of these areas, but also indirectly by its purchases of chemicals. [Pg.453]

Arayanarakul, K., N. Choktaweesap, D. Ant-ong, C. Meechaisve, and P. Supaphol (2006). Effects of poly(ethylene glycol), inorganic salt, sodium dodecyl sulfate, and solvent system on electrospinning of poly(ethylene oxide). Macromolecular Materials and Engineering 291(6) 581-591. [Pg.329]

Electrolytes and Fillers Inorganic salts such as sodium sulfate are added to laundry formations to bring them up to uniform cleaning strength and to provide appropriate measurable quantities for addition in laundering by the consumer. These materials may be considered fillers but also are electrolytes in solution that serve to enhance to some degree the migration and action of the surfactant as well as improve the physical characteristics of the product. [Pg.218]

The most common impurities are the corresponding acid and hydroxy compound (i.e. alcohol or phenol), and water. A liquid ester from a carboxylic acid is washed with 2N sodium carbonate or sodium hydroxide to remove acid material, then shaken with calcium chloride to remove ethyl or methyl alcohols (if it is a methyl or ethyl ester). It is dried with potassium carbonate or magnesium sulfate, and distilled. Fractional distillation then removes residual traces of hydroxy compounds. This method does not apply to esters of inorganic acids (e.g. dimethyl sulfate) which are more readily hydrolysed in aqueous solution when heat is generated in the neutralisation of the excess acid. In such cases, several fractional distillations, preferably under vacuum, are usually sufficient. [Pg.64]

Nitrogen sources include proteins, such as casein, zein, lactalbumin protein hydrolyzates such proteoses, peptones, peptides, and commercially available materials, such as N-Z Amine which is understood to be a casein hydrolyzate also corn steep liquor, soybean meal, gluten, cottonseed meal, fish meal, meat extracts, stick liquor, liver cake, yeast extracts and distillers solubles amino acids, urea, ammonium and nitrate salts. Such inorganic elements as sodium, potassium, calcium and magnesium and chlorides, sulfates, phosphates and combinations of these anions and cations in the form of mineral salts may be advantageously used in the fermentation. [Pg.1062]

The complete analysis of alcohol sulfates is described in the Standard Methods of the International Organization of Standards (ISO) [200] and of the American Society for Testing and Materials (ASTM) [201]. These methods describe the analysis of inorganic sulfate content, chloride content, unsulfated matter, and water as well as other analytical values. Other ISO standards describe the analysis of sodium secondary alkyl sulfates [202], determination of pH [203], determination of water content [204,205], chlorides [206], total active matter in sul fated ethoxylated alcohols and alkylphenols [207], mean relative molecular mass in sulfated ethoxylated alcohols and alkylphenols [208], sulfate content... [Pg.279]


See other pages where Inorganic materials sodium sulfate is mentioned: [Pg.455]    [Pg.11]    [Pg.463]    [Pg.530]    [Pg.1182]    [Pg.223]    [Pg.90]    [Pg.17]    [Pg.414]    [Pg.721]    [Pg.1494]    [Pg.523]    [Pg.193]    [Pg.3203]    [Pg.125]    [Pg.406]    [Pg.1005]    [Pg.504]    [Pg.32]    [Pg.256]    [Pg.418]    [Pg.451]    [Pg.152]    [Pg.138]    [Pg.382]    [Pg.273]    [Pg.223]    [Pg.1186]    [Pg.60]    [Pg.117]    [Pg.106]    [Pg.593]    [Pg.81]    [Pg.55]    [Pg.199]    [Pg.6]    [Pg.180]   
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