Equipment used

The capacity of a trommel increases with increasing speed of rotation until a critical speed is achieved. At speeds greater than this, the material does not cascade over the surface but is carried round and centrifugal force and separation is seriously impaired. The critical speed of a trommel is given by 

Arrangements for revolving screens (a) parallel type and (b) concentric drum. 

---

The accredited laboratory must confirm that all the equipment used in NDT implementation is tested with regular intervals in compliance with relevant state standards. 

Measurements are made using appropriate equipment or instruments. The array of equipment and instrumentation used in analytical chemistry is impressive, ranging from the simple and inexpensive, to the complex and costly. With two exceptions, we will postpone the discussion of equipment and instrumentation to those chapters where they are used. The instrumentation used to measure mass and much of the equipment used to measure volume are important to all analytical techniques and are therefore discussed in this section. 

A twin-screw extmder is used to reduce residual monomers from ca 50 to 0.6%, at 170°C and 3 kPa with a residence time of 2 min (94). In another design, a heated casing encloses the vented devolatilization chamber, which encloses a rotating shaft with specially designed blades (99,100). These continuously regenerate a large surface area to faciUtate the efficient vaporization of monomers. The devolatilization equipment used for the production of polystyrene and ABS is generally suitable for SAN production. 

If a linear mbber is used as a feedstock for the mass process (85), the mbber becomes insoluble in the mixture of monomers and SAN polymer which is formed in the reactors, and discrete mbber particles are formed. This is referred to as phase inversion since the continuous phase shifts from mbber to SAN. Grafting of some of the SAN onto the mbber particles occurs as in the emulsion process. Typically, the mass-produced mbber particles are larger (0.5 to 5 llm) than those of emulsion-based ABS (0.1 to 1 llm) and contain much larger internal occlusions of SAN polymer. The reaction recipe can include polymerization initiators, chain-transfer agents, and other additives. Diluents are sometimes used to reduce the viscosity of the monomer and polymer mixture to faciUtate processing at high conversion. The product from the reactor system is devolatilized to remove the unreacted monomers and is then pelletized. Equipment used for devolatilization includes single- and twin-screw extmders, and flash and thin film evaporators. Unreacted monomers are recovered for recycle to the reactors to improve the process yield. 

Some industrial processes produce predorninately latent air conditioning loads. Others dictate very low humidities and when the dew point falls below 0°C, free2ing becomes a major concern. Dehydration equipment, using soHd sorbents such as siUca gel and activated alurnina, or Hquid sorbents such as lithium chloride brine and triethylene glycol, may be used. The process is exothermic and may require cooling the exiting air stream to meet space requirements. Heat is also required for reactivation of the sorbent material. 

The De Danske Sukkerfabriker (DDS) diffuser extractor (Fig. 6) is a relatively simple version of this family of machines, employing a double screw rotating in a vessel mounted at about 10° to the horizontal. The double screw is used to transport the soHds up the gradient of the sheU, while solvent flows down the gradient. Equipment using a single screw in a horizontal sheU for countercurrent extraction of soHds under pressure has been described (19). 

Physical requirements of fluid fertilizers include freedom from sediments, suitably low viscosity, low vapor pressure, and noncorrosivity with regard to available handling equipment. Using anhydrous ammonia, the chief physical concerns, are in the safety of handling under pressure and the minimizing of vapor loss during injection into the sod. 

As with all tests, frequent caUbration of the test equipment using standard hardness blocks is a prerequisite for rehable hardness testing (see ASTM E18). Standard hardness blocks are available through commercial sources in the United States but do not have traceabiUty to internationally accepted standards as in Europe. 

The softened seawater is fed with dry or slaked lime (dolime) to a reactor. After precipitation in the reactor, a flocculating agent is added and the slurry is pumped to a thickener where the precipitate settles. The spent seawater overflows the thickener and is returned to the sea. A portion of the thickener underflow is recirculated to the reactor to seed crystal growth and improve settling and filtering characteristics of the precipitate. The remainder of the thickener underflow is pumped to a countercurrent washing system. In this system the slurry is washed with freshwater to remove the soluble salts. The washed slurry is vacuum-filtered to produce a filter cake that contains about 50% Mg(OH)2. Typical dimensions for equipment used in the seawater process may be found in the Hterature (75). 

Fig. 28. Schematic representation of dead-end and cross-flow filtration with microfiltration membranes. The equipment used in dead-end filtration is simple, but retained particles plug the membranes rapidly. The equipment required for cross-flow filtration is more complex, but the membrane lifetime is...

The general pieces of equipment used in grinding flake mica or mica concentrate into saleable mica products are hammer mills of various types, fluid energy mills, Chaser or Muller mills for wet grinding, and Raymond or WiUiams high side roUer mills. Another method is being developed, called a Duncan mill (f. M. Huber, Inc.), that is similar in many respects to an attrition mill. AH of these mills are used in conjunction with sieves, and all but some types of hammer mills incorporate air classifiers as a part of the circuit. 

The American faciUties also differed fundamentally from the British faciUties in regard to maintenance philosophy. The American plants were designed to employ remote maintenance, ie, to remove and replace equipment using shielded cranes operating inside the shielded stmcture. The British developed a contact approach based on simplified designs for equipment downstream of the fission product removal step. The British approach has been used at all commercial faciUties. 

Rheology. Both PB and PMP melts exhibit strong non-Newtonian behavior thek apparent melt viscosity decreases with an increase in shear stress (27,28). Melt viscosities of both resins depend on temperature (24,27). The activation energy for PB viscous flow is 46 kj /mol (11 kcal/mol) (39), and for PMP, 77 kJ/mol (18.4 kcal/mol) (28). Equipment used for PP processing is usually suitable for PB and PMP processing as well however, adjustments in the processing conditions must be made to account for the differences in melt temperatures and rheology. 

Health and Safety. Petroleum and oxygenate formulas are either flammable or combustible. Flammables must be used in facUities that meet requirements for ha2ardous locations. Soak tanks and other equipment used in the removing process must meet Occupational Safety and Health Administration (OSHA) standards for use with flammable Hquids. Adequate ventilation that meets the exposure level for the major ingredient must be attained. The work environment can be monitored by active air sampling and analysis of charcoal tubes. 

Fig. 3. Solvent-processing equipment using partial condenser. Level a on the water overflow line to the receiver should be about 3 cm below level b on the solvent-return line. Dimension b—c must be great enough to overcome pressure drop in the vapor piping, condenser, solvent piping, and rotameter. In a 4 m (1000-gaI) ketde, dimension b—c would be at least 1.25 m. The volume of the piping described by the dimension c—d—e should contain twice the volume of dimension b—c, thus providing an adequate Hquid seal against normal ketde operating pressures.

Much of the equipment used in the recovery system is identical with or closely related to equipment used in other chemical industries. This includes multiple-effect evaporators, and forced-circulation concentrators, causticizing equipment, and lime kiln. The function and nature of equipment essentially unique to the kraft recovery system are discussed herein. 

---