Twin-screw extruder preparation

The blends prepared by twin-screw extruder with two different draw ratios were extruded with the Brabender single-screw extruder at temperatures ranging from 180 280°C, The sample designation and specific processing conditions are given in Table 1. 

In an extension of this work, pellets of a blend of PCL and hy-droxypropylcellulose containing fluridone were prepared by grinding, blending, and then melt-spinning the mixture with a Berstorff twin screw extruder (78). The extruded rod was subsequently water-quenched and pelletized. Pellets were also prepared by coating bundles of extruded rods with the water-soluble excipients PEG 3350 and PEG 600 (95 5). In vitro release rate measurements were conducted in the simulant medium of 50% aqueous ethanol or hardened water. 

Homopolymers and copolymers from amido-sulfonic acid or salt containing monomers can be prepared by reactive extrusion, preferably in a twin screw extruder [1660]. The process produces a solid polymer. Copolymers of acrylamide, N-vinyl-2-pyrrolidone, and sodium-2-acrylamido-2-methyl-propane sulfonate have been proposed to be active as fluid loss agents. Another component of the formulations is the sodium salt of naphthalene formaldehyde sulfonate [207]. The fluid loss additive is mixed with hydraulic cements in suitable amounts. 

Fig. 28. Screw and barrel configuration of a co-rotating intermeshing twin-screw extruder for the preparation of filled thermoplastics compounds...

Nakamichi K, Nakano T, Yasuura H, Izumi S, Kawashima Y. The role of the kneading paddle and the effects of screw revolution speed and water content on the preparation of solid dispersions using a twin-screw extruder. Int J Pharm 2002 241 203-211. 

A mixture consisting of powdered polypropylene (59.91 g) and the step 1 product (90 mg) were tumble-mixed in a glass container for 24 hours. Thereafter the mixture (4.5 g) was compounded at 239°C using a small co-rotating twin-screw extruder. The sample required 4 minutes at a screw speed of 40rpm to be prepared. The extruded material only had a slight haze content. 

The antistatic properties of the step 2 product were evaluated by preparing tapes of blends with polystyrene by extruding in a twin-screw extruder using a flat die at 200°C. The contact angle of the tapes was measured using the sessile drop method and water as the measuring liquid. Testing data not supplied by author. 

The aliphatic-aromatic poly(ester)s discussed above are prepared from butanediol and a mixture of adipic acid and terephthalic acid. Blending can be performed on twin-screw extruder equipped with a medium shear mixing screw. 

Composite formulations were prepared as follows The straw samples as received from INEEL were ground to 0.69 mm in a hammer mill and oven dried to 1.1% moisture. The dried straw samples were then blended with various amounts of high-density polyethylene (HDPE), lubricants, and maleated polyethylene blends (MAPE) (see Table 2). The mixed formulations were then extruded with a 35-mm Cincinnati Milacron Model CMT 35 counterrotating conical twin screw extruder (Cincinnati Milacron, Batavia, OH), which produced a 9.525 x 38.1 mm2 solid cross-section. Flexural strength, density, and water sorption were measured for the extruded samples according to ASTM Standard Methods (13,14). 

Tang et al. (52) fabricated CNT-HDPE composite film by the following technique the first step was the preparation of a precursor material in the form of CNT-HDPE composite pellets. The pellets of neat HDPE and CNTs were combined in a beaker and heated in an oven at 200 °C for 10 min. Then the mixture was mechanically stirred to mix the CNTs into the melt and to form a viscous suspension. The dough-like suspension was then compressed and cooled to form a solid plate. The plate was then chopped into smaller pieces, which were fed into a twin-screw extruder. In the extruder, the temperature was maintained... 

Compounds with 2% to 10% (vol.) filler and an antioxidant additive (Irganox N225 0.2wt%) were prepared with a twin screw extruder (ZSK), at a temperature of 190°C. In case of silica, a first compound was prepared with a high shear mixer (Brabender) before extrusion, to obtain a good dispersion. 

Polyamide-6 (PA-6) and polypropylene (PP) are both semi-crystalline polymers and the combination of an engineering plastic (PA) and the best commodity product (PP) could lead to new blends with Interesting Intermediate properties. We tested systems containing 50 wt% of each product and the ones obtained by addition of 3% of the reactive PP-g-AM resulting from previous continuous grafting in the extruder. The blends were prepared by simple mixing in the ZSK 30 twin-screw extruder and the samples for mechanical testing were molded by injection in a BILLION equipment. 

Even though in principal, the visualization of ID simulations in a three-dimensional space is not too meaningful, the visualization of a number of ID-functions with exact geometrical placement can be an interesting alternative. In addition to that, the simple and natural interaction metaphors that are used in VEs can ease the task of configuration construction. Figure 3.53 depicts the prototype we developed for the interactive configuration of twin screw extruders that uses fast ID simulations to prepare functional zones for expensive FEM simulations. 

To toughen PA, 2-5 wt% of either PO, elastomer, ionomer, acidified or epoxidized copolymer may be added. PA/PO blends of type (2) were developed to improve dimensional stability and to reduce water absorbency of PA. Alloying PA with PO reduces the rate of water migration to and from the blend, but not the inherent water absorption of PA [Utracki and Sammut, 1991, 1992]. The alloying is either a two- or three-step reactive process (1°) acidification of PO, (2°) preparation of a compatibilizer, and (3°) compounding PP, PA, and the compatibilizer. Usually, the reactive blending is carried out in a twin screw extruder [Nishio et al., 1990 Hu and Cartier, 1998], Since it may cause reduction of the blend crystallinity (thus performance), the extend must be optimized. The rigid PA/PP blends usually comprise PA PP =... 

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