Records of Analysis

Sampling points for analysis should be planned in order to give the whole record of analysis, e.g. in oil production from the well via processing facilities to the export facilities. Correlation with plant parameters such as temperatures, pressures, flow rates and, stream compositions can provide valuable records. Emphasis on chemical analysis should be incorporated in the design of process plant. Automatic analysis systems especially those using ion-sensitive electrodes with recording of data are recommended. 

RECORDING AND DOCUMENTATION Detailed Recording of Analysis Report Preparation Report over seen by members Signing off the report by Team Report submission... 

However curves summing all measured levels may a bit conceal some weighty information about course of damaging. From this reason it is necessary to pay attention even detail analysis of individual measured levels. Example of distinguishable number of counts and record of counts fiequency in all levels summing curve in comparison with same records in some selected levels shows the Fig.7. 

In a titrimetric method of analysis the volume of titrant reacting stoichiometrically with the analyte provides quantitative information about the amount of analyte in a sample. The volume of titrant required to achieve this stoichiometric reaction is called the equivalence point. Experimentally we determine the titration s end point using a visual indicator that changes color near the equivalence point. Alternatively, we can locate the end point by recording a titration curve showing the titration reaction s progress as a function of the titrant s volume. In either case, the end point must closely match the equivalence point if a titration is to be accurate. Knowing the shape of a titration... 

The principal tool for performance-based quality assessment is the control chart. In a control chart the results from the analysis of quality assessment samples are plotted in the order in which they are collected, providing a continuous record of the statistical state of the analytical system. Quality assessment data collected over time can be summarized by a mean value and a standard deviation. The fundamental assumption behind the use of a control chart is that quality assessment data will show only random variations around the mean value when the analytical system is in statistical control. When an analytical system moves out of statistical control, the quality assessment data is influenced by additional sources of error, increasing the standard deviation or changing the mean value. 

A database management system (DBMS) is used by most LIMS systems for storing data. Examples of commercially available DBMS are DB2, DBASE, Informix, INGRES, ORACLE, and RDB. AH of these DBMS conform to the "relational" model developed by Codd (19). Eigure 3 demonstrates the use of a relational DBMS for storing LIMS data. Here data is grouped by type so customer and analysis requests are stored separately from sets of sample information which are, in turn, stored separately from sets of analysis results. Individual records are linked or related by unique identification data. 

It is axiomatic that sales analysis depends on detailed records of sales of a specific chemical to a specific company. Paramount to the success of such studies is the existence of data recorded on a systematic and continuous basis. It follows that these studies are done best by an ia-house staff on products already produced by the company. However, on occasion, a product new to the company can be studied by the ia-house group with the assistance of their field sales force. For example, a producer of polypropylene could use its people to secure data on the consumption of other thermoplastics by their customers. Such an exercise might identify opportunities for a new producer, but a more detailed marketing research study would probably be done before entry iato the new product area was made. 

Market researchers doing sales analysis usually have an excellent record of accuracy over the short term. This is a result of good data, good judgment, and the easier predictabiUty of events a year ahead rather than three or five years ahead. In the case of a completely new product, the first year or two can be difficult and the analyst either too optimistic or too conservative. 

Seismie analysis is carried out for all important engineering structures such as dams, bridges and nuclear power plants. For regions where these are to be located the likely expectations of an earthquake as well as the extent of its magnitude must be assessed on the basis of the seismic history and the earthquake records of the region (Figures 14.12 to Figure 14.16). Based on these and other factors such as soil stratification, site dependent response spectra are determined. These are the RRS for equipment mounted... 

A depth profile is a record of the variation of a property (such as composition) as a function of depth. Some of the techniques in this volume have essentially no intrinsic depth profiling capabilities the signal is representative of the material integrated over a fixed probing depth. Most, however, can vary the depth probed by varying the condition of analysis, or by removing the surface, layer by layer, while collecting data. 

Names and training records of staff involved in sampling and analysis, or details of contract analysts and any quality standards/accreditation schemes with which they comply. 

The audit team, through its systematic analysis, should document areas that require corrective action as well as where the process safety management system is effective. This provides a record of the audit procedures and findings and serves as a baseline of operation data for future audits. It will assist in determining changes or trends in future audits. 

If Cm -I- 3Cii > 0, a centered simple wave will be produced by impact loading, and a record of this waveform suffices to determine the entire uniaxial stress-strain relation over the range of strains encountered. Vitreous silica is a material responding in this manner, and its coefficients have been determined by Barker and Hollenbach [70B01] (see also [72G02]) on the basis of a simple-wave analysis. 

This report is by Battelle Columbus Division to the Line Pipe Research Supervisory Committee of the American Gas Association. It presents an analysis of statistical data obtained from reports of lea)c or rupture (service) incidents and test failures in natural gas transmission and gathering lines over the 14.5 year period from 1970 through June, 1984. All gas transmission companies were required to notify the Office of Pipeline Safety Operations in the event of a "reportable" incident, as defined by the Code of Federal Regulations. The purpose of the study is to organize the reportable incident data into a meaningful format from which the safety record of the industry can be assessed. 

Raw data The original records from which reliability data are extracted the facility records of equipment failure, repair, outage, and exposure hours or demands that require analysis and encoding in order to be placed into data elements. 

The Guggenheim method requires that data be taken at constant time increments equal to At. In the past this was often a disadvantage, particularly when the experiment was not designed to be analyzed by this method, but with modem instm-mental methods of analysis it is common to acquire a continuous record of instrument response as a function of time, so that data can be taken from this record at any desired times. 

A wide range of analysis instruments, either of the portable or permanently installed type, can be used. The latter will frequently be recording instruments and may have control capabilities. Various principles are employed in analysis equipment, including ... 

Once the best method of dealing with interferences has been decided upon and the most appropriate method of determination chosen, the analysis should be carried out in duplicate and preferably in triplicate. For simple classical determinations the experimental results must be recorded in the analyst s notebook. However, many modern instruments employed in instrumental methods of analysis are interfaced with computers and the analytical results may be displayed on a visual display unit, whilst a printer will provide a printout of the pertinent data which can be used as a permanent record. 

The use of a catalyst with oxidase enzyme is an example of the use of a combined enzyme system, which illustrates the wide potential offered by multi-enzyme electrode systems. Various enzymes can be arranged to work sequentially to transform quite complex substances and eventually produce a measurable concentration-dependent change, which is detected by the output signal and recorded for analysis. 

It is obvious that a record of the kind in Figure 7-1 can yield valuable information about an unknown mineral in the minimum time at little cost. The x-ray emission spectrograph may well become the most valuable single tool for the qualitative analysis of minerals. Its advantages are obvious enough to make further discussion supererogatory. 

The mass spectrometer sampling capillary or the dispersive infra-red analyzers used for continuous analysis and monitoring of the gas phase composition are situated between the reactor and the sampling valve, as close to the reactor as possible, in order to avoid any delay in the recording of changes in the composition of reactants or products. This delay should be taken into account when plotting simultaneously the time dependence of catalyst potential or current and gas phase concentration of the reactants or products. 

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