Tetracycline liquid chromatography-mass spectrometry

Lindsey M.E., M. Meyer, and E.M. Thurman (2001). Analysis of trace levels of sulfonamide and tetracycline antimicrobials in groundwater and surface water using solid-phase extraction and liquid chromatography/mass spectrometry. Analytical Chemistry 73 4640-4646. [Pg.273]

WJ Blanchflower, RJ McCracken, AS Haggan, DG Kennedy. Confirmatory assay for the determination of tetracycline, oxytetracycline, chlortetracycline and its isomers in muscle and kidney using liquid chromatography-mass spectrometry. J Chromatogr B 692 351-360, 1997. [Pg.683]

Aga, D.S., S. O Connor, S. Ensley, et al. 2005. Determination of the persistence of tetracycline antibiotics and their degradates in manure-amended soil using enzyme-linked immunosorbent assay and liquid chromatography-mass spectrometry. J. Agric. Food Chem. 53 7165-7171. [Pg.184]

P.J. Kijak, M.G. Leadbetter, M.H. Thomas, E.A. Thomson, Confirmation of oxytetracycline, tetracycline and chlortetracycline residues in milk by particle-beam liquid chromatography-mass spectrometry, Biol. Mass Spectrom., 20 (1991) 789. [Pg.102]

Lindsey ME, Meyer M, Thurman EM (2001) Analysis of Trace Level of Sulfonamide and Tetracycline Antimicrobials in Groundwater and Surface Water Using Solid-Phase Extraction and Liquid Chromatography/Mass Spectrometry. Anal Chem 73, 4640-4646... [Pg.430]

FSIS laboratories also use chemical techniques and instrumentation to identify select antibiotic residues. The tetracyclines of interest are identified by thin layer chromatography. Sulfonamides are detected and quantified by fluorescence thin lay chromatography and confirmed by gas chromatography/mass spectrometry. Amoxicillin and gentamycin are identified and/or quantified by high pressure liquid chromatography. Similar techniques are used to identify ionophores and other antimicrobials of interest. [Pg.141]

Tricyclazole and tetracycline have been determined by gas chromatography - mass spectrometry [247]. Persistent tetracycline residues have been determined in soil by high-performance liquid chromatography with electrospray ionisation tandem mass spectrometry [248]. [Pg.111]

For confirmatory assay, liquid chromatography-tandem mass spectrometry (LC-MS/MS) is becoming more frequently used in the analysis of OTC owing to its high sensitivity and ability. Electrospray ionization (ESI) [55-57] and atmospheric pressure chemical ionization (APCI) [41] methods combined with tandem mass spectrometry are favored because of their higher sensitivity and better reproducibility. Hamscher et al. [58] developed a method for the determination of persistent TC residues in soil fertilized with manure by HPLC tandem mass spectrometry, MS-MS, and confirmation by MS-MS-MS. Zhu et al. [59] developed an LC-tandem mass spectrometry for the analysis of common tetracyclines in water. The detection limit for oxytetracycline was 0.21 pg/L. Lykkeberg et al. [60] used LC-MS/MS for determination of oxytetracycline and its impurities EOTC, TC, ETC, ADOTC, oc-AOTC, and /i-AOTC. [Pg.111]

Yang S, Cha J, Carlson K (2005) Simultaneous extraction and analysis of 11 tetracycline and sulphonamide antibiotics in influent and effluent domestic wastewater by solid-phase extraction and liquid chromatography-electrospray ionization tandem mass spectrometry. J Chromatogr A 1097 40-53... [Pg.238]

Hamscher G., S. Sczesny, H. Hdper, and H. Nau (2002). Determination of persistent tetracycline residues in soil fertilized with liquid manure by high-performance liquid chromatography with electron spray ionization tandem mass spectrometry. Analytical Cheminstry 74 1509-1518. [Pg.264]

Coupling of liquid chromatography with mass spectrometry provides unequivocal online spectrometric identification of tetracycline antibiotics in animal-derived foods. Typical applications of mass spectrometry in confirming tetracycline residues in edible animal products describe coupling of liquid chromatography with mass spectrometry via particle-beam (280), electrospray (292), or atmospheric pressure chemical ionization (307), using negative-ion detection interfaces. [Pg.999]

MC Carson, MA Ngoh, SW Hadley. Confirmation of multiple tetracycline residues in milk and oxytetracycline in shrimp by liquid chromatography-particle beam mass spectrometry. J Chromatogr B 712 113-128, 1998. [Pg.682]

H Oka, Y Ikai, J Hayakawa, K Masuda, KI Harada, M Suzuki. Improvement of chemical analysis of antibiotics. 19. Determination of tetracycline antibiotics in milk by liquid chromatography and thin-layer chromatography fast atom bombardment mass spectrometry. J AOAC Int 77 891-895, 1994. [Pg.683]

Pena A, Lino CM, Alonso R, Barcelo D, Determination of tetracycline antibiotic residues in edible swine tissues by liquid chromatography with spectrofluorometric detection and confirmation by mass spectrometry, J. Agric. Food Chem. 2007 55(13) 4973-4979. [Pg.223]

Fang Y, Zhai H, Zho Y, Determination of Multi-Residue Tetracyclines and Their Metabolites in Milk by High Performance Liquid Chromatography-Tandem Mass Spectrometry, Agilent Technologies Application Note, Wilmington, DE, 2009. [Pg.260]

Blasco C, Corcia A, Pico Y, Determination of tetracyclines in multi-specie animal tissues by pressurized liquid extraction and liquid chromatography-tandem mass spectrometry, FoodChem. 2009 116 1005-1012. [Pg.260]

Cherlet M, ScheUcens M, Croubels S, De Backer P, Quantitative multi-residue analysis of tetracyclines and their 4-epimers in pig tissues by high-performance liquid chromatography combined with positive ion electrospray ionization mass spectrometry, Anal. Chim. Acta 2003 492 199-213. [Pg.260]

Castellari M, Gratacos-Cubarsi M, Garcia-Regueiro 1, Detection of tetracycline and oxytetracycline residues in pig and calf hair by ultra-high performance liquid chromatography tandem mass spectrometry, J. Chromatogr. A 2009 1216 8096-8100. [Pg.260]

Anderson W, Roybal J, Gonzales S, et al.. Determination of tetracycline residues in shrimp and whole milk using liquid chromatography with ultraviolet detection and residue confirmation by mass spectrometry. Anal. Chim. Acta 2005 529- 145-150. [Pg.260]

Khong S-P, Hammel Y-A, Guy P, Analysis of tetracyclines in honey by high-performance liquid chromatography-tandem mass spectrometry, Rapid Commun. Mass Spectrom. 2005 19 493-502. [Pg.260]

Zhu, J., Snow, D.D., Cassada, D.A., Monson, S.J., and Spalding, R.F. (2001) Analysis of oxytetracycline, tetracycline, and chlortetracycline in water using solid-phase extraction and liquid chromatography-tandem mass spectrometry. Journal of Chromatography A 928, 177-186. [Pg.726]

Tso J, Dutta S, Inamdar S, Aga DS. Simultaneous analysis of free and conjugated estrogens, sulfonamides, and tetracyclines in runoff water and soils using solid-phase extraction and liquid chromatography—tandem mass spectrometry. J Agri Food Chem 2011 59(6) 2213-22. [Pg.408]

Bogialli S, Coradazzi C, Di Corcia A, Lagana A, Sergi M. A rapid method based on hot water extraction and liquid chromatography—tandem mass spectrometry for analyzing tetracycline antibiotic residues in cheese. J AO AC Int 2007 90 864—71. [Pg.475]

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