Inductively coupled plasma overview

Inductively coupled plasma mass spectrometry is now such an important technique in archaeology, as elsewhere, that we devote a whole chapter to it. There are now a number of different ICP MS modes of operation (solution analysis, laser ablation, multicollector, high resolution) this chapter provides a general overview. Further description of the instrumentation for ICP MS may be found in Harris (1997) and Montaser (1998). Some general applications of solution ICP MS are discussed by Date and Gray (1989), Platzner (1997), and Kennett et al. (2001). 

Figure 2.12 Overview of different sample introduction systems in an inductively coupled plasma source. (]. S. Becker and H. ]. Dietze, Spectrochim. Acta 53B, 1475 (1998). Reproduced by permission of Elsevier.)...

This multiauthored book aims at highlighting the role played by atomic and mass spectrometry (with particular reference to atomic absorption spectrometry, inductively coupled plasma atomic emission spectrometry and inductively coupled plasma mass spectrometry) in supporting and promoting research and control of foodstuffs and food commodities as regards both essential and potentially toxic chemical elements. The progress made so far in this field is overviewed and emphasis is put on the open problems that require further investment and development in the public and private sectors. 

Pruszkowski, E. Neubauer, K. Thomas, R. An overview of clinical applications by inductively coupled plasma mass spectrometry. At. Spectrosc. 1998,19 (4), 111-115. 

Here the discussion focuses on the analytical procedure adopted to determine trace metals concentration in sea water in the dissolved phase. Particular attention will be given to the procedures preceding the analytical measurement (sampling, sample treatment and storage), the analytieal determination of total concentration by DPASV and Inductively Coupled Plasma Mass Speetrometry (ICP-MS) the contamination control procedure will also be discussed. The direct DPASV procedure for determining metal complexation in sea water is reported in detail and after a discussion of theoretical aspects an outline of the experimental procedure is presented. Finally, an overview of the distribution in the Southern Ocean of some metals of particular interest is examined and the evaluation of traee metals distribution is carried out also by comparison with results obtained in different geographical areas. 

See also Atomic Emission Spectrometry Inductively Coupled Plasma. Atomic Mass Spectrometry Inductively Coupled Plasma. Liquid Chromatography Overview. Mass Spectrometry Eiectrospray. 

Flame atomic absorption was until recently the most widely used techniques for trace metal analysis, reflecting its ease of use and relative freedom from interferences. Although now superceded in many laboratories by inductively coupled plasma atomic emission spectrometry and inductively coupled plasma mass spectrometry, flame atomic absorption spectrometry still is a very valid option for many applications. The sample, usually in solution, is sprayed into the flame following the generation of an aerosol by means of a nebulizer. The theory of atomic absorption spectrometry (AAS) and details of the basic instrumentation required are described in a previous article. This article briefly reviews the nature of the flames employed in AAS, the specific requirements of the instrumentation for use with flame AAS, and the atomization processes that take place within the flame. An overview is given of possible interferences and various modifications that may provide some practical advantage over conventional flame cells. Finally, a number of application notes for common matrices are given. 

See also Atomic Emission Spectrometry Inductively Coupled Plasma. Atomic Spectrometry Overview. 

See also Activation Anaiysis Neutron Activation. Air Anaiysis Workpiace Air. Amperometry. Atomic Absorption Spectrometry Principies and Instrumentation. Atomic Emission Spectrometry Principles and Instrumentation Inductively Coupled Plasma. Atomic Mass Spectrometry Inductively Coupled Plasma. Capillary Electrophoresis Overview. Cement. Elemental... 

See also Atomic Mass Spectrometry Inductively Coupled Plasma Laser Microprobe. Gas Chromatography Mass Spectrometry. Liquid Chromatography Liquid Chromatography-Mass Spectrometry. Mass Spectrometry Ionization Methods Overview Atmospheric Pressure Ionization Techniques Electrospray Liquid Secondary Ion Mass Spectrometry Matrix-Assisted Laser Desorption/ionization. Surface Analysis Secondary Ion Mass Spectrometry of Polymers Laser Ionization. 

Inductively Coupled Plasma. Fire Assay. Gravimetry. Ion Exchange Overview. Sampling Theory Practice. Titrimetry Overview. 

See also Atomic Absorption Spectrometry Principles and Instrumentation. Atomic Emission Spectrometry Inductively Coupled Plasma. Cosmetics and Toiletries. Derivatization of Analytes. Electrophoresis Is-otachophoresls. Environmental Analysis. Enzymes Overview. Extraction Supercritical Fluid Extraction Solid-Phase Extraction Solid-Phase Microextraction. Ion Exchange Ion Chromatography Applications. Liquid Chromatography Reversed Phase Liquid Chromatography-Mass Spectrometry. Nuclear Magnetic Resonance Spectroscopy - Applicable Elements Carbon-13 Phosphorus-31. Perfumes. 

See also Atomic Absorption Spectrometry Interferences and Background Correction. Atomic Emission Spectrometry Principles and Instrumentation Interferences and Background Correction Flame Photometry Inductively Coupled Plasma Microwave-Induced Plasma. Atomic Mass Spectrometry Inductively Coupled Plasma Laser Microprobe. Countercurrent Chromatography Solvent Extraction with a Helical Column. Derivatization of Analytes. Elemental Speciation Overview Practicalities and Instrumentation. Extraction Solvent Extraction Principles Solvent Extraction Multistage Countercurrent Distribution Microwave-Assisted Solvent Extraction Pressurized Fluid Extraction Solid-Phase Extraction Solid-Phase Microextraction. Gas Chromatography Ovenriew. Isotope Dilution Analysis. Liquid Chromatography Ovenriew. 

Balcerzak, M. (2003) An overview of analytical applications of time of flight-mass spectrometric (TOF-MS) analyzers and an inductively coupled plasma-TOF-MS technique. Analytical Sciences, 19, 979-989. 

Durrant, S. F. (1993). Alternatives to all-argon plasmas in inductively coupled plasma mass spectrometry (ICP-MS) An overview. Fresenius J.Atul. Chem. 347(10-11), 389-392. 

HiU, S. J., Pitts, L. J., and Fisher, A. S. (2000). High-performance liquid chromatography-isotope dilution inductively coupled plasma mass spectrometry for speciation studies An overview. Trends Anal. Chem. 19(2), 120. 

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