Adhesion tests accelerated testing

Metal specimens coated with the various blends were immersed in water in an accelerated test to determine the effect of high humidity. Cellulose acetate butyrate blends containing carboxylated polyesters prepared with hexahydroterephthalic acid [H(NPG), T50H(NPG)] were particularly susceptible to moisture and failed the adhesion test after immersion for only 0.5 hour similar blends containing T50I(NPG) extended with dianhydride Via or with PMDA passed the adhesion test after immersion for 16 hours. When coatings on cold-rolled steel of cellulose acetate butyrate (EAB-381-0.5) blends containing 1% of each of the... 

Figures 30.17-30.19 depict the durability of the surface treatments examined with ETA-3183, which is the most difficult one to modify the surface effectively among samples employed. Because the water can reach the interface directly through cross-cuts, this accelerated adhesion test was much more severe when cross-cuts were...

It is evident in Figures 30.18 and 30.19 that, after the accelerated adhesion test, the primer-coated air LPCAT treated TPOs showed poor adhesion performance as compared to argon and methane LPCAT-treated TPOs. This is a clear indication that air-plasma treatment can achieve the paintable surface but cannot provide the treated surface that can be painted in a durable manner. The poor durability can be attributed to (1) the water-sensitive nature of adhesion and (2) the excessive degradation of polypropylene that causes weaker boundary layer. 

In the case of direct application of E-coat to IVD specimens (one of the systems that showed excellent adhesion performance in both the tape test and the accelerated adhesion test), due to the high throw power of the E-coating process, the deep penetration of E-coat into the porous IVD structure creates mechanical interlocking and thus strong adhesion. Because of this development of mechanical interlocking, neither the tape test nor the accelerated adhesion test could distinguish the effect of plasma treatment on adhesion performance. 

EN 14814 2007 Adhesives for thermoplastic piping systems for fluids under pressure. Specifications EN 1903 2008 Adhesives - test method for adhesives for plastic or rubber floor coverings or wall coverings -determination of dimensional changes after accelerated ageing... 

Static fatigue is the slow growth of a crack under ambient stress and environmental conditions. The static fatigue failure in oxide materials can be accelerated by moisture or hydrogen, which weaken the chemical bonds at the crack tip. This moisture can be supplied by breathing on the films to condense moisture. This moisture condensation method is an easy way to quickly determine if the residual film stresses are high or the adhesion is poor, and the nature (compressive or tensile stress) of the stresses in a film. This moisture condensation is the basis of the bad breath adhesion test (Sec. 12.5.2). 

One of the more weird adhesion tests is the Mattox bad breath test . In this test, a person breathes on the film to condense moisture. If the film has a high residual stress, the moisture accelerates fracture propagation. When the film fails it blisters or flakes. Obviously, the uninformed individual attributes the failure to the bad breath of the tester. This test has the advantage that it can be done immediately and without equipment. If the film cannot pass this test it will probably fail in the future. The condensing breath often contaminates the film surface for further use and the test could probably be improved to be non-destructive. 

The routine compositional and functional testing done on the adhesives includes gas chromatographic testing for purity, potentiometric titrations for acid stabilizer concentrations, accelerated thermal stabiUty tests for shelf life, fixture time cure speed tests, and assorted ASTM tests for tensile shear strengths, peel and impact strengths, and hot strengths. 

Specification for electroplated coatings of 65/35 tin/nickel alloy Method for the evaluation of results of accelerated corrosion tests on metallic coatings Methods of test for paints Cross-cut test Pull-off test for adhesion Resistance to artificial weathering (enclosed carbon arc) and Addendum No. 1 Resistance to continuous salt spray Notes for guidance on the conduct of natural weathering test... 

There is a need for an accurate assessment of the mechanism of cathodic debonding of thick adherends. This would contribute to better control over the selection of formulations resistant to attack. One of the objectives of this work was to develop an accelerated screening test. The screening test was used to evaluate the relative performance profiles of a number of commercial adhesives which were recommended for marine applications. It is hoped that a screening test such as this one could be used to isolate measurable primer properties which can be related to the long term prospectus of the primer, and the variability of this prospectus under permutation of substrate type or additives. 

CRS which had been phosphated prior to bonding exhibited a significant enhancement of durability and corrosion resistance under the same accelerated conditions (Figure 4). The crystalline barrier layer restricted the exposure of the metal oxide to moisture by reducing the rate of water penetration at the interface. Even samples exposed to the cycle test were able to maintain failure within the adhesive for up to 10 days, after which varying amounts of interfacial failure were noted. Again, room temperature control samples maintained initial joint strength and failure remained cohesive within the adhesive. 

The extent of adhesive bond failure under corrosive environments is greatly accelerated when cyclic mechanical stresses are imposed on the adhesive bond during exposure. Three to four orders of magnitude reduction in fatigue life of adhesive bonds is observed for bonds exposed to environment prior to fatigue testing. 

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