Rotary pressure filter

In the propane process, part of the propane diluent is allowed to evaporate by reducing pressure so as to chill the slurry to the desired filtration temperature, and rotary pressure filters are employed. Complex dewaxing requires no refrigeration, but depends on the formation of a soHd urea—/ -paraffin complex which is separated by filtration and then decomposed. This process is used to make low viscosity lubricants which must remain fluid at low temperatures (refrigeration, transformer, and hydraulic oils) (28). 

McFadyen-Stevens reaction, 13 571 McGaskell rotary pressure filter, 11 374 McLafferty ester pyrolysis reaction, 20 43 MCLs (maximum contaminant levels), 17 804... 

CTA and PTA filtration using rotary pressure filters, proven in commercial operation on PTA since 2007, resulting in a significant reduction in equipment count, improved reliability and lower energy usage. 

The principle of pressure filters differs from that of vacuum filters only in the fact that a positive rather than a negative pressure is used to force the filtrate through the filter membrane. On this account, pressures as high as feasible can be attained. Consequently, materials not filterable on vacuum filters may be handled by this means. Filter presses are of three general types those employing both plates and frames, those using recessed plates, and continuous rotary pressure filters. 

Rotary vacuum filters are used in ketone dewaxers and rotary pressure filters are used in propane plants. The principles of operation are the same. A typical filter is shown in Figure 30. 

Rotary Pressure filters are used to filter the slurry. Filtration rate is a function of the pressure drop across the filter. The temperature of the slurry also depends on the pressure. This requires carefully controlled pressure balance from the filter feed dmm to the filters and to the filtrate drum. If the pressure in the filtrate dmm is too high the temperature will be high and the resulting dewaxed oil pour point will be too high. If the filter pressure is not increased to maintain the Delta P then filtration rate will also be reduced. 

Another option available with rotary vacuum dmm filters is fiiU enclosure. This enables operation under nitrogen or other atmospheres, for reasons such as safety, prevention of vapor loss, etc. Enclosure may also be used to prevent contamination of the material being filtered or to confine the spray from washing nozzles. The rotary dmm filter also can be enclosed in a pressure vessel and operated under pressure. 

Most continuous pressure filters available (ca 1993) have their roots in vacuum filtration technology. A rotary dmm or rotary disk vacuum filter can be adapted to pressure by enclosing it in a pressure cover however, the disadvantages of this measure are evident. The enclosure is a pressure vessel which is heavy and expensive, the progress of filtration cannot be watched, and the removal of the cake from the vessel is difficult. Other complications of this method are caused by the necessity of arranging for two or more differential pressures between the inside and outside of the filter, which requires a troublesome system of pressure regulating valves. 

Drum Filters. The rotary dmm filter, also borrowed from vacuum filtration, makes relatively poor use of the space available in the pressure vessel, and the filtration areas and capacities of such filters cannot possibly match those of the disk pressure filters. In spite of this disadvantage, however, the pressure dmm filter has been extensively developed. 

Following carbonation, the product can be further purified by screening. This screening, also used to control the maximum size of the product, is followed by dewatering (qv). Rotary vacuum filters, pressure filters, or centrifuges are used in the mechanical removal of water. Final drying is accompHshed as with natural calcium carbonate in either a rotary, spray, or flash dryer. Products having mean particle sizes from submicrometers (- O-OS fiTo) to several micrometers are available. 

Rotary Drum Filters The rotaiy drum filter is the most widely used of the continuous filters. There are many design variations, including operation as either a pressure filter or a vacuum filter. The major difference between designs is in the technique for cake discharge, to be discussed later. All the alternatives are characterized by a horizontal-axis drum covered on the cylindrical portion by filter medium over a grid support structure to allow drainage to manifolds. Basic materials of construc tion may be metals or plastics. Sizes (in terms of filter areas) range from 0.37 to 186 m (4 to 2000 ft ). 

The operation of the eontinuous rotary vaeuum filter is illustrated in Figure 4.17. The filter drum is immersed in a bath of slurry from where the liquor is drawn through the filter medium by the pressure drop eaused by the appliea-tion of a vaeuum within the drum. During filtration eake builds up on the outside surfaee of the drum between points A and B as if by eonstant pressure bateh operation. It then travels to point C where it is removed and the eyele repeated. 

Sodium hydrosulfite is produced through the Formate process where sodium formate solution, sodium hydroxide, and liquid sulfur dioxide reacted in the presence of a recycled stream of methanol solvent. Other products are sodium sulfite, sodium bicarbonate, and carbon monoxide. In the reactor, sodium hydrosulfite is precipitated to form a slurry of sodium hydrosulfite in the solution of methanol, methyl formate, and other coproducts. The mixture is sent to a pressurized filter system to recover sodium hydrosulfite crystals that are dried in a steam-heated rotary drier before being packaged. Heat supply in this process is highly monitored in order not to decompose sodium hydrosulfite to sulfite. Purging is periodically carried out on the recycle stream, particularly those involving methanol, to avoid excessive buildup of impurities. Also, vaporized methanol from the drying process and liquors from the filtration process are recycled to the solvent recovery system to improve the efficiency of the plant. 

A rotary drum filter 6 ft in diameter and 8 ft long is to be used to filter a slurry. The drum rotates at 0.5 rpm, and one-third of the drum s surface is submerged in the slurry. A vacuum is drawn in the drum so that a constant pressure drop of 10 psi is maintained across the drum and filter cake. You test the slurry in the lab by pumping it at a constant filtrate rate of 20 gpm through 1 ft2 of the drum filter screen and find that after 1 min the pressure drop is 8 psi and after 3 min the pressure drop is 12 psi. How long will it take to filter 100,000 gal of filtrate from the slurry using the rotary drum ... 

A rotary drum filter is used to filter a slurry. The drum rotates at a rate of 3 min/cycle, and 40% of the drum surface is submerged in the slurry. A constant pressure drop at 3 psi is maintained across the filter. If the drum is 5 ft in diameter and 10 ft long, calculate the total net filtration rate in gpm that is possible for a slurry having properties as determined by the following lab test. A sample of the slurry was pumped at a constant flow rate of 1 gpm through 0.25 ft2 of the filter medium. After 10 min, the pressure difference across the filter had risen to 2.5 psi. The filter medium resistance may be neglected. 

A slurry is being filtered at a net rate of 10,000 gal/day by a plate and frame filter with 15 frames, with an active filtering area of 1.5 ft2 per frame, fed by a positive displacement pump. The pressure drop varies from 2 psi at start-up to 25 psi after 10 min, at which time it is shut down for cleanup. It takes 10 min to disassemble, clean out, and reassemble the filter. Your boss decides that it would be more economical to replace this filter with a rotary drum filter using the same filter medium. The rotary filter operates at a vacuum of 200 mmHg with 30% of its surface submerged and rotates at a rate of 5 min/rev. If the drum length is equal to its diameter, how big should it be ... 

You want to select a rotary drum filter to filter a coal slurry at a rate of 100,000 gal of filtrate per day. The filter operates at a differential pressure of 12 psi, and 30% of the surface is submerged in the slurry at all times. A sample of the slurry is filtered in the lab through a 6 in diameter sample of the filter medium at a constant rate of 1 gpm. After 1 min the pressure drop across this filter is 3 psi, and after 5 min it is 10 psi. If the drum rotates at a rate of 3 rpm, what total filter area is required ... 

A slurry is to be filtered with a rotary drum filter that is 5 ft in diameter and 8 ft long, rotates once every 10 s, and has 20% of its surface immersed in the slurry. The drum operates with a vacuum of 20 in.Hg. A lab test was run on a sample of the slurry using 1/4 ft2 of the filter medium at a constant flow rate of 40 cm3/s. After 20 s the pressure drop was 30 psi across the lab filter, and after 40 s it was 35 psi. How many gallons of filtrate can be filtered per day in the rotary drum ... 

A rotary drum filter is to be installed in your plant. You run a lab test on the slurry to be filtered using a 0.1 ft2 sample of the filter medium at a constant pressure drop of 10 psi After 1 min you find that 500 cm3 of filtrate has passed through the filter, and after 2 min the filtrate volume is 715 cm3. If the rotary drum filter operates under a vacuum of 25 in.Hg with 25% of its surface submerged, determine ... 

A slurry containing 0.2 kg solids/kg water is filtered through a rotary drum filter operating at a pressure difference of 65 kN/m2. The drum is 0.6 m in diameter and 0.6 m long, rotates once every 350 s, and has 20% of its surface submerged in the slurry. 

Filtration is carried out in a plate and frame filter press, with 20 frames 0.3 m square and 50 mm thick, and the rate of filtration is maintained constant for the first 300 s. During this period, the pressure is raised to 350 kN/m2, and one-quarter of the total filtrate per cycle is obtained. At the end of the constant rate period, filtration is continued at a constant pressure of 350 kN/m2 for a further 1800 s, after which the frames are full. The total volume of filtrate per cycle is 0.7 m3 and dismantling and refitting of the press takes 500 s. It is decided to use a rotary drum filter, 1.5 m long and 2.2 m in diameter, in place of the filter press. Assuming that the resistance of the cloth is the same in the two plants and that the filter cake is incompressible, calculate the speed of rotation of the drum which will result in the same overall rate of filtration as was obtained with the filter press. The filtration in the rotary filter is carried out at a constant pressure difference of 70 kN/m2, and the filter operates with 25 per cent of the drum submerged in the slurry at any instant. 

A slurry containing 40 per cent by mass solid is to be filtered on a rotary drum filter 2 m diameter and 2 m long which normally operates with 40 per cent of its surface immersed in the slurry and under a pressure of 17 kN/m2. A laboratory test on a sample of the slurry using a leaf filter of area 200 cm2 and covered with a similar cloth to that on the drum, produced 300 cm3 of filtrate in the first 60 s and 140 cm3 in the next 60 s, when the leaf was under pressure of 84 kN/m2. The bulk density of the dry cake was 1500 kg/m3 and the density of the filtrate was 1000 kg/m3. The minimum thickness of cake which could be readily removed from the cloth was 5 mm. 

A slurry, containing 0.2 kg of solid per kilogram of water, is fed to a rotary drum filter 0.6 m long and 0.6 m diameter. The drum rotates at one revolution in 360 s and 20 per cent of the filtering surface is in contact with the slurry at any instant. If filtrate is produced at the rate of 0.125 kg/s and the cake has a voidage of 0.5, what thickness of cake is produced when filtering with a pressure difference of 65 kN/m2 The density of the solids is 3000 kg/m3. 

It is decided to use a rotary drum filter, 1.5 m long and 2.2 m in diameter, in place of the filter press. Assuming that the resistance of the cloth is the same in the two plants and that the filter cake is incompressible, calculate the speed of rotation of the drum which will result in the same overall rate of filtration as was obtained with the filter press. The filtration in the rotary filter is carried out at a constant pressure difference of 70 kN/m2, and the filter operates with 25 per cent of the drum submerged in the slurry at any instant. 

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