Liquid Chromatography Review

Introduction to fast performance liquid chromatography. Review Buffer preparation, Definitions of pH, Henderson-Hasselbalch equation, and Buffer calculations. 

Quantification. High Pressure Liquid Chromatography. Review of methods for the analysis of antibiotics in biological fluids—I. Nilsson-Ehle, J. liq. Chromat., 1983, 6, 251-293. 

Chen, S. H. and Chuang, Y. J., Analysis of fatty acids by column liquid chromatography. Review, Anal. Chim. Acta, 465, 145-155, 2002. 

High Pressure Liquid Chromatography.- Reviews on the analysis of sugars by h.p.l.c., in which packings and detection techniques are discussed (258 refs.), and on the advantages and limitations of several separation and detection techniques for sugars, including... 

Okamoto M (2002) Reversal of elution order during the chiral separation in high-performance liquid chromatography Review. Journal of Pharmaceutical and Biomedical Analysis 27 401—407. 

High-Pressine liquid Chromatography.- Reviews on the biomedical applications of h.p.l.c.-m.s., and immobilised enzyme reactors in h.p.l.c. detector systems, have included carbohydrate applications. 

High Performance Liquid Chromatography (hpic). Hplc is currently the fastest growing analytical method and is now available in many laboratories. DL-Analysis by hplc has already been described and hplc methods have been reviewed (122). 

Coupled liquid chromatography-gas chromatography is an excellent on-line method for sample enrichment and sample clean-up. Recently, many authors have reviewed in some detail the various LC-GC transfer methods that are now available (1, 43-52). For the analysis of normal phase eluents, the main transfer technique used is, without doubt, concurrent eluent evaporation employing a loop-type interface. The main disadvantage of this technique is co-evaporation of the solute with the solvent. 

E. A. Hogendoom and P. van Zoonen, Coupled-column reversed-phase liquid chromatography in envhonmental analysis (review) , ]. Chromatogr. 703 149-166 (1995). 

The use of multidimensional chromatography in environmental analysis has been reviewed in the literature (1-6). Of the multidimensional systems described in previous chapters, GC-GC liquid chromatography LC-LC and LC-GC, whose applications to environmental analysis will be detailed in this chapter, are the ones most often used in environmental analysis. 

HPLC separations are one of the most important fields in the preparative resolution of enantiomers. The instrumentation improvements and the increasing choice of commercially available chiral stationary phases (CSPs) are some of the main reasons for the present significance of chromatographic resolutions at large-scale by HPLC. Proof of this interest can be seen in several reviews, and many chapters have in the past few years dealt with preparative applications of HPLC in the resolution of chiral compounds [19-23]. However, liquid chromatography has the attribute of being a batch technique and therefore is not totally convenient for production-scale, where continuous techniques are preferred by far. 

New types of ion exchange resins have also been developed to meet the specific needs of high-performance liquid chromatography (HPLC) (Chapter 8). These include pellicular resins and microparticle packings (e.g. the Aminex-type resins produced by Bio-Rad). A review of the care, use and application of the various ion exchange packings available for HPLC is given in Ref. 19. 

For monographs on the use of liquid chromatography to effect resolutions, see Lough, W.J. Chiral Liquid Chromatography, Blackie and Sons London, 1989 Krstulovic, A.M. Chiral Separations by HPLC Ellis Horwood Chichester, 1989 Zief, M. Crane, L.J. Ref. 122. For a review, see Karger, B.L. Anal. Chem., 1967, 39 (8), 24A. 

The use of high performance liquid chromatography (HPLC) for the study of paralytic shellfish poisoning (PSP) has facilitated a greater understanding of the biochemistry and chemistry of the toxins involved. HPLC enables the determination of the type and quantity of the PSP toxins present in biological samples. An overview of the HPLC method is presented that outlines the conditions for both separation and detection of the PSP toxins. Examples of the use of the HPLC method in toxin research are reviewed, including its use in the determination of the enzymatic conversion of the toxins and studies on the movement of the toxins up the marine food chain. 

MERKEN H M and BEECHER G R (2000) Measurement of food flavonoids by high-performance liquid chromatography A review , JAgric Food Chem, 48 (3), 577-99. 

The comprehensive review by Gocan et al. [25] focused specifically on lipophilic-ity measurements by liquid chromatography, including reversed phase, thin-layer, micellar, RP-ion-pair and countercurrent chromatography. 

Mukherjee, P. S. and Karnes, H. T., Ultraviolet and fluorescence derivatization reagents for carboxylic acids suitable for high performance liquid chromatography A review, Biomed. Chromatogr., 10, 193, 1996. 

How does one choose a solvent A review on the strategy for solvent selection in order to achieve extraction or liquid chromatography has appeared [25]. 

Gas and liquid chromatography directly coupled with atomic spectrometry have been reviewed [178,179], as well as the determination of trace elements by chromatographic methods employing atomic plasma emission spectrometric detection [180]. Sutton et al. [181] have reviewed the use and applications of ICP-MS as a chromatographic and capillary electrophoretic detector, whereas Niessen [182] has briefly reviewed the applications of mass spectrometry to hyphenated techniques. 

Worldwide, some 500 LC-FTIR users are registered. A review on the determination of rubber and plastic chemicals by liquid chromatography-spectroscopy has appeared [494]. 

Wilson [664,672] has reviewed multiple hyphenation of liquid chromatography. 

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