Filtration precoat pressure filters

Precoat filtration can be incorporated within a wide range of pressure filters including leaf, multi-element and plate and frame types (see Section 1.4.2). Up to 700 g m of precoat is typically filtered onto the filter medium prior to introduction of the feed suspension. The feed, which may also contain a significant addition of filter aid to improve cake permeability, is filtered until the filtrate flow rate is sufficiently low to warrant cake discharge in the normal way. It is not economical to recover the feed solids from the precoat, and it follows that washing of the solids is not practised. Moreover, the filter aid tends to abrade the pumps used to promote the filtration. Precoat pressure filtration is most often used for the removal of finer particles from dilute suspension where other potential processes would require too high an investment. 

If the vacuum tests are not successfiil because the rate is too slow or, if the tests are successful but the equipment for vacuum filtration would be too large or too costly, or simply because filtration is not achieved, then one has to look at four possible alternatives. These are a bottom feed vacuum filter with precoating flocculating the feed or adding body feed, either for bottom feed or top feed vacuum filters or pressure filtration in all its ramifications, either with or without flocculation or body feed. In certain cases one can even look at precoating pressure filters. In this respect, of course, pressure filters can equally well be centrifugal filters, or compression filters. 

In the precoat and body feed mode, filter aids allow appHcation of surface filtration to clarification of Hquids, ie, filtration of very dilute suspensions of less than 0.1% by volume, such as those normally treated by deep bed filters or centrifugal clarifiers. Filter aids are used in this mode with pressure filters. A precoat is first formed by passing a suspension of the filter aid through the filter. This is followed by filtration of the feed Hquid, which may have the filter aid mixed with it as body feed in order to improve the permeabiUty of the resulting cake. The proportion of the filter aid to be added as body feed is of the same order as the amount of contaminant soHds in the feed Hquid this limits the appHcation of such systems to low concentrations. Recovery and regeneration of filter aids from the cakes normally is not practiced except in a few very large installations where it might become economical. 

Filtration. Any type of clarification is foUowed by filtration through leaf-type vertical or horizontal pressure filters. Carbonatated Hquors, containing calcium carbonate, may require addition of diatomaceous earth as a filter precoat. Phosphatated Hquors are generally filtered with the addition of diatomaceous earth as precoat and body feed. 

In cake or surface filtration, there are two primary areas of consideration continuous filtration, in which the resistance of the filter cake (deposited process solids) is veiy large with respec t to that of the filter media and filtrate drainage, and batch pressure filtration, in which the resistance of the filter cake is not veiy Targe with respect to that of the filter media and filtrate drainage. Batch pressure filters are generally fitted with heavy, tight filter cloths plus a layer of precoat and these represent a significant resistance that must be taken into account. Continuous filters, except for precoats, use relatively open cloths that offer little resistance compared to that of the filter cake. 

In the operation of a filtration system, the filter is first precoated by circulating a mixture of filter aid and clear or filtered liquid from the precoat tank through the filter and back to the precoat tank. This is continued until all the filter aid is deposited on the filter. The body feed injection system is then started and the filter is changed over, with minimum fluctuations in pressure, from precoating to filtering. 

Run No. Filter Module and/or Precoat Type Feed Temp., °F/°C % Solids in Food Vacuum = in. Fig. Pressure = PSI. TIME, MIN. Air Flow Filtrate Precoat Penetration Wash Cake/Precoat Thickness, In. Dia. of Shared Area, In. Cake Weights ... 

The resistivity of the cake, however, very often increases with time. Under the pressure of filtration or the friction of the fluid that continues to pass through the cake, the filtered particles continue to compact and reduce the area available for flow. Section 7.S.4.2 also describes the empirical methods that are used to characterize the compressibility of the cake. It is significant that the particles produced by precipitation from the brine are often highly compressible. At the same time, they have a tendency to become lodged in the pores of the filter medium. Filtration of these particles can become very difficult. The usual solution to this problem is the use of a filter aid. The filter aid is applied to the surface of the filter medium before introducing the brine. This is the precoating operation. Filter aids are selected for their desirable characteristics, and the precoat material protects the pores from penetration by filtered solids while at the same time offering little resistance to the flow. Compression of the precipitates still occurs, and so filter aid ( admix ) is also added in small quantities to the brine to improve the characteristics of the cake. 

Addition of Inert Filter Aids. FUtet aids ate rigid, porous, and highly permeable powders added to feed suspensions to extend the appheabUity of surface filtration. Very dilute or very fine and slimy suspensions ate too difficult to filter by cake filtration due to fast pressure build-up and medium blinding addition of filter aids can alleviate such problems. Filter aids can be used in either or both of two modes of operation, ie, to form a precoat which then acts as a filter medium on a coarse support material called a septum, or to be mixed with the feed suspension as body feed to increase the permeabihty of the resulting cake. 

It is both convenient and reasonable in continuous filtration, except for precoat filters, to assume that the resistance of the filter cloth plus filtrate drainage is neghgible compared to the resistance of the filter cake and to assume that both pressure drop and specific cake resistance remain constant throughout the filter cycle. Equation (18-51), integrated under these conditions, may then be manipulated to give the following relationships ... 

External-Cake Tubular Filters Several filter designs are available with vertical tubes supported by a filtrate-chamber tube sheet in a vertical cylindrical vessel (Fig. 18-115). The tubes may be made of wire cloth porous ceramic, carbon, plastic, or metal or closely wound wire. The tubes may have a filter cloth on the outside. Frequently a filter-aid precoat will be applied to the tubes. The prefilt slurry is fed near the bottom of the vertical vessel. The filtrate passes from the outside to the inside of the tubes and into a filtrate chamber at the top or the bottom of the vessel. The sohds form a cake on the outside ofthe tubes with the filter area actually increasing as the cake builds up, partially compensating for the increased flow resistance of the thicker cake. The filtration cycle continues until the differential pressure reaches a specified level, or until about 25 mm (1 in) of cake thickness is obtainea... 

Body-aid (i.e., the filter-aid) and precoating are often mentioned in connection with pressure filtration and the difference in their application is (1) Body aid is used when the slurry is low in solids content with fine and slimy particles that are difficult to filter. To enhance filtration coarse solids with large surface area are added to the slurry and serve as a body-aid that captures and traps in its interstices... 

Another method, which is even more successful in preventing binding of the septum, is the use of a precoat.53 Before filtration is begun a coating of 2-6 in (5-15 cm) of diatomaceous earth or perlite filter aid is deposited on the surface of the septum. During filtration operations the scraper is set so that it slowly removes the precoat and, of course, with it the materials that would have plugged the filter. Since the precoat causes a considerable pressure drop, the rate of filtration is slowed down. Flow rates may vary from 2 to 50 gal/hr/ft2 (0.025-0.60 m/hr). The precoat material costs around 3 or 40/lb and is used at the rate of 10- 15 lb/1,000 gal of feed (1,200 to 1,800 kg/m3). 

The material to be filtered is fed into the vessel under pressure, and separation takes place with the solids being deposited on the leaf surface, and the liquid passing through the drainage system and out of the filter. Cycle times are determined by pressure, cake capacity or batch quantity. Where particularly fine solids must be removed, a layer of precoat material may be deposited on the leaves prior to filtration, using diatomaceous earth, Perlite, or other suitable precoat materials. 

Filtration. Filtration in Washington wineries is performed almost exclusively with plate-and-frame filter presses. In some cases, these filters have wide frames so that they are capable of performing diatomaceous earth filtrations. There is only one stainless steel, screened, diatomaceous earth, pressure-leaf filter in use in the Washington wine industry. Two major wineries have found they can utilize a paper septum over a medium pad in their plate-and-frame filters. This allows them to precoat and body feed with diatomaceous earth as the wine is filtered. This accomplishes both a coarse and medium filtration in one movement of the wine. 

Conventional pressure or vacuum filtration techniques are widespread in industry for separating cells and other biological materials from a liquid phase which can be solvent based or aqueous. A pressure differential between the dirty and clean sides of the filter, created with over pressure or vacuum, provides a driving force for the liquid to be forced through the filter material which retains solids above a particular size. This type of filter is often used in conjunction with a precoat material on the filter to improve the separation characteristics. 

---