Solvent microextraction

Jeannot, M.A. and F.F. Cantwell. 1996. Solvent microextraction into a single drop. Anal. Chem. 68 2236-2240. 

Solvent Liquid/liquid extraction (LLE) Steam distillation/extraction (SDE) Solvent microextraction (SME) - SDME - LPME - DLLME Headspace-solvent-microextraction (HS-SME) - Headspace single-drop microextraction (HS-SDME) - Headspace liquid phase microextraction (HS-LPME) ... 

HSPE Headspace solvent microextraction HS extraction of volatile compounds into a single drop of solvent, which is then injected into the GC For volatile, GC-amenable compounds, particularly in water and flavor analysis... 

Yamini, Y., M. Hojjati, and M. Haji-Hosseini. 2004. Headspace solvent microextraction. Talanta 62 265-270. 

Ma, M. and F.L. Cantwell. 1999. Solvent microextraction with simultaneous back-extraction for sample cleanup and preconcentration Preconcentration into a single microdrop. Anal. Chem. 71 388-393. 

Bagheri, H. and A. Salemi. 2006. Headspace solvent microextraction as a simple and highly sensitive sample pretreatment technique for ultra trace determination of geosmin in aquatic media. J. Sep. Sci. 29 57-65. 

Bagheri, H., A. Saber, and S.R. Mousavi. 2004. Immersed solvent microextraction of phenol and chloro-phenols from water samples followed by gas chromatography-mass spectrometry. J. Chromatogr. A 1046 27-33. 

Headspace solvent microextract (HSME) of aniseed contained 90% f-anethole (Abbas et al., 2005). 

Abbas, B.S., Jabbari, A. and Yamini, Y. (2005) Headspace solvent microextraction a very rapid method for identification of volatile components of Iranian Pimpinella anisum seed. Analytics Chimica Acta 530(1), 155-161. 

King S, Meyer JS, and Andrews ARJ. Screening method for polycychc aromatic hydrocarbons in soil using hollow fiber membrane solvent microextraction. J. Chromatogr. A 2002 982 201-208. 

The mode of extraction for PAHs is highly dependent on the matrix. For solid-based matrices such as food samples, sediments, soil, marine organisms, etc. extraction methods such as Soxhlet extraction with nonpolar solvent [35 6], hollow fiber membrane solvent microextraction (HFMSME) [10], pressimzed hquid extraction (PLE) [37,38], sonication extraction [3], microwave-assisted extraction (MAE) [3], supercritical fluid extraction, (SEE) [39], accelerated solvent extraction (ASE) [40], cold extraction [41], soxtec extraction [42], microwave-assisted alkaline saponification (MAAS) [43], dynamic microwave-assisted extraction (DMAE) [44], add-induced cloud point extraction (ACPE) [45], methanolic saponification extraction (MSE) [7], etc. are employed. Of all these, Soxhlet extraction is the most common for solid samples and has achieved excellent extraction with high-level recovery but its setback is the high consmnption of solvent and time associated with it. 

Przyjazny, A. and Kokosa, J.M. Analytical characteristics of the determination of benzene, toluene, ethylbenzene and xylenes in water by headspace solvent microextraction. Journal of Chromatography A 2002, 977 (2), 143-153. 

Bahramifar, N. Yamini, Y. Shariati-Feizabadi, S. and Shamsipur, M. Trace analysis of methyl ferf-butyl ether in water samples using headspace solvent microextraction and gas chromatography-flame ionization detection. Journal of Chromatography A 2004,1042 (1-2), 211-217. 

Psillakis, E. and Kalogerakis, N. Application of solvent microextraction to the analysis of nitroaromatic explosives in water samples. Journal of Chromatography A 2001,907 (1-2), 211-219. 

Kaykhaii, M. Nazari, S. and Chamsaz, M. Determination of aliphatic amines in water by gas chromatography using headspace solvent microextraction. Talanta 2005,65 (1), 223-228. 

Pena-Pereira, F. Costas, M. Bendicho, C. Lavilla, I. A Solvent Microextraction Approach for Envirornnenlal Analysis Colorimetric Assay for Phosphoms Determination in Natural Waters. J. Chem. Educ. 2014,91, 586-589. 

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