Diagram instrumentation

The research [5] showed the inspection records fulfilled by different instruments are very close each other. Nevertheless some of the instruments are able to put an information out to a computer, main inspection records usually are performed as chart diagrams of the LMA and LF channels. 

Fig. 1 shows the block diagram of the vibrometer, in which the most sensible to small phase variations interferometric scheme is employed. It consists of the microwave and the display units. The display unit consists of the power supply 1, controller 2 of the phase modulator 3, microprocessor unit 9 and low-frequency amplifier 10. The microwave unit contains the electromechanical phase modulator 3, a solid-state microwave oscillator 4, an attenuator 5, a bidirectional coupler 6, a horn antenna 7 and a microwave detector 11. The horn antenna is used for transmitting the microwave and receiving the reflected signal, which is mixed with the reference signal in the bidirectional coupler. In the reference channel the electromechanical phase modulator is used to provide automatic calibration of the instrument. To adjust the antenna beam to the object under test, the microwave unit is placed on the platform which can be shifted in vertical and horizontal planes. 

A sehematie diagram of a SIFT apparatus is shown in figure Bl.7.12. The instrument eonsists of five basie regions, the ion soiiree, initial quadnipole mass filter, flow tube, seeond mass filter and finally the deteetor. The heart of the instrument is the flow tube, whieh is a steel tube approximately 1 m long and 10 em in diameter. The pressure in the flow tube is kept of the order of 0.5 Torr, resulting in earrier gas flow rates of... 

Another instrument used in physical chemistry research that employs quadnipole mass filters is the guided ion beam mass spectrometer [31]. A schematic diagram of an example of this type of instrument is shown in figure B 1.7.13. A... 

A schematic diagram of a simple TOP instrument is shown in figure B 1.7.17(a). Since the ion source region of any instrument has a finite size, the ions will spend a certain amount of time in the source while they are accelerating. If the... 

Time-of-flight mass spectrometers have been used as detectors in a wider variety of experiments tlian any other mass spectrometer. This is especially true of spectroscopic applications, many of which are discussed in this encyclopedia. Unlike the other instruments described in this chapter, the TOP mass spectrometer is usually used for one purpose, to acquire the mass spectrum of a compound. They caimot generally be used for the kinds of ion-molecule chemistry discussed in this chapter, or structural characterization experiments such as collision-induced dissociation. Plowever, they are easily used as detectors for spectroscopic applications such as multi-photoionization (for the spectroscopy of molecular excited states) [38], zero kinetic energy electron spectroscopy [39] (ZEKE, for the precise measurement of ionization energies) and comcidence measurements (such as photoelectron-photoion coincidence spectroscopy [40] for the measurement of ion fragmentation breakdown diagrams). 

Rotating cone viscometers are among the most commonly used rheometry devices. These instruments essentially consist of a steel cone which rotates in a chamber filled with the fluid generating a Couette flow regime. Based on the same fundamental concept various types of single and double cone devices are developed. The schematic diagram of a double cone viscometer is shown in... 

Fig. XI, 2, 5 is a drawing of the Hilger "Abbe refractometer, whilst Fig. XI, 2, 6 is a fine diagram showing the essential parts of the instrument.

Block diagram for a filter photometer with photo showing a typical hand-held instrument suitable for field work. Colorimeterrw is manufactured by Hach Company/photo courtesy of Hach Company. 

Block diagram for a single-beam fixed-wavelength spectrophotometer with photo of a typical instrument. 

Molecular Fluorescence A typical instrumental block diagram for molecular fluorescence is shown in Figure 10.45. In contrast to instruments for absorption spectroscopy, the optical paths for the source and detector are usually positioned at an angle of 90°. 

Schematic diagram of an orthogonal Q/TOF instrument. In this example, an ion beam is produced by electrospray ionization. The solution can be an effluent from a liquid chromatography column or simply a solution of an analyte. The sampling cone and the skimmer help to separate analyte ions from solvent, The RF hexapoles cannot separate ions according to m/z values and are instead used to help confine the ions into a narrow beam. The quadrupole can be made to operate in two modes. In one (wide band-pass mode), all of the ion beam passes through. In the other (narrow band-pass mode), only ions selected according to m/z value are allowed through. In narrow band-pass mode, the gas pressure in the middle hexapole is increased so that ions selected in the quadrupole are caused to fragment following collisions with gas molecules. In both modes, the TOF analyzer is used to produce the final mass spectrum.

The process and instrumentation (P I) diagram provides a graphical representation of the control configuration for the process. The P I diagrams illustrate the measurement devices that provide inputs to the control strategy, the actuators that will implement the results of the control calculations, and the function blocks that provide the control logic. 

P IDs (piping and instrumentation diagrams) should identify instruments, sample locations, the presence of sample valves, nozzle blinding, and control points. Of particular importance are the bypasses and alternate feed locations. The isolation valves in these hues may leak and can distort the interpretation of the measurements. 

Piping and Instrument Diagram (P ID) A diagram that shows the details about the piping, vessels, and instrumentation. 

The elevated pressure in Proeess 2, shown sehematieally in Figure 4-6, again ineludes a tail gas expander as part of the eombustion air eompressor train (Figure 4-7). A typieal eontrol and instrument diagram for Proeess 2 is given in Figure 4-8. The nomenelature deseribed in Proeess 1 also pertains here. 

Finally, the dual-pressure eyele of Proeess 3 ean be seen sehematieally in Figure 4-9, and in its physieal eonfiguration in Figure 4-10. Note that the lineup starts with the axial flow air eompressor to the left, the radial flow nitrous gas eompressor is in the middle, and the expander in the right foreground. Figure 4-11 shows the typieal eontrol and instrument diagram for Proeess 3. 

Figure 4-5. Typical control and instrument diagram for Process 1.

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