Vacuum differential

All filtering and extraction systems must be checked for compatibility with the analyte of interest. Some or all of the analytes may be absorbed or otherwise lost during the extraction process, and this must be known beforehand. Carbon may be lost by high vacuum differentials between sampler and soil water. Long extraction times may lead to distortions in the results of the sample analysis [5],... 

The method relies on the ability to provide a vacuum differential across the objective aperture in the electron optical column. This is in principle possible in all SEMs, but in practice easier to achieve in some microscopes than others. Image formation requires a BSE detector rather than the more commonly used SE detector. While any backscattered electron detector can be used, the high resolution potential of the SEM can only be maintained by employing a high efficiency detector, such as the Robinson detector used here. 

Differential pumping of the two hexapole sections keeps the second at a pressure of about ICk mbar. The two consecutive hexapole sections are sometimes described as bridges between the pressure in the inlet and the following vacuum in the TOP mass analyzer. 

Moving-belt (ribbon or wire) interface. An interface that continuously applies all, or a part of, the effluent from a liquid chromatograph to a belt (ribbon or wire) that passes through two or more orifices, with differential pumping into the mass spectrometer s vacuum system. Heat is applied to remove the solvent and to evaporate the solute into the ion source. 

Most continuous pressure filters available (ca 1993) have their roots in vacuum filtration technology. A rotary dmm or rotary disk vacuum filter can be adapted to pressure by enclosing it in a pressure cover however, the disadvantages of this measure are evident. The enclosure is a pressure vessel which is heavy and expensive, the progress of filtration cannot be watched, and the removal of the cake from the vessel is difficult. Other complications of this method are caused by the necessity of arranging for two or more differential pressures between the inside and outside of the filter, which requires a troublesome system of pressure regulating valves. 

Two main operational variables that differentiate the flotation of finely dispersed coUoids and precipitates in water treatment from the flotation of minerals is the need for quiescent pulp conditions (low turbulence) and the need for very fine bubble sizes in the former. This is accompHshed by the use of electroflotation and dissolved air flotation instead of mechanically generated bubbles which is common in mineral flotation practice. Electroflotation is a technique where fine gas bubbles (hydrogen and oxygen) are generated in the pulp by the appHcation of electricity to electrodes. These very fine bubbles are more suited to the flotation of very fine particles encountered in water treatment. Its industrial usage is not widespread. Dissolved air flotation is similar to vacuum flotation. Air-saturated slurries are subjected to vacuum for the generation of bubbles. The process finds limited appHcation in water treatment and in paper pulp effluent purification. The need to mn it batchwise renders it less versatile. 

In general, once the curtain of filaments has been produced, it is necessary to attenuate the filaments in order to provide strength and resistance to deformation. The most commonly practiced approach is to utilize a single slot, which is at least the width of the curtain, at a point below the spinning plate and above the laydown screen. There are two practical approaches taken. The first utilizes the injection of low pressure air at a point above the slot so that the fibers attain sufficient acceleration in the slot to provide adequate draw (22) (Fig. 7). The second utilizes a low pressure vacuum below a venturi to provide the pressure differential requited for sufficient acceleration and resulting attenuation (30). 

Pipeline transport involves the appHcation of force to the material being moved, either through the use of pumps to transport Hquids, compressors to move gases, or flowing water to move soHds. In some appHcations, vacuum may create the pressure differential. 

Moisture. Moisture is usually determined by a vacuum oven-dry method at 80°C. Moisture levels of more than 0.05% are likely to lead to caking or lumping problems which can make storage and transfer of bulk sugar difficult. The usual standard is 0.03%, which manufacturers can easily meet. Care must be taken to avoid temperature differentials ia storage which cause moisture to migra te and estabUsh pockets of unacceptably high moisture levels. 

The fluid dehvery in an air-spray system can be pressure or suction fed. In a pressure-fed system, the fluid is brought to the atomizer under positive pressure generated with an external pump, a gas pressure over the coating material in a tank, or an elevation head. In a suction system, the annular flow of air around the fluid tip generates sufficient vacuum to aspirate the coating material from a container through a fluid tube and into the air stream. In this case, the paint supply is normally located in a small cup attached to the spray device to keep the elevation differential and frictional pressure drop in the fluid-supply tube small. 

Strain-gauge pressure transducers are manufactured in many forms for measuring gauge, absolute, and differential pressures and vacuum. Full-scale ranges from 25.4 mm of water to 10,134 MPa are available. Strain gauges bonded direc tly to a diaphragm pressure-sensitive element usually have an extremely fast response time and are suitable for high-frequency dynamic-pressure measurements. 

Heat is transferred by radiation, condurtion, and convection. Radiation is the primaiy mode and can occur even in a vacuum. The amount of heat transferred for a given area is relative to the temperature differential and emissivity from the radiating to the absorbing surface. Conduction is due to molecular motion and occurs within... 

The te.st is carried out by using an apparatus shown in Figure 11.8, consisting of a closed test chamber in which talcum powder can pass through a sieve having square openings of 75 fim, and is held in suspension by an air current. The amount of talcum powder is supplied at 2 kg per cubic metre size of the test chamber. The enclosure under lest is placed inside the chamber and is connected to a vacuum pump which maintains, inside the enclosure, a differential pressure equivalent to not more than a 200 mm eolumn of water. 

If the system differential pressure requirements are low, sometimes a fan can be used. A fan is limited to a maximum of about 65 inches of water (just over 2psi) in vacuum service or 77 inches of water in pressure service (just under 3psi). To estimate fan horsepower use the equations found in Chapter 6 in the section entitled Horsepower Calculation. In lieu of manufacturer s data use an adiabatic efficiency of 50% for initial work. 

Vacuums of about 8psi (some can go to 11 psi with water injection) and pressure differentials of 15 psi. 

As time goes on, the ultimate resolution of the SEM operated in these modes will probably level out near 1 nm. The major growth of SEMs now seems to be in the development of specialized instruments. An environmental SEM has been developed that uses differential pumping to permit the observation of specimens at higher pressures. Photographs of the formation of ice crystals have been taken and the instrument has particular application to samples that are not vacuum compatible, such as biological samples. 

Two vacuum systems are used to provide both the high vacuum needed for the mass spectrometer and the differential pumping required for the interface region. Rotary pumps are used for the interface region. The high vacuum is obtained using diffusion pumps, cryogenic pumps, or turbo pumps. 

When the space above the suspension is subjected to compressed gas or the space under the filter plate is under a vacuum, filtration proceeds under a constant pressure differential (the pressure in the receivers is constant). The rate of filtration decreases due to an increase in the cake thickness and, consequently, flow resistance. A similar filtration process results from a pressure difference due to the hydrostatic pressure of a suspension layer of constant thickness located over the filter medium. 

After condensation, the clusters are transported by the He-flow through a nozzle and a differential pumping stage into a high vacuum chamber. For ionization of the clusters, we used excimer and dye laser pulses at various wavelengths. The ions were then mass analyzed by a time-of-flight mass spectrometer, having... 

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