Static purge

See alsa Distillation. Enzymes Overview Enzyme-Based Electrodes. Food and Nutritional Analysis Antioxidants and Preservatives Alcoholic Beverages. Forensic Sciences Alcohol in Body Fluids Blood Analysis. Headspace Analysis Static Purge and Trap. Infrared Spectroscopy Overview. Optical Spectroscopy Refractometry and Reflectometry. Quality Assurance Quality Control. Sensors Amperometric Oxygen Sensors. [Pg.1168]

See also Air Analysis Sampling Workplace Air. Gas Chromatography Multidimensional Techniques High-Temperature Techniques High-Speed Techniques Online Coupled LC-GC Pyrolysis Detectors. Head-space Analysis Static Purge and Trap. [Pg.1874]

See also Air Analysis Sampling Outdoor Air Workplace Air. Dioxins. Headspace Anaiysis Static Purge and Trap. Isotope Dilution Anaiysis. Liquid Chromatography Overview. Mass Spectrometry Overview. Pesticides. Surfactants and Detergents. Water Anaiysis Overview Industrial Effluents. [Pg.2925]

Static Purge and Trap. Membrane Techniques Dialysis and Reverse Osmosis Ultrafiltration Liquid Membranes. Potentiometric Stripping Analysis. Titrimetry Potent-iometric. [Pg.3002]

See also Activation Analysis Neutron Activation. Atomic Absorption Spectrometry Principles and Instrumentation. Atomic Emission Spectrometry Principles and Instrumentation. Chromatography Overview Principles. Gas Chromatography Pyrolysis Mass Spectrometry. Headspace Analysis Static Purge and Trap. Infrared Spectroscopy Near-Infrared Industrial Applications. Liquid Chromatography Normal Phase Reversed Phase Size-Exclusion. Microscopy Techniques Scanning Electron Microscopy. Polymers Natural Rubber Synthetic. Process Analysis Chromatography. Sample Dissolution for Elemental Analysis Dry... [Pg.3732]

See also Extraction Solvent Extraction Principles Solid-Phase Extraction. Fluorescence Environmental Applications. Gas Chromatography Mass Spectrometry Environmental Applications. Gravimetry. Headspace Analysis Static Purge and Trap. Immunoassays Overview. Infrared Spectroscopy Overview. Liquid Chromatography Overview. Sampling Theory. [Pg.5092]

Purging Carrier and Makeup Gases Carrier-gas and makeup-gas systems require a static purge, followed by a dynamic purge, to ensure the desired purity levels. [Pg.528]

DYNAMIC PURGE After the last static purge, close the shutoff valves at the vent ends of the lines and bring the mainline pressure to 20 psig (1.4 bar). Choose a shutoff valve as far downstream from the cylinder as possible. Open this valve and adjust the valve to allow a 60 mL/min flow of gas. Purge for 24 hs. For this step an extra flow controller, installed after the opened shutoff valve, will make it easy to regulate the flow and will help minimize backdiffusion into the line. [Pg.528]

The labyrinth portion of the seal was designed to withstand the static and dynamic differential pressure (in the event of a major seal failure) while passing the minimum volume of purge gas. [Pg.340]

FIGURE 14.18 Flow diagram of split flow capillary LC system. 1. Solvent reservoirs. 2. Model 5000 syringe pump (Varian, Walnut Creek, California). 3. Static mixer. 4. Injection port. 5. Column. 6. Detector. 7. Pressure transducer. 8. Pulse dampener. 9. Purge valve. 10. U-flow controlling device. 11. Waste. [Pg.374]

VOCs GC/MS Purge-and-trap static headspace azeotropic distillation ... [Pg.192]

The key advantage of this headspace method, compared to static headspace analysis, is the sensitivity obtained. While static headspace shows the status at equilibrium and can measure thermodynamic constants, purge-and-trap or dynamic headspace can measure the kinetics of... [Pg.1008]

In flavor analysis, the most frequent use of volatile traps is in analyzing the flavor compounds in foods using purge-and-trap or dynamic headspace, followed by GC-MS or GCO. Additionally, the traps can be used to measure static headspace and air-matrix partition coefficients where air is pushed out of an equilibrated cell containing the sample onto a volatile trap (Chaintreau et al., 1995). Volatile traps have been also used for flavor release measurements during eating (Linforth and Taylor, 1993) or simulated eating (Roberts and Acree, 1995). [Pg.1009]

For a compound to contribute to the aroma of a food, the compound must have odor activity and volatilize from the food into the head-space at a concentration above its detection threshold. Since aroma compounds are usually present in a headspace at levels too low to be detected by GC, headspace extraction also requires concentration. SPME headspace extraction lends itself to aroma analysis, since it selectively extracts and concentrates compounds in the headspace. Some other methods used for sample preparation for aroma analysis include purge-and-trap or porous polymer extraction, static headspace extraction, and solvent extraction. A comparison of these methods is summarized in Table Gl.6.2. [Pg.1076]