Purge valve

The bleeding of gas from the purge valve will release a mixture which can he estimated from the total pressure. 

FIGURE 14.18 Flow diagram of split flow capillary LC system. 1. Solvent reservoirs. 2. Model 5000 syringe pump (Varian, Walnut Creek, California). 3. Static mixer. 4. Injection port. 5. Column. 6. Detector. 7. Pressure transducer. 8. Pulse dampener. 9. Purge valve. 10. U-flow controlling device. 11. Waste. 

Proportional valve 2 open Purge valve open... 

Fig. 14.5. Schematic of splitless inlet with purge valve closed showing the major components. Note the position of the purge valve in comparison to Fig. 14.4. Reprinted with permission from the 6890 Gas Chromatograph Operating Manual. Copyright (2004), Agilent Technologies.

Fig 2. Apparatus for the desorption of volatiles Iron Tenax. A Splitter valve B Septum purge valve C Toggle valve... 

Set the upper pressure limit (typically at 3500 to 4000 psi). Perform dry prime by opening the prime/purge valve and draw out 10mL from each solvent line if the system has been idle for a long time or the pump has run dry. 

A 500-L solution containing 2 mg/L of free chlorine residual in distilled water was pumped onto the four-column system the columns were eluted and the eluants were processed as described earlier. This chlorine blank and resin eluant blanks were analyzed by GC-MS by using a Finnigan 4023 with the I NCOS data system and a 31,000-compound National Bureau of Standards library. Electron impact spectra were obtained by using an electron energy of 70 eV and a scan time of 1 s for the mass range 33-550 amu. A 30-m WCOT SE-54 fused-silica capillary column (J W Scientific) was used for separations. Injections were made with the oven at 40 °C and the door open, the injector at 220 °C, and the interface at 270 °C. Two minutes after injection, the door was closed and the temperature was raised ballistically to 60 °C, ramped at 4 °C/min to 280 °C, and held there for 4 min. The split and septum purge valves were closed for injection and opened after 1 min. 

Figure 18.1 Diagram of the glass vacuum line showing the major components mechanical pumps, diffusion pump, vacuum gauge, main vacuum manifold, and purge valve.

H Pressure Sensor I Bores for Heating Wire J Air Cylinder K Air Cylinder Piston L Back Pressure Regulator M Compressed Air Cylinder P Pressure Gauge R Regulator Unit VB Bleed Valve VN Needle Valve VP Purging Valve... 

Treatment 1 Open a purge valve. Prime the pump with degassed solvent. 

As an additional feature, an auxiliary filter can be fitted with a drain valve to regularly clean the filter and prevent clogging. This drain can also, on demand, be piped to the main valve outlet or it can be piped on site to a purge collector. The purge valve can be programmed to open at pre-set intervals. The mini-valve for the drain, shown in Figure 5.43, can also be an automated ball valve I would recommend not lower than a 55 j, filter element with a minimum area of 80 cm2 and an approximate volume of 50 to 75 cc. 

Close customer purge valve and replace dust cap. 

Open customer purge valve purge for 3 minutes. 

Step 2. This process has 12 degrees of freedom. One of these is agitation rate, which we simply hold constant. This leaves 11 degrees of freedom four fresh feeds F,A. F0d. FoE. and FcC, purge valve gas recycle valve separator base valve stripper base valve steam valve reactor cooling water valve and condenser cooling water valve. 

The control system is shown in Fig. 8.9. The override controller on low F,a flow7 was used to open the purge valve. The override controller on low yA composition was used to pinch the fresh feed flowrate FrjD. 

Step 2. There are 23 control degrees of freedom. They include two fresh feed valves for hydrogen and toluene purge valve separator base and overhead valves cooler cooling water valve liquid quench valve furnace fuel valve stabilizer column steam., bottoms, reflux, cooling water, and vapor product valves product column steam, bottoms, reflux, distillate, and cooling water valves and recycle column steam, bottoms, reflux, distillate, and cooling water valves. 

Step 2. There are 26 control degrees of freedom in this process. They include three feed valves for oxygen, ethylene, and acetic acid vaporizer and heater steam valves reactor steam drum liquid makeup and exit vapor valves vaporizer overhead valve two coolers and absorber cooling water valves separator base and overhead valves absorber overhead, base, wash acid, and liquid recirculation valves gas valve to CO removal system gas purge valve distillation column steam and cooling water valves column base, reflux, and vent valves and decanter organic and aqueous product valves. 

The high-pressure inlet is attached to a f in. cross to provide ports for gas introduction, pressure measurement, and thermocouple placement just in front of the frit. The Bourdon gauge (0-10 bar) should be connected via a tee to a purge valve to facilitate gas changes. Before use the assembly should be tested at 10 bar for leaks. Thermal insulation such as glass wool should be wrapped around the frit assembly to keep the expansion as adiabatic as possible. 

Purge valve Tighten valve replace purge valve. 

Purge the hose and regulator of air. Open the cylinder wheel slowly up to full cylinder pressure and then open regulator valve to around 20 psi. Grab the quick-connect DESO stem that is attached to the hose and push down on the center of the stem inside the connection with a stick or small steel rod, to allow the gas to escape. Do this for a few seconds at a time for about ten times. This should be done outdoors so the gas can dissipate and not collect in a confined space. The best way to do this is to add another hose on to the regulator with a on/off valve and use this as a purging valve. 

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