Tubes silica

The furnace and thermostatic mortar. For heating the tube packing, a small electric furnace N has been found to be more satisfactory than a row of gas burners. The type used consists of a silica tube (I s cm. in diameter and 25 cm. long) wound with nichrome wire and contained in an asbestos cylinder, the annular space being lagged the ends of the asbestos cylinder being closed by asbestos semi-circles built round the porcelain furnace tube. The furnace is controlled by a Simmerstat that has been calibrated at 680 against a bimetal pyrometer, and the furnace temperature is checked by this method from time to time. The furnace is equipped with a small steel bar attached to the asbestos and is thus mounted on an ordinary laboratory stand the Simmerstat may then be placed immediately underneath it on the baseplate of this stand, or alternatively the furnace may be built on to the top of the Simmerstat box. 

A dynamic-FAB probe having a simple copper target. The narrow fused-silica tube passes through the shaft, its end lying flush with the target surface. 

Hot wire anemometer An instrument for the measurement of fluid velocity by measuring the resistance of a fine platinum or nichrome wire, which may or may not be shielded by a silica tube. The wire resistance is proportional to the temperature and the fluid flow rate. 

Heating diethyl (2-pyridylamino)methylenemalonates 304 (R = COOEt, = Me, OH) in AcOH afforded 4-oxo-4//-pyrido[l, 2-n]pyrimidine-3-carboxylates 305 (R = Me, OH) (96JHC1041). Flash vacuum thermolysis of 2-substituted 3-(2-pyridylamino)acrylates 304 (R = CN, COOEt, R = H) through a packed silica tube (530 °C, 0.01 mmHg) gave 3-substituted 4//-pyrido[l,2-n]pyrimidm-4-ones 306 (R = CN, COOEt) (94AJC1263). Ethyl 7-methyl-4-oxo-l, 4-dihydro-1,8-naphthyridine-3-carboxylate (79%) was... 

Capillary columns are fabricated from thin-walled stainless steel, glass, or high-purity fused silica tubing (the last is preferred for its inertness). Typical dimensions of the columns, which are coiled, are 25-200 m long and 0.2-0.5 mm i.d. 

In general, a Raman adsorption cell consists of a length of pyrex or silica tubing, one end of which is sealed with an optical flat, and the other either connected to a gas line for admitting the adsorbate or to a vacuum line for evacuating the cell. Activation of the samples may then be carried out in situ 27). 

Premier and Schupp have made vapour-density measurements with sulphur enclosed in a quartz bulb heated electrically and connected with a manometer consisting of a spiral of silica tubing attached to a small mirror. The pressure was measured by the amount of unwinding of the spiral. The same method has been used by Bodenstein and Katavama in studving the equilibrium ... 

Figure 5.6 shows typical two-phase flow patterns observed in an air-water flow in a 25 pm silica tube at nearly atmospheric pressure. 

There has been relatively little work done on the development of two-phase flow regime maps for micro-channels. The general trends of how the transition lines are shifted as the diameter is decreased are unclear. Figure 5.19 shows a flow pattern map obtained for air-water two-phase flow in a 20 pm i.d. silica tube by Serizawa et al. (2002) at nearly atmospheric pressure. 

Fig. 5.26 Cross-sectional average void fraction in air-water two-phase flow in a 20 pm i.d. silica tube. Reprinted from Serizawa et al. (2002) with permission...

Mg-Hg alloys and compounds have been produced by mixing the two metals in either Ar-filled Fe crucibles " or evacuated silica tubes . 

Inside" processes—such as modified chemical vapor deposition (MCVD) and plasma chemical vapor deposition (PCVD)—deposit doped silica on the interior surface of a fused silica tube. In MCVD, the oxidation of the halide reactants is initiated by a flame that heats the outside of the tube (Figure 4.8). In PCVD, the reaction is initiated by a microwave plasma. More than a hundred different layers with different refractive indexes (a function of glass composition) may be deposited by either process before the tube is collapsed to form a glass rod. 

The synthesis of quaternary thiospinels, like Ag2FeSn3Sg [5], Ag2MnSn3Sg [6], and Cu2NiSn3Sg [7], has been achieved by reacting metals along with sulfur powder in an evacuated silica tube. Pure phases of these compounds were obtained at 750 °C, 670 °C and 750 °C respectively. 

Inspect the culture tubes in the manifold to determine if there is water in the organic eluent for any sample. If a water layer is present, quantitatively transfer the organic phase into a clean culture tube using a small amount of additional solvent as necessary. Return the culture tube containing the organic extract to its proper location in the manifold rack. Remove the Cig and sodium sulfate mbes, and reinstall the silica tubes on the manifold. With the sample remaining in the culture tube, continue to apply vacuum to the manifold to remove excess solvent. When the solvent volume is < 1 mL, discontinue vacuum, and allow the sample to return to room temperature. Adjust the sample volume in the culture mbe to 1 mL with isooctane-ethyl acetate (9 1, v/v). Transfer the entire sample into an autosampler vial for GC/MS analysis. Sample extracts may be stored for up to 1 month in a refrigerator (< 10 °C) before analysis. 

Lauer, H. H. and McManigill, D., Capillary zone electrophoresis of proteins in untreated fused silica tubing, Anal.Chem., 58, 166, 1986. 

The traditional sample volumes in CGC (0.1-3 xL) limit sample preparation possibilities. Specialised large-volume injection (LVI) techniques are designed to load more sample in the GC system (typically 150 xL) by placing a length of uncoated fused-silica tubing in front of the analytical column. This procedure also provides... 

Dynamic headspace GC-MS involves heating a small amount of the solid polymer sample contained in a fused silica tube in a stream of inert gas. The volatile components evolved on heating the sample are swept away from the sample bulk and condensed, or focused on a cryogenic trap before being introduced onto the chromatographic column via rapid heating of the trap. The technique can be used qualitatively or quantitatively DHS-GC-MS is considered to be well suited towards routine quantitative analysis. 

During preparation of aluminium copper(I) disulfide from the elements in an air-free silica tube at 900-1000° C, initial heating must be slow to prevent explosion of the tube by internal pressure of unreacted sulfur vapour. 

Gautier, C., Lopez, P.J., Hemadi, M., Livage and J., Coradin, T. (2006) Biomimetic growth of silica tubes in confined media. Langmuir, 22, 9092-9095. 

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