Packing Packed Tower

Tower diameter selection is usually made with the maximum expected gas and liquid flow rates and depends on the size and type of tower packing The portion of Fig. 3 with solid lines illustrates the pressure-drop relationship for 1.5-m. [3.81 -cm] Pull rings supplied by the manufacturer for typical superficial gas and liquid flow rates used in the chemical processing industry.1 This relationship is usually available in graphical form from any manufacturer of packed-tower packing elements. While these... 

Structured packing— Tower packing that is installed in a column in a precise array. 

The gas to be purified passes up the tower and is met by a stream of liquid introduced by a series of sprays. The space inside the lower is empty without packing. 

Industrially an aqueous solution of chlorine dioxide can be prepared by passing nitrogen dioxide up a packed tower down which sodium chlorate(V) flows ... 

Ammonia. Small quantities of ammonia may be prepared with the aid of the apparatus depicted in Fig. II, 48,4. Concentrated ammonia solution (sp. gr. 0-88) is gently heated in the flask surmounted by an efficient reflux condenser. The gas is dried by passage through the tower which is loosely packed with soda lime or quicklime, and is then passed... 

Design Procedure. The packed height of the tower required to reduce the concentration of the solute in the gas stream from to acceptable residual level ofjy 2 may be calculated by combining point values of the mass transfer rate and a differential material balance for the absorbed component. Referring to a sHce dh of the absorber (Fig. 5),... 

Sometimes the height equivalent to a theoretical plate (HETP) is employed rather than and to characterize the performance of packed towers. The number of heights equivalent to one theoretical plate required for a specified absorption job is equal to the number of theoretical plates,... 

Nonisothermal Gas Absorption. The computation of nonisothermal gas absorption processes is difficult because of all the interactions involved as described for packed columns. A computer is normally required for the enormous number of plate calculations necessary to estabUsh the correct concentration and temperature profiles through the tower. Suitable algorithms have been developed (46,105) and nonisothermal gas absorption in plate columns has been studied experimentally and the measured profiles compared to the calculated results (47,106). Figure 27 shows a typical Hquid temperature profile observed in an adiabatic bubble plate absorber (107). The close agreement between the calculated and observed profiles was obtained without adjusting parameters. The plate efficiencies required for the calculations were measured independendy on a single exact copy of the bubble cap plates installed in the five-tray absorber. 

The reactors were thick-waked stainless steel towers packed with a catalyst containing copper and bismuth oxides on a skiceous carrier. This was activated by formaldehyde and acetylene to give the copper acetyUde complex that functioned as the tme catalyst. Acetylene and an aqueous solution of formaldehyde were passed together through one or more reactors at about 90—100°C and an acetylene partial pressure of about 500—600 kPa (5—6 atm) with recycling as required. Yields of butynediol were over 90%, in addition to 4—5% propargyl alcohol. 

Includes cyclonic, dynamic, filtration, inertial impaction (wetted targets, packed towers, turbulent targets), spray chambers, and venturi. 

When two phases are present the situation is quite complex, especially in beds of fine soHds where interfacial forces can be significant. In coarse beds, eg, packed towers, the effects are often correlated empirically in terms of pressure drops for the single phases taken individually. 

Decomposition by Caustic Scrubbing. The waste gas stream is led through packed towers where a sodium hydroxide solution is introduced at the top of the towers. Venturi scmbbers can also be used. Makeup sodium hydroxide is added under pH control (32). 

Decomposition with Moist Activated Carbon. The waste gas stream is passed through packed activated carbon towers where water is fed at the top of the towers. The water is normally recycled. If the hydrochloric acid concentration in the recycled water exceeds 10%, the decomposition efficiency is greatly reduced. Thus, a sufficient supply of fresh water must be assured and a hydrochloric acid stream continuously taken out (33). 

Environmental Protection. Fumes resulting from exposure of anhydrous aluminum chloride to moisture are corrosive and acidic. Collection systems should be provided to conduct aluminum chloride dusts or gases to a scmbbing device. The choice of equipment, usually one of economics, ranges from simple packed-tower scmbbers to sophisticated high energy devices such as those of a Venturi design (11). 

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