Normal requirement

Cross flow inside the casing can also be prevented by isolating one zone. However, this may still result in reduced production. Installing a selective completion can solve the problem but is an expensive option. To repair cross flow behind casing normally requires a full workover with a rig. Cement has to be either squeezed or circulated behind the production casing and allowed to set, after which cement inside the casing is drilled out, and the producing zones perforated and recompleted. 

A molecular orbital is a linear combination of basis functions. Normalization requires that the integral of a molecular orbital squared is equal to 1. The square of a molecular orbital gives many terms, some of which are the square of a basis function and others are products of basis functions, which yield the overlap when integrated. Thus, the orbital integral is actually a sum of integrals over one or two center basis functions. 

A typical example is total monomers. 100 sodium stearate, 5 potassium persulfate, 0.3 lauryl mercaptan, 0.4 to 0.7 and water, 200 parts. In this formula, 75 parts of 1,3-butadiene and 25 parts of 4-methyl-2-vinylthiazole give 86% conversion to a tacky rubber-like copolymer in 15 hr at 45°C. The polymer contains 62% benzene-insoluble gel. Sulfur analysis indicates that the polymer contains 21 parts of combined 4-methyl-2-vinylthiazole (312). Butadiene alone in the above reaction normally requires 25 hr to achieve the same conversion, thus illustrating the acceleration due to the presence of 4-methyl-2-vinylthiazole. 

Lactones whose rings are three or four membered (a lactones and p lactones) are very reactive making their isolation difficult Special methods are normally required for the laboratory synthesis of small ring lactones as well as those that contain rings larger than SIX membered... 

Converting the C 2 alkylated derivative to the corresponding malonic acid deriva tive by ester hydrolysis gives a compound susceptible to thermal decarboxylation Tern peratures of approximately 180°C are normally required... 

Nonisothermal Gas Absorption. The computation of nonisothermal gas absorption processes is difficult because of all the interactions involved as described for packed columns. A computer is normally required for the enormous number of plate calculations necessary to estabUsh the correct concentration and temperature profiles through the tower. Suitable algorithms have been developed (46,105) and nonisothermal gas absorption in plate columns has been studied experimentally and the measured profiles compared to the calculated results (47,106). Figure 27 shows a typical Hquid temperature profile observed in an adiabatic bubble plate absorber (107). The close agreement between the calculated and observed profiles was obtained without adjusting parameters. The plate efficiencies required for the calculations were measured independendy on a single exact copy of the bubble cap plates installed in the five-tray absorber. 

In normal practice, inhibitors such as hydroquinone (HQ) [123-31 -9] or the monomethyl ether of hydroquinone (MEHQ) [150-76-5] are added to acrylic monomers to stabilize them during shipment and storage. Uninhibited acrylic monomers should be used prompdy or stored at 10°C or below for no longer than a few weeks. Improperly iahibited monomers have the potential for violent polymerizations. HQ and MEHQ require the presence of oxygen to be effective inhibitors therefore, these monomers should be stored in contact with air and not under inert atmosphere. Because of the low concentration of inhibitors present in most commercial grades of acrylic monomers (generally less than 100 ppm), removal before use is not normally required. However, procedures for removal of inhibitors are available (67). 

The sohd can be contacted with the solvent in a number of different ways but traditionally that part of the solvent retained by the sohd is referred to as the underflow or holdup, whereas the sohd-free solute-laden solvent separated from the sohd after extraction is called the overflow. The holdup of bound hquor plays a vital role in the estimation of separation performance. In practice both static and dynamic holdup are measured in a process study, other parameters of importance being the relationship of holdup to drainage time and percolation rate. The results of such studies permit conclusions to be drawn about the feasibihty of extraction by percolation, the holdup of different bed heights of material prepared for extraction, and the relationship between solute content of the hquor and holdup. If the percolation rate is very low (in the case of oilseeds a minimum percolation rate of 3 x 10 m/s is normally required), extraction by immersion may be more effective. Percolation rate measurements and the methods of utilizing the data have been reported (8,9) these indicate that the effect of solute concentration on holdup plays an important part in determining the solute concentration in the hquor leaving the extractor. 

Feed Ga.s Purifica.tion. Because nickel-based reforming catalysts are quite sensitive to sulfur, halogen, and heavy metal poisons which may be found ia natural gas, a feedstock purification system is normally required. Sulfur compounds, ia both organic and inorganic forms, are the most common... 

Sulfur is the almost universal, primary vulcanizing agent for all elastomers, whether in latex or dry form. Less sulfur is normally required for latex than for dry mbber compounds. By increasing sulfur concentration to 30—50 parts by weight (30—50 parts/100 parts dry mbber content (DRC)) in latex compound, satisfactory hard mbber articles, particularly mbber—metal coatings, are obtained. 

For an analyte of molecular weight 5000 and good chromatographic conditions, most photometric detectors can be expected to provide detection limits of 2—5 ng. Improvement into the mid-picogram or lower range normally requires the use of more sensitive detection means such as fluorescence or electrochemical detectors. 

Dactinomycin is useful against several tumors especially Wilms tumor of the kidney and rhabdomyosarcoma. Wilms tumor normally requires a combination of surgery, x-ray irradiation, and dactinomycin plus vincristine [57-22-7] or other antitumor agents. Resistance of the multidmg... 

Table 1 Hsts several of the chemical deterrninations and the corresponding reactions uti1i2ed, which are available on automated clinical analy2ers. With the exception of assays for various electrolytes, eg, Na", K", Cl , and CO2, deterrnination is normally done by photometric means at wavelengths in the ultraviolet and visible regions. Other means of assay include fluorescence, radioisotopic assay, electrochemistry, etc. However, such detection methods are normally required only for the more difficult assays, particularly those of semm or urine constituents at concentrations below )Tg/L. These latter assays are discussed more fully in the Hterature (3,4).

This requirement of a physical property system is generally accommodated by enabling the user to create the equivalent of the permanent system data bank by expHcitly entering data in the same format. Such private data banks can be used independently or in conjunction with the system data bank. Data supphed in this way normally require that the user has access to expertise in physical property data and possibly in computer use as well. In these circumstances the user may also wish to provide data in tabular or polynomial form for use by an appropriate set of interpolative point generation routines. This facihty is shown at the top right of Figure 5. 

Other Considerations. Some carrier-active products, especially o-phenylphenol and methylnaphthalenes, have an adverse effect on the lightfastness of the finished dyeing. The reason for this is not clear, but the effect is readily estabhshed. This problem is overcome by submitting the dyed material to temperatures higher than those normally required in drying. Under the conditions (150—175°C) that are usually required to heat-set dyed fabrics or to cure resins apphed in finishing operations, the residual carrier is volatilized. 

To allow flexibility, the database manager must also perform point addition or deletion. However, the abihty to create a point type or to add or delete attributes of a point type is not normally required because, unlike other data processing systems, a process control system normally involves a fixed number of point types and related attributes. For example, analog and binary input and output types are required for process I/O points. Related attributes for these point types include tag names, values, and hardware addresses. Different system manufacturers may define different point types using different data structures. We will discuss other commonly used point types and attributes as they appear. 

Hazards that pose a risk to the public. Complete redundancy is normally required. 

Hazards that could re.sult in major equipment damage and consequently lengthy plant downtime. No redundancy is normally required for these, although redundancy is always an option. Situations that result in minor equipment damage that can be quickly repaired do not generally require a safety interlock however, a process interlock might be appropriate. 

Figure 10-104 illustrates the level of vacuum normally required to perform many of the common mauiifactiiriug processes. The attainment of various levels is related to available equipment in Fig. 10-105. 

FIG, 10-104 Vacuum levels normally required to perform common manufacturing processes. (Couriesy of Compressed Air magazine.)... 

Examination Normally Required Fiping not covered by Category D fluid service or severe cyclic conditions shall be examined as follows or to any greater extent specified in the engineering design. 

The secondaiy ejector systems used for removing air require steam pressures of 2,5 bar or greater. When the available steam pressure is lower than this, an electrically driven vacuum pump is used for either the final secondaiy ejector or for the entire secondaiy group. The secondary ejectors normally require 0,2-0,3 kg/h of steam per kW of refrigeration capacity,... 

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