Synthesis and Analysis

SOURCE Center for Information and Numerical Data Analysis and Synthesis (CINDAS), Purdue University, West Lafayette, Ind. 

Dong, Z. 1989 Automatic Tolerance Analysis and Synthesis in CAD Environment. PhD Thesis State University of NY, Buffalo, NY. 

Wu, Z., Elmaraghy, W. H. and Elmaraghy, H. A. 1988 Evaluation of Cost-Tolerance Algorithms for Design Tolerance Analysis and Synthesis. Manufacturing Review, 1(3), October, 168-179. 

Venable, H. Dean, The K Factor A New Mathematical Tool for Stability Analysis and Synthesis, POWERCON March 1983. 

Analysis proceeds from the assumption that in order to understand a system one must first break it up into its constituent parts. Understanding then comes from the knowledge gained by reconstructing the system. But for systems whose dynamics depend critically on interaction between pai ts, analysis often misses the essential characteristics of the whole system. Synthesis is the complementary act of putting the individual pieces together in order to understand what they do collectively. Understanding complex synthesis requires that both analysis and synthesis be done. 

Guderian, R. Air Pollution by Photochemical Oxidants] Guderian, R. Ed. Ecological Studies Analysis and Synthesis Springer-Verlag New York, NY, 1985 Vol. 52 p 346. 

Richard D. Colberg and Manfred Moiari, Analysis and Synthesis of Resilient Heat Exchanger Networks... 

A number of conceptual frameworks were set up for comparative analysis and synthesis of country data. These included spheres of regulation, historical development and stmcture-process-outcome of regulation. 

Chemical analysis and synthesis on mitrochips promise a variety of potential benefits... 

Since the student will build neither, and since the professor probably cannot answer certain questions because of secrecy agreements or lack of knowledge, the student must learn to live with uncertainty. He will also learn how to defend his own views, and how to present material so as to obtain a favorable response from others. These learning experiences, coupled with exposure to the process of design as distinct from that of analysis and synthesis, are the major purposes of an introductory design course. 

Scheme 1. Retrosynthetie Analysis and Synthesis of Methyl Deoxypodocarpate a 9 then LiBF4, 99% b [(CH3)2N]2CHOC4H9-t then TsS(CH2)3STs, 91% c NaOCH3, CH3OH, 100% CHjI, CH3CN, H30, 100% (Ph3P)3RhCl, CH3CN, 64%...

Scheme 2. Retrosynthetic Analysis and Synthesis of Hinesol Precursor...

Scheme 4. Retrosynthetic Analysis and Synthesis of Trihydroxydecipiadiene 30 then H 52% b [(CH3)2N]2CHO-t-C4H9, 100% c CH3OH, TsOH, 92% d DIBAL-H ether then CH3OH, Dowex-50W-X-8-H + then PCC 87% See ref. 79 f HC1, H20, THF then Ph3PC(CH3)C02CH3, PhCH3, 100° then DIBAL-H, ether 56%...

Scheme 6. Retrosynthetic Analysis and Synthesis of Potential Verrucarol Intermediate " See secosulfenylation section and ref. 75) b 30 then TsOH, PhH, H20, 62 % c NaOH, H202...

Scheme 12. Retrosynthetic Analysis and Synthesis of 11-Deoxyprostaglandin E a C4H9Li, CHjMgl then 58 followed by DHP, PPTS, 67% b KF, H20, DMF then nC4H9Li, THF, n-CjH CHO followed by C2H5OH, PPTS, 61% c LAH, THF then TMS-C1, (C2H5)3N, DMSO, 72% " FVT, 100% c LiNH2, liq. NH3, BrCH2CH=CHCH2CH2—CH2-C02CH3,45%...

Scheme 13. Retrosynthetic Analysis and Synthesis of Isoretronecanol 37a b NH4C1, xylene c CH3OH, HC1 d LAH then Raney Ni (No yields)...

Scheme 15. Retrosynthetic Analysis and Synthesis of Methyl Trisporate B a C4H9Li then 43 then KH/THF followed by TMS-C1, C5H5N, ether 70% b FVT, 95% CH3OH, HC(OCH,)3, HC1, 68% d CH3MgBr, (dppp)NiCl2, THF, 75% HC1, H20, CH3CN, 100% f See Ref. 975...

Lavoisier, quoting Condillac, in the Dover edition, xiiixiv on analysis and synthesis, 33 on analogy,... 

Chenchik, A., Moqadam, F. and Siebert, P. A new method for full-length cDNA cloning by PCR. In A Laboratory Guide to RNA Isolation, Analysis and Synthesis. PA. Krieg, (ed.) Wiley Liss, Inc. pp. 273-321, 1996. 

R.J. Wiegerink, Analysis and Synthesis of MOS Translinear Circuits, Kluwer, 1993. 

R.E. Skelton. Dynamic Systems Control. Linear Systems Analysis and Synthesis. John Wiley Sons, New York, 1988. 

Katz, B. A., and H. Leith. Seasonality of decomposers, pp. 163-184. In H. Leith, Ed. Phenology and Seasonality Modeling (Ecological Studies Analysis and Synthesis, Vol. 8). New Yoilc Springer-Verlag, 1974. 

Volume 18 of Advances in Chemical Engineering returns to the dominant twin themes of modern chemical engineering the microscale of molecules and small particles, and the macroscale of entire engineering systems, of analysis and synthesis. 

The idea that the composition of a body could be confirmed by the cycle of analysis and synthesis is visible in practice, especially with neutral salts, but again the idea is only implicit through practice, but not explicitly stated. 

Of the modern ideas implicit in this book, the most important ones that become explicit in the next few decades are the concept of neutral salt as a combination of an acid with a base, that is, an alkali, an earth, or a metal. Neutral salts also provide the best examples of material composition as confirmed by analysis and synthesis. 

---