Spouting

Beakers. The usual Griffin form with spout. Fig. II, 1, 2, a, are widely used. Sizes between 30 ml. and 6 litres are available. The tall form without spout (Fig. II, 1, 2 6) occasionally finds application in organic laboratories. 

Fig. 13. Multistage spout-fluid-bed reactor. 1, spouted bed 2, perforated plate 3, spray no22le 4, air header 5, fluidi2ed bed.

Group D particles are large, on the order of 1 or more millimeters (1000 fim) in average particle size. In a fluidized bed, they behave similarly to Group B particles. Because of the high gas velocities required to fluidize Group D particles, it is often more economical to process these particles in spouted or in moving beds, where lower gas rates suffice. 

The ease with which the separated products leave the bowl determines the richness of the fat. Fluid whole milk enters the separator under pressure from a positive displacement pump or centrifugal pump with flow control (Fig. 1). The fat (cream) is separated and moves toward the center of the bowl, while the skimmed milk passes to the outer space. There are two spouts or oudets, one for cream and one for skimmed milk. Cream leaves the center of the bowl with the percentage of fat ( 30 40%) controlled by the adjustment of a valve, called a cream or skim milk screw, that controls the flow of the product leaving the field of centrifugal force and thus affects the separation. 

Flammable Hquids used in indoor workplaces and laboratories should be contained in approved safety cans having self-closing spouts and flash... 

Suspended Particle Techniques. In these methods of size enlargement, granular soHds are produced direcdy from a Hquid or semiliquid phase by dispersion in a gas to allow solidification through heat and/or mass transfer. The feed Hquid, which may be a solution, gel, paste, emulsion, slurry, or melt, must be pumpable and dispersible. Equipment used includes spray dryers, prilling towers, spouted and fluidized beds, and pneumatic conveying dryers, all of which are amenable to continuous, automated, large-scale operation. Because attrition and fines carryover are common problems with this technique, provision must be made for recovery and recycling. 

Chisso-Asahi uses a spouted bed process for the production of their coated materials (12). A 12,000 t/yr faciHty is located in Japan. The semicontinuous process consists of two batch fluid-bed coaters. A dilute polymer solution is prepared by dissolving 5% polymer and release controlling agent into a chlorinated hydrocarbon solvent such as trichloroethylene. The solution is metered into the spouted bed where it is appHed to the fertilizer core. Hot air, used to fluidize the granules, evaporates the solvent which is recovered and reintroduced into the process. Mineral talc, when used, is either slurried into the polymer solution or introduced into the fluidizing air. 

Spouted beds are used for coarse particles that do not fluidize well. A single, high velocity gas jet is introduced under the center of a static particulate bed. This jet entrains and conveys a stream of particles up through the bed into the vessel freeboard where the jet expands, loses velocity, and allows the particles to be disentrained. The particles fall back into the bed and gradually move downward with the peripheral mass until reentrained. Particle-gas mixing is less uniform than in a fluid bed. 

Spouted Beds The spoutedT)ed technique was developed primarily for sohds which are too coarse to be handled in fluidized beds. Although their applications overlap, the methods of gas-sohds mixing... 

On the basis of experimental studies, Mathur and Gishler derived an empirical correlation to describe the minimum fluid flow necessaiy for spouting, in 3- to 12-in-diameter columns ... 

Increasing bed diameter increases spoutable depth. By employing a bed-orifice diameter ratio of 12 for air spouting, a 9-in-diameter bed was spouted at a depth of 65 in while a 12-in-diameter bed was spouted at 95 in. 

As indicated by Eq. (12-62) the superficial fluid velocity required for spouting increases with bed depth and orifice diameter and decreases as the bed diameter is increased. 

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