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Process sensors calibration

Details are given of the development of an on-line sensor using near IR spectroscoy for monitoring carbon dioxide concentration in polymeric extrusion foaming processes. The calibration curve relating the absorbance spectrum at 2019 nm to the dissolved gas concentration was derived so as to infer dissolved carbon dioxide gas concentration... [Pg.57]

The second group consists of algorithms associated with the pesticide concentration quantification. In this case, the initial data is the processed sensor response for an unknown pesticide concentration and the parameters of the calibration curve (which is derived from preliminary experimental calibration measurements for a range of standard pesticide concentrations) or alternatively, a set of sensor responses obtained by addition of known amounts of pesticide to the analysed sample. This group of algorithms allows the automation of the pesticide quantification, thereby enabling the use of the instrumentation by unskilled personal. This removes the sensing platform from specialised laboratories to the realm of the end-users. [Pg.324]

Process chemometrics is a field where multi-way methods were introduced more recently. A batch process gives rise to an array of batches followed over time and measured by multiple process sensors such as temperature and pressure sensors or perhaps spectroscopy, as in Figure 10.3. Multi-way component models are used for the construction of control charts and multi-way regression is used for constructing predictive calibration models. [Pg.257]

Deflection and radius of curvature data, usually corrected for pavement temperature, are processed by specially developed software. Curviameter test standards and documents of CEDEX (2006), AENOR (1991) and MDRW (2002) include a detailed description of the measuring system and the test preparation, sensor calibration and the measurement principle and procedure. More details on the curviameter device can also be found in Ramos et al. (2013). [Pg.769]

The sensor calibration process encoimters several problems due to aperture effects (diameter of the sensor element is of the order of the wave-... [Pg.62]

Calibration of Process Sensors under the 21st Century Initiative. 255... [Pg.245]

In this chapter we address the issues stemming from calibration and validation of process sensors that will be used or interchanged with analyzers. Technically speaking, the establishment treats them rather differently. For cahbration and validation issues, in most cases a sensor element may make up one component of the analyzer, and the overriding issue is where these instruments are going to be used (e.g., in the manufacturing suite). It is from this vantage point that we will treat sensors and sensor systems equally with analyzers. [Pg.246]

The objective of this chapter will be to propose a scheme for demonstrating the accuracy, precision, and suitability of sensors. As will be seen, no matter what sensor, device, or measurement approach is chosen, these three simple criteria will be at the heart of the calibration/validation exercise. Depending on the complexity of the process, the sensor system, and process requirements necessary to achieve a mechanistic understanding, more parameters may be necessary. For example, linearity, range, specificity, robustness, raggedness, detection limit, and quantification hmit may also need to be investigated. By definition (see calibration and validation definition in this chapter), accuracy, precision, and suitability will be the minimum requirements for the cahbration/validation exercise of process sensors. [Pg.246]

This chapter explores the fundamental meaning and rationale behind measurement and control mechanisms and hopefully will lead the reader to view calibration and validation of process sensors as a very different exercise than the one that most analytical minds working in regulated industries have previously experienced in the laboratory. [Pg.246]

Under these practices then, calibration and validation of process sensor elements, sensors, and sensor systems used in a pharmaceutical manufacturing facility would have to be... [Pg.248]

The elements of calibration and validation of sensor systems are thus composed of all of the physical attributes that make up sensor systems, the functional aspects that determine the operational capability of these systems, and finally the parameters that determine the frequency of verification, the sensor system variables that determine the operational range, and the process/sensor standards that will be used during the verification phases of the sensor systems. [Pg.249]

Calibration of process sensors is verified at minimum by demonstrating accuracy and precision of signal transduction, and that the resultant impulse is transmitted accurately and precisely to its intended target. [Pg.249]

CALIBRATION OF PROCESS SENSORS UNDER THE 21 ST CENTURY INITIATIVE... [Pg.255]

Keeping in mind the nominal requirements for cGMP compliance requirements for lab-based instruments for demonstrating calibration (checking, adjustments, accuracy, precision, and traceability), what are some of the capabilities that will need to exist for process sensors or monitoring systems, and how will they be calibrated ... [Pg.255]

With respect to cGMPs that will be used to regulate how process sensors will be calibrated and validated, new application and architectural schemes are being proposed for the design, qualification, installation, operation, and maintenance of in-line and on-line sensors. [Pg.258]

Comparison between Traditional Calibration and Validation Strategy for Laboratory-Based Instruments and Process Sensors and Analyzers... [Pg.262]

Provides new chapters on diffuse reflection theories, the calibration and validation of process sensors, and the NIR spectra of gases... [Pg.817]

Consistency sensor calibration Measurement of fiber or filler consistency is one of the most demanding process measurements. Accuracy has to be very high for control purpose but consistency meters are sensitive to a lot of process parameters like gas content, flow rates, etc. Therefore wet end control comprises a means to improve the calibration of consistency meters, by taking other process parameters into account. Thus the advanced consistency sensor calibration uses a soft sensor calibration technique. [Pg.414]


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