Filtration characteristics determination

The overriding factor will be the filtration characteristics of the slurry whether it is fast filtering (low specific cake resistance) or slow filtering (high specific cake resistance). The filtration characteristics can be determined by laboratory or pilot plant tests. A guide to filter selection by the slurry characteristics is given in Table 10.3 which is based on a similar selection chart given by Porter et al. (1971). 

Determine the permeation and filtration characteristics of a coffee filter. 

Fig. 11.12. Diagram of a system used to determine filtration characteristics 1, compressed air source 2, feed vat 3, pressure gauge 4, valve 5, single disk Alter (surface area of 22 cm ) 6, purge valve 7, graduated container...

Qin et have studied the filtration characteristics of nanofibre layers with different area densities that were electrospun onto spunlaid or meltblown substrates. The fibre diameter, pore diameter, filtration efficiency, and filtration resistance of nanofibre webs and sublayers were determined. It was found that the pore diameter of nanofibre web is much smaller than sublayers and the coefficient of variation of the pore diameter of nanofibre webs is also smaller than that of the sublayers. Consequently, the filtration efficiency and filtration resistance of sublayers are lower than the nanofibre webs. These researchers also found that there is an optimum region for the maximum filtration efficiency at minimum pressure drop and that this optimum is at a lower add-on weight for meltblown webs than for spunlaid webs. 

Nanoparticle penetration has been measured with a wide range of filter media by using silver nanoparticles from 3 nm to 20 nm at three different face velocities in order to define nanoparticle filtration characteristics of commercial fibrous filter media. After size classification by using a nano-DMA, the particle counts were measured by an ultrafine condensation particle counter (UCPC) both upstream and downstream of the test filter in order to determine the nanoparticle penetration for each specific... 

Murase, T. Mtani, E., Cho, J.H., Nakanomori, S. and Shirato, M., 1987, Determination of filtration characteristics due to sudden reduction in filtration area of fiber cake surface, Chem Eng. Japan J. 20, pp 246-251. 

Tlie time required to reduce the solubles in a slurry to a desired level is a function of the feed solids concentration. The qrtimum washing concentration can be determined from tlie slurry s filtration characteristics. 

Apart from the availability of a wide range of materials for manufacturing the fibres themselves, the construction and filtration characteristics of a filter cloth are determined by the type of yam, the weave or fabric construction properties and the finish applied to the cloth. 

The examples which follow show how data from the correlations justpresented and a knowledge of thephysical characteristics of a particular filter are used to determine a filtration cycle and, subsequently, the size of the filter itself. The three examples which follow involve a disk, a drum belt, and a horizontal belt filter. 

To use Eq. (18--50) one must know the pattern of the filtration process, i.e., the variation of the flow rate and pressure with time. Generally the pumping mechanism determines the filtration flow characteristics and serves as a basis for the following three categories [Tiller and Crump, Chem. Eng. Prog., 73(10), 65 (1977)] ... 

Effect of pH, dye concentration, size of pores of paper filters and their hydrophobic characteristics, filtration rate, nature and hydrocarbon radical length cSurf on sensitivity of their determination was studied. 

Typical new equipment design efficiencies are between 99 and 99.9%. Older existing equipment have a range of actual operating efficiencies of 95 to 99.9%. Several factors determine fabric filter collection efficiency. These include gas filtration velocity, particle characteristics, fabric characteristics, and cleaning mechanism. In general, collection efficiency increases with increasing filtration velocity and particle size. 

Parameters q and W are variables when filtration conditions are changed. Coefficient (rj, is a function of pressure (rj, = f(P). The exact relationship can be derived from experiments in a device called a compression-permeability cell. Once this relationship is defined, the integral of the right hand side of the above equation may be evaluated analytically. Or, if the relationship is in the form of a curve, the evaluation may be made graphically. The interrelation between W and P, is established by the pump characteristics, which define q = f(W) in the integral. Filtration time may then be determined from dq/dt = W, from which we may state ... 

Filtration operations are capable of handling suspensions of varying characteristics ranging from granular, incompressible, free-filtering materials to slime-like compositions, as well as finely divided colloidal suspensions in which the cakes are incompressible. These latter materials tend to contaminate or foul the filter medium. The interaction between the particles in suspension and the filter medium determines to a large extent the specific mechanisms responsible for filtration. 

Filter aids may be applied in one of two ways. The first method involves the use of a precoat filter aid, which can be applied as a thin layer over the filter before the suspension is pumped to the apparatus. A precoat prevents fine suspension particles from becoming so entangled in the filter medium that its resistance becomes exces-sive. In addition it facilitates the removal of filter cake at the end of the filtration cycle. The second application method involves incorporation of a certain amount of the material with the suspension before introducing it to the filter. The addition of filter aids increases the porosity of the sludge, decreases its compressibility, and reduces the resistance of the cake. In some cases the filter aid displays an adsorption action, which results in particle separation of sizes down to 0.1 /i. The adsorption ability of certain filter aids, such as bleached earth and activated charcoals, is manifest by a decoloring of the suspension s liquid phase. This practice is widely used for treating fats and oils. The properties of these additives are determined by the characteristics... 

The characteristics of the pump relate the applied pressure on the cake to the flowrate at the exit face of the filter medium. The cake resistance determines the pressure drop. During filtration, liquid flows through the porous filter cake in the direction of decreasing hydraulic pressure gradient. The porosity (e) is at a minimum at the point of contact between the cake and filter plate (i.e., where x = 0) and at a maximum at the cake surface (x = L) where sludge enters. A schematic definition of this system is illustrated in Figure 2. 

The selection of column characteristics is determined by solvent resistance, the need to visually inspect the bed, the pressure rating of the system, and the dimensions [column inner diameter (i.d.) and length (L)] required from productivity considerations. Productivity considerations will vary if the requirement is based on the amount of information per unit time (analytical gel filtration) or the amount of substance per unit time (preparative gel filtration). 

API Filtration. A filter press is used to determine the wall building characteristics of mud. The press consists of a cylindrical mud chamber made of materials resistant to strongly alkaline solutions. A filler paper is placed on the bottom of the chamber just above a suitable support. The filtration area is 7.1 ( 0.1) in.-. Below the support is a drain tube for discharging the filtrate into a graduate cylinder. The entire assembly is supported by a stand so that a 100-psi pressure can be applied to the mud sample in the chamber. At the end of the 30-min filtration time volume of filtrate is reported as API filtration in milliliters. To obtain correlative results, one thickness of the proper 9-cm filter paper, Whatman No. 50, S S No. 5765, or the equivalent, must be used. 

Resistivity. Control of the resistivity of the mud and mud filtrate while drilling may be desirable to permit better evaluation of formation characteristics from electric logs. The determination of resistivity is essentially the measurement of the resistance to electrical current flow through a known sample configuration. Measured resistance is converted to resistivity by use of a cell constant. The cell constant is fixed by the configuration of the sample in the cell and is determined by calibration with standard solutions of known resistivity. The resistivity is expressed in ohm-meters. 

Some properties of Penicillium fellutanum pectinesterase were studied. The optimum of pectinesterase action was detected at pH 5 and 45 °C. The enzyme was stable at pH 4 — 5 and 40 °C (pH 5) for 240 min. and was specific towards lemon pectin. An enzyme preparation composed mainly of pectinesterase was partially purified by gel filtration. Pectinesterase activity was accumulated in one of the obtained fractions. Molecular weights of fraction determined were found to be 46,000 and 1,200. Disk electrophoresis in polyacrilamide gel of the purified preparation revealed two protein bonds with one active component. The partially purified enzyme had the kinetic characteristics =... 

For fine suspended solids with particles that are too small to be separated from the liquid by gravitational or centrifugal methods, a barrier method such as a filter may be used. The liquid is passed through a filter medium (usually a cloth or screen) that provides a support for the solid particles removed from the slurry. In actuality, the pores in the filter medium are frequently larger than the particles, which penetrate some distance into the medium before being trapped. The layer of solids that builds up on the surface of the medium is called the cake, and it is the cake that provides the actual filtration. The pressure-flow characteristics of the porous cake primarily determine the performance of the filter. 

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