Biogenic amines liquid chromatography

Figure 7. Separation of eight biogenic amines using ion pair partition liquid chromatography. Conditions 30 cm column with 4 fim silica stationary phase, 0.1M HClO /0.9M NaClO mobile phase, ethylacetate/tributyl phosphate/hexane (72.5/10/17.5) velocity, 0.8 cm/sec (47).

Hoekstra, J. C. and Johnson, D. C., Comparison of potential-time waveforms for the detection of biogenic amines in complex mixtures following their separation by liquid chromatography, Anal. Chem., 70, 83, 1998. 

Song Y, Quan Z, Evans JL, Byrd EA, Liu YM. 2004. Enhancing capillary liquid chromatography/tandem mass spectrometry of biogenic amines by pre-column derivatization with 7-fLuoro-4-nitrobenzoxadiazole. Rapid Commun Mass Spectrom 18 989. 

Niederwieser A, Staudenmann W, Wetzel E (1984) High-performance liquid chromatography with column switching for the analysis of biogenic amine metabolites and pterins. J Chromatogr 290 237-246... 

I Krause, A Bockhardt, H Neckermann, T Henle, H Klostermeyer. Simultaneous determination of amino acids and biogenic amines by reversed-phase high-performance liquid chromatography of the dabsyl derivatives. J Chromatogr A 715 67-79, 1995. 

T Bauza, A Blaise, F Daumas, JC Cabanis. Determination of biogenic amines and their precursor amino acids in wines of the Vallee du Rhone by high-performance liquid chromatography with precolumn derivatization and fluorimetric detection. J Chromatogr A 707 373-379, 1995. 

Antila, P., Antila, V., Mattila, J., and Hakkarainen, H. (1984). Biogenic amines in cheese. 1. Determination of biogenic amines in Finnish cheese using high performance liquid chromatography. Milchwissenschaft 39, 81-85. 

Lange, J., Thomas, K., and Wittmann, C. (2002). Comparison of a capillary electrophoresis method with high-performance liquid chromatography for the determination of biogenic amines in various food samples. /. Chromatogr. B. 779, 229-239. 

J. C. Hoekstra and D. C. Johnson, Comparison of Potential-Time Waveforms for the Detection of Biogenic Amines in Complex Mixtures Following Their Separation by Liquid Chromatography, Anal. Chem. 70, 83-88, (1998). 

Hlabangana, L., Hemandez-Cassou, S., and Saurina J. Determination of biogenic amines in wines by ion-pair liquid chromatography and post-column derivatization with... 

Lavizzari, T. et al. Improved method for determination of biogenic amines and polyamines in vegetable products by ion-pair high-performance liquid chromatography. J. Chromatogr. A. 2006, 1129, 67—72. 

Thin-Layer Chromatography (TLC) is a rapid and simple technique to detect several amines. This was one of the first techniques used to determine biogenic amines in foods (Halasz et al. 1994). Recently, a simple and rapid qualitative TLC method to determine the ability of bacteria to produce biogenic amines in liquid culture media containing the amino acid precursor was described by Garci a-Moruno et al. (2005). 

Constantini, A., Cersosimo, M., Del Prete, V. Garcta-Moruno, E. (2006). Production of biogenic amines by lactic acid bacteria screening by PCR, thin-layer chromatography, and high-performance liquid chromatography of strains isolated from wine and must. J. Food Prot., 69, 391-396. 

Mdlan, S., Sanpedro, M.C., Unceta, N., Goicolea, M.A. Barrio, R.J. (2007). Simple and rapid determination of biogenic amines in wine by liquid chromatography-electronspray ionization ion trap mass spectrometry. Anal. Chim. Acta, 584, 145-152. 

M7. Mee, T. J. X., and Smith, ]. A., High pressure chromatographic separation of some biogenic amines and derivatives implicated in the aetiology of schizophrenia. In High Pressure Liquid Chromatography in Clinical Chemistry (P. F. Dixon, C. H. Gray, C. K. Lim, and M. S. Stoll, eds.), pp. 119-124. Academic Press, New York, 1976. 

Many analytical techniques such as, radiochemistry, gas chromatography, and liquid chromatography have been developed for the determination of biogenic amines, their precursors, and metabolites. HPLC with electrochemical detection is considered to be one of the most popular methods for determining biogenic amines, owing to its simplicity, versatility, sensitivity, and specificity. 

Schmizu, T. and Mihara, M., High-performance liquid chromatography of biogenic amines in the corpus cardiacum of the American cockroach, Periplanela americana, J. Chromalogr., 539, 193-197, 1991. 

Wei, Q.-K., Chen, T.-R., and Fang, C.-W. (1995). Analysis of biogenic amines in fish muscles by high performance liquid chromatography. J. Food Drug Anal. 3(4), 313. 

Ion-pair reversed-phase liquid chromatography (LC), as introduced by Johansson et al. in 1978 (1) is still the most widely used separation technique for analysis of the biogenic amines. It is usually coupled with electrochemical detection (ECD). The use of microbore LC was introduced by Scott and Kucera in 1976 (2). These systems use columns with an internal diameter (id) of 1 mm or less. Microbore LC provides a significant advantage over conventional LC The sample injected on to a microbore column is diluted by about 20-fold less than when injected on to a normal bore (e.g., 4.6 mm id) column. In this way, the compounds of interest become easier to detect. Microbore LC offers several other advantages ... 

Almeida, C., Fernandes, J. O., Cunha, S. C. (2012). A novel dispersive liquid-liquid microextraction (DLLME) gas chromatography-mass spectrometry (GC-MS) method for the determination of eighteen biogenic amines in beer. Food Control, 25, 380-388. http //dx.doi.Org/10.1016/j.foodcont.2011.10.052. 

Jia, S., Kang, Y. R, Park, J. H., Lee, J., Kwon, S. W. (2011). Simultaneous determination of 23 amino acids and 7 biogenic amines in fermented food samples by liquid chromatog-raphy/quadrupole time-of-flight mass spectrometry. Journal of Chromatography A, 1218, 9174-9182. http //dx.doi.Org/10.1016/j.chroma.2011.10.040. 

Kirschbaum, J., Rebscher, K., Bruckner, H. (2000). Liquid chromatographic determination of biogenic amines in fermented foods after derivatization with 3,5-dinitrobenzoyl chloride. Journal of Chromatography, 881,517-530. http //dx.doi.org/ 10.1016/S0021 -9673(00)00257-0. 

Lee, S., Eom, H.-S., Yoo, M., Cho, Y, Shin, D. (2011). Determination of biogenic amines in Cheonggukjang using ultra high pressure liquid chromatography coupled with mass spectrometry. Food Science and Biotechnology, 20, 123-129. http //dx.doi.org/ 10.1007/S10068-011-0017-6. 

Mayer, H. K., Fiechter, G., Fischer, E. (2011). A new ultra-pressure liquid chromatography method for the determination of biogenic amines in cheese. Journal of Chromatography A, 1217, 3251-3257. 

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