Problems troubleshooting guide

With all types of plastic processes, troubleshooting guides are set up to take fast, corrective action when products do not meet their performance requirements. This problem-solving approach fits into the overall fabricating-design interface. One brief example of troubleshooting an RP/composite is in Table 8-44. 

Problems with the mechanics of a procedure can involve an improperly diluted sample (perhaps manifested by an absorbance reading that is greater than specified or expected), an obstruction in the sample or reference beam, an improperly aligned source or mirror, the incomplete programming of a scan, or improper or inappropriate software entry. In these cases, the operator will need to carefully examine his or her technique or procedure, or instrumental parameters, such as the optical path, perhaps with the help of the instrument troubleshooting guide, to solve the problem. 

Problems that arise with HPLC experiments are usually associated with abnormally high or low pressures, system leaks, worn injectors parts, air bubbles, or blocked in-line filters. Sometimes these manifest themselves on the chromatogram and sometimes they do not. In the following subsections, we address some of the most common problems encountered, pinpoint possible causes, and suggest methods of solving the problems. You can also refer to the troubleshooting guide in Chapter 12 for possible solutions. 

Spruce, B. and Bakalyar, S. R., Troubleshooting Guides for HPLC Injector Problems, Rheodyne.com/Docs/Tech/Docs/TSl.html... 

Often troubleshooting guides are provided by equipment manufacturers for common problems. These guides are helpful for many of the simpler problems associated with the equipment. Some resin manufacturers are an excellent resource for troubleshooting processing problems that are specific to a resin. Subject matter experts or extrusion consultants are also resources for troubleshooting an extrusion process. 

It is imperative that the HPLC instrument, including the detector, is working correctly. The easiest way to check this is by first running a blank. If there is no response, one can move onto injecting the standards. If there is a response to the blank, the column may have been overloaded prior to this run. Refer to a troubleshooting guide for the specific HPLC system. The internet is also an invaluable source for troubleshooting (e.g., see Internet Resources). Keep in mind that the source of the problem may not be the system but may in fact be the column. 

Technical Report, A Troubleshooting Guide to Plumbing Problems in HPLC, MAC-MOD Analytical Inc., Chadds Ford, PA. 

Records also help prevent mistakes, such as introducing water into a silica column, or precipitating buffer in the system by adding too much organic solvent. Many analysts occasionally modify their HPLC systems for a variety of reasons. Reliable records are the best way to ensure that a modification does not introduce problems. For problems relating to pumps, detectors, automatic samplers, and data systems, instrument manuals provide suitable troubleshooting guides. 

The above troubleshooting guide does not cover every possible cause for an assay failure, but it discusses the most common problem origins. Other resources are available on company web sites and in assay design guidebooks. 

Table 3-11. Troubleshooting Guide Common Extrusion Problems and How to Solve Them.

Table 3-12 presents a troubleshooting guide for plastic foam film. One must be aware that causes of problems are not always obvious for example, Fig. 3-35 shows contamination in the die presenting a problem that is almost impossible to resolve by equipment controls. 

As described in Chapters 2, 3, and 10, there is a logical approach to setting up a troubleshooting guide. Details reviewed in those chapters concerning the approach to be used are applicable to BM and other processes. Table 4-14 lists some of the common BM problems with information on causes and solutions (192). 

This appendix follows the instructions in the appendices to Chapters 2 and 6. Although the Aspen Plus simulator is referred to, other process simulators can be used. The three problems in this appendix all employ recycle streams in distillation columns. The procedures shown here to obtain convergence are all forms of stream tearing. Since these are not the only methods that will work, you are encouraged to experiment with other approaches. If problems persist while running the simulator, see Appendix A Aspen Plus Separations Troubleshooting Guide, at the end of the book. 

Older motor drive systems generally consist of a DC brush motor, a power conversion unit (PCU), and operator controls. A frequent problem with the motor itself Is worn brushes these should be replaced at regular Intervals as recommended by the manufacturer. In troubleshooting an extruder drive, one should follow the procedure recommended by the manufacturer of the drive. A typical troubleshooting guide for a DC motor is shown in Table 11.2. 

By way of example Tables D. 1-D.6 present a troubleshooting guide to the problems that may be encountered during the operation of a diaphragm filter press descriptions of basic press operation are provided in Sections 1.4.2.5 and 6.1.4. Each potential phase in the filter cycle is considered in turn, and the effects of faults that either exist at the start of the cycle or develop during operation are related to the resultant operation of the press. It is intended that the reader can use the guidance presented to troubleshoot the operation of other filters and presses. 

Table 8-2 presents in chart form a troubleshooting guide for molding problems. 

The preparation of troubleshooting guides provides a very effective training exerci.se for commissioning supervisors and can be of great value later, such as when problems develop in the early hours during a night shift. 

Guidelines are presented for the maintenance of mixers used in the rabber industry. A troubleshooting guide lists typical operational problems, their causes and solutions. 

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