Piston seal, replacing

Piston Seal The piston seal replacement procedure can be more elaborate and is highly dependent on the particular pump model. A piston seal service kit from the manufacturer should be purchased and the procedure from the service manual should be followed closely for this operation. Typically, the piston should be fully retracted before dismantling the pump head and replacing the seal. A lower than expected system pressure and/or a leak behind the pump head are indications for the need to... 

LC pumps—replace or clean piston seals, pistons, in-line filter, solvent filter sinkers and check valves. 

Annual preventive maintenance, in which most wearable items such as pistons, seals, lamps, and filters are replaced, is to be scheduled before calibration. 

Cautionary note A number of the HPLC methods listed in this chapter use phosphate buffers as solvents. It should always be remembered that phosphate salts are very abrasive to piston seals and pistons. If using these systems, always remember to wash out the aqueous pump thoroughly with water at the end of a run. If this operation is not carried out, the piston seal lifetime will be significantly reduced and in some cases, if left too long, pistons can stick and possibly fracture, which will be expensive to repair/replace. 

Piston seal(s) worn. Replace piston seal(s). 

Piston seals become worn and need to be replaced, e.g. once a year (they cannot be repaired). For this purpose the pump head is removed from the pump body then the seals become visible. They are removed with the special tool which was delivered together with the pump. Removing the seals with a screwdriver can scratch the pump head which causes leaking The new seals are brought in place with another special tool. It is necessary to follow the instructions exactly. One must not mix up the two different sides of a seal. A seal which is placed the wrong way must be removed and thrown away it cannot be used once again. The new seals need to be broken in with a low solvent flow and without a column connected. Water should be avoided to break in a new seal. Well suited solvents are isopropanol and methanol. 

Common maintenance tasks that can be easily performed by the user are the replacement of solvent filters (sinkers), in-line filters, check valves, and piston seals. Most modern HPLC pumps are designed for easy maintenance, with front panel access to many internal components. Figure 10.1 is a diagram of a slide-out pump unit showing the two pump heads with check valves, the purge valve, the in-line filter, and other components. Procedures for replacing some consumable items are summarized below ... 

If reconnecting the column fails to correct the leak, then other common areas to search for leaks are the detector flow cell, the pump (around the pistons), and the injector valve. The same process should be followed until the source of the leak is identified and corrected. New parts maybe required for example, the pump piston seals may have worn out. Always consult the manufacturer s user manual when attempting to replace any part. If in doubt, contact the manufacturer and ask for installation of the new part. It will be necessary to undertake system performance qualification on the replacement of any worn out or damaged part (see Chapter 8). 

Leak around the piston flushing seals or of the high pressure seals —> Replace the seals, check the pistons for damage and replace if necessary. 

A first round of the systematic review of the reactor operating eiqierience has been completed for the absorber rod drive mechanisms, main sodium pumps and intermediate heat exchangers (IHXs) which has revealed sensitive points for EFR. Examples are the importance of succeeding with the EFR features which prevent die sodium aerosol problems on the absorber mechanisms, the need to confirm adequate operational flexibility whilst avoiding the check valve at the primary pump outlet and to ensure full benefit is taken of the piston seal experience for the IHX / pool boundary replacing the gas bell originally selected for EFR. 

Broken piston No flow visual observation Replace piston and piston seal... 

Replace piston seals at least once a year and pistons every two years. 

If aggressive or toxic materials have to be conveyed, hermetically sealed constructions are necessary. Diaphragm pumps meet this requirement because the never absolutely leakproof piston seal (dynamic or grinding seals are never absolutely leakproof) has been replaced by the diaphragm s static seals at the diaphragm clamp. 

This pump is the same in principle as the piston type but differs in that the gland is at one end of the cylinder making its replacement easier than with the standard piston type. The sealing of piston and ram pumps has been much improved but, because of the nature of the fluids frequently used, care in selecting and maintaining the seal is very important. The piston or ram pump may be used for injections of small quantities of inhibitors to polymerisation units or of corrosion inhibitors to high pressure systems, and also for boiler feed water applications. 

By essential difference of offered presses (Fig. 4 also [6]) is the hermetic sealing of mobile plungers executed on the scheme barrel - seal [5], At the expense of replacement of a sliding coupler - barrel - cylinder piston by a pair barrel - seal and selection of radial spaces under the offered mathematical formula [5], the airtightness is guaranteed, close to absolute (weight of an offset of working fluid on a surface of a rod is peer to zero point). 

In case of pump seal failure, pump seals should be replaced, or the piston should be checked for scratches and should be replaced if necessary. 

The frequent use of ethanol in UFA systems is an example of a required process modification. These systems have required alterations to the elastomers used in the valves and seals of filling equipment due to different extraction and solvent profiles. Also, ethanol is corrosive to unprotected aluminum, and this must be taken into consideration [1]. In terms of manufacturing environment, large quantities of potentially flammable solvents must also be a factor in process design. For pressure filling of HFA propellants, the piston ram system may be replaced by the diaphragm displacement system [1]. 

Replace the frit. If black particles are visible on the frit (rather common) it is necessary to replace the high-pressure seal and perhaps also the piston. In addition, check if the seal is resistant to the solvent in use. (However, today s seal materials should be resistant to all common solvents, including water.)... 

Replace the seals, check the pistons for damage and replace if necessary. 

Seals Worn due to issues with piston Buffer salt deposits Months Replace the pump seals on a 3-month basis, depending on the nature of the mobile phase... 

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