Pellet micro

A natural extension of the investigations of single-pellet micro-imaging is to explore the effect of pore structure on the spatial distribution of coke deposition... 

Particle Pellet Micro Macro Total Macro Micro... 

A natural extension of the investigations of single-pellet micro-imaging is to... 

Insulin (molecular weight 7000) has been formulated in controlled release microbeads and pellets (135,136). A solvent evaporation micro-encapsulation procedure was used to produce microspheres with up to 20% by weight insulin. Solvent-casting techniques were used to prepare pellets. The investigations demonstrated that the PLA... 

In order to compare the micro-channel and the fixed-bed reactor, the design and operation parameters should be adjusted in such a way that certain key quantities are the same for both reactors. One of those key quantities is the porosity s, defined as the void fraction in the reactor volume, i.e. the fraction of space which is not occupied by catalyst pellets or channel walls. The second quantity is the specific... 

In order to verify that the fixed bed and the micro-channel reactor are equivalent concerning chemical conversion, an irreversible first-order reaction A —) B with kinetic constant was considered. For simplicity, the reaction was assumed to occur at the channel surface or at the surface of the catalyst pellets, respectively. Diffusive mass transfer to the surface of the catalyst pellets was described by a correlation given by Villermaux [115]. 

In practice, granular beds comprising a very large number of catalyst pellets are used. It is well known that the efficiency of a catalytic reactor depends crucially on the liquid phase distribution within the catalyst bed [14]. It is likely that the development of hot spots in a catalyst bed is also related to the character of liquid phase distribution. Therefore, it is very important to map the spatial distribution of the liquid phase in a catalytic reactor for various operation regimes. This eventually should lead to the formulation of the mechanisms responsible for the development of critical phenomena on both a micro- and macroscale. 

Only in a few cases are test samples measurable without any treatment. As a rule, test samples have to be transformed into a measurable form that optimally corresponds to the demands of the measuring technique. Therefore, sample preparation is a procedure that converts a test sample into a measuring sample. Whereas test samples represent the material in its original form, measuring samples embodies a form that is able to interact with the measuring system in an optimum way. In this sense, measuring samples can be solutions, extracts, pellets, and melt-down samples, but also definite surface layers and volumes in case of micro- and nanoprobe techniques. 

The high specific surface area supports (10 to 100 m2/g or more) are natural or man-made materials that normally are handled as fine powders. When processed into the finished catalyst pellet, these materials often give rise to pore size distributions of the macro-micro type mentioned previously. The micropores exist within the powder itself, and the macropores are created between the fine particles when they... 

Resuspend the cells pellet with 350 [A of lysis buffer, transfer to a micro tube with a screw cap, and add ice-cold glass beads (diameter 0.4—0.6 mm) to cover the cells and lysis buffer. 

Transfer the resulting lysate from the 15-ml tube to a new ice-cold micro tube. Usually, there is a small pellet that should be resuspended with the supernatant and also transferred to the micro tube. 

K. Shen, S. Curran, H. Xu, S. Rogelj, Y. Jiang, J. Dewald, and T. Pietrass, Single-walled carbon nanotube purification, pelletization, and surfactant-assisted dispersion a combined term and resonant micro-Raman spectroscopy study. J. Phys. Chem. B 109, 4455 1463 (2005). 

For the chemical reactor, the researchers used a nanoparticle catalyst deposited on metallic micro-structured foils. They tested Cu/ZnO and Pd/ZnO catalysts deposited on the microstructured foils. The Cu/ZnO catalyst was more active than the Pd/ZnO catalyst and had a lower selectivity to undesired carbon monoxide. However, because the Pd/ZnO catalyst was more stable, it was selected for use in their fuel processor. The Pd/ZnO carbon monoxide selectivity of the powder catalyst pressed into a pellet was lower than that of the nanoparticle catalyst deposited on the microstructured foils. This effect was attributed to contact phases between the catalyst and the metal foils. ... 

Mineral standards were hand crushed to -1/4 inch, then ground to a fine powder in a ball mill (alumina elements) or Bleuler Model 526/LFS678 puck mill. The resultant powder was aerodynamically classified in a Bahco Model 6000 micro particle classifier and the finest fraction ( 18 throttle) was collected. A size criterion of 90% or more by weight of particles 5 micron and smaller in diameter was used for the mineral standards. Sizes were verified by Coulter Counter. Duplicate 13 mm KBr pellets were prepared and the spectra were weight-scaled by techniques similar to those reported by Painter (3) and Elliot (4). With one exception, all the mineral standard spectra were averages of spectra from duplicate pellets. The one exception was the iron sulfate spectrum, which was obtained as the difference spectrum by subtracting the spectrum of HCl-washed weathered pyrite from that of the weathered pyrite. A weight correction was applied to the difference spectrum. 

For ethanol production a substantial improvement over the packed bed reactor is offered by the gas-solid fluidized bed fermenter which uses a liquid instead of a solid substrate and replaces the packed bed of substrate or micro-organisms with a fluidized bed of yeast pellets (Smith et al, 1997). This system can be viewed as a standard fermentation against which the performance of different bioreactors may be assessed. 

Polymer processing can be defined as the process whereby raw materials are converted into products of desired shape and properties. Thermoplastic resins are generally supplied as pellets, marbles, or chips of varying sizes and they may contain some or all of the desired additives. When heated above their Tg, thermoplastic materials soften and flow as viscous liquids that can be shaped using a variety of techniques and then cooled to lock in the micro- and gross structure. 

Wakao and Smith [20] originally developed the random pore model to account for the behaviour of bidisperse systems which contain both micro- and macro-pores. Many industrial catalysts, for example, when prepared in pellet form, contain not only the smaller intraparticle pores, but also larger pores consisting of the voids between compressed particles. Transport within the pellet is assumed to occur through void regions... 

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