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The shape of nanocrystallites of natural cellulose is a subject of discussion. In several studies the cross-sectional shape of the crystallites was depicted as a square or rectangle. However, recent studies have shown that the most likely cross-sectional shape of the crystallites of natural cellulose is a hexagon (Ding and Himmel, 2006 loelovich, 1991 Yang et al., 2011). Three groups of planes (100), (110), and (110) are located on the surface of crystallites, allowing the co-crystallization process of adjacent crystallites in different lateral directions (loelovich, 1991). The co-crystallization process observed during extraction and hydrolysis of cellulose leads to an increase in lateral sizes of crystallites. [Pg.248]

Once the primary electron beam is created, it must be demagnified with condenser lenses and then focused onto the sample with objective lenses. These electron lenses are electromagnetic in nature and use electric and magnetic fields to steer the electrons. Such lenses are subject to severe spherical and chromatic aberrations. Therefore, a point primary beam source is blurred into a primary beam disk to an extent dependent on the energy and energy spread of the primary electrons. In addition, these lenses are also subject to astigmatism. AH three of these effects ultimately limit the primary beam spot size and hence, the lateral resolution achievable with sem. [Pg.271]

The perforated pipe distributor comprises a central feed sump and pipes that branch out from the sump to provide the liquid discharge. The level in the sump varies with liquid total flow rate, and the size of the lateral pipes and their perforations must be determined carefully to ensure that the ends of the pipes are not starved for hquid. The orifices are typically 4 to 6 mm diameter, and can be subject to phigging if foreign matter is present. The pipes must be leveled carefully, especially for large diameter columns. [Pg.1396]

In water-retaining structures or basement concrete subject to high hydrostatic pressure, materials of this type are generally not beneficial. However, some dampproofing admixtures do contain water-reducing admixtures and will result in a reduction in permeability under an applied hydrostatic head. In addition, the reduced capillary size and quantity will increase the hydrostatic pressure required to enter the concrete surface (see later). [Pg.230]

Prior to radiochemical analysis the samples were ashed and separated into size fractions by means of procedures described by Nathans et al. The determinations of the fraction weights and of the mean diameters of the particles in the fractions have also been described extensively in the same paper. An aliquot of each size fraction was dissolved and subjected to a separation procedure to isolate Sr, Ru, Sb, Cs, Ce, Pm, U, and Pu fractions. The procedure is sketched in Figure 1. Further decontamination of Ru and Ce was carried out only with the Johnie Boy sample. The Sb and Pu fractions were set aside for later analysis. After complete analysis of the Cs fractions, anomalies were found in the data for the coral samples. These samples had been ashed at about 475°C. Apparently some Cs had volatilized at this temperature. Such a behavior explained the anomalies, and this was confirmed by Heft by more extensive experimentation (4). Thus, Cs data are reported only for the Johnie Boy sample, which was ashed at low temperature in a Tracerlab low temperature asher. [Pg.362]


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See also in sourсe #XX -- [ Pg.38 ]




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