Solid-state nuclear magnetic resonance quantitative analysis

Abstract Modern solid state nuclear magnetic resonance presents new powerful opportunities for the elucidation of medium range order in glasses in the sub-nanometer region. In contrast to standard chemical shift spectroscopy, the strategy presented here is based on the precise measurement and quantitative analysis of internuclear magnetic dipole-dipole interactions, which can be related to distance information in a straightforward manner. The... 

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Cody G. D., Alexander C. M. O D., and Tera E. (2002) Solid-state ( H and C) nuclear magnetic resonance spectroscopy of insoluble organic residue in the Murchison meteorite a self-consistent quantitative analysis. Geochim. Cosmochim. Acta 66, 1851-1865. 

A 13C nuclear magnetic resonance (NMR) study in solution and in the solid state has been reported for three thermochromic spirooxazines, 29-31.32 From a quantitative analysis of I3C cross-polarization/magic-angle-spinning (CP-MAS) NMR spectra shielding anisotropies were estimated and a correlation of these characteristics with thermochromic activity was suggested. 

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