Scanning electron microscopy materials

Physical testing appHcations and methods for fibrous materials are reviewed in the Hterature (101—103) and are generally appHcable to polyester fibers. Microscopic analyses by optical or scanning electron microscopy are useful for evaluating fiber parameters including size, shape, uniformity, and surface characteristics. Computerized image analysis is often used to quantify and evaluate these parameters for quaUty control. 

To ensure quality control material suppliers and developers routinely measure such complex properties as molecular weight and its distribution, crystallinity and crystalline lattice geometry, and detailed fracture characteristics (Chapter 6). They use complex, specialized tests such as gel permeation chromatography (2, 3), wide- and narrow-angle X-ray diffraction, scanning electron microscopy, and high-temperature pressurized solvent reaction tests to develop new polymers and plastics applications. 

This paper summarises an initial feasibility on reeyling scrap automotive plasties and eomposites using a eatalytie conversion process. The eharaeterisationofhydroearbon products is presented for sheet moulding compound (SMC), auto shredder residue (ASR) and reinforeed polypropylene (R-PP) materials and mixtures of body panels. Gas chromatography and scanning electron microscopy is used for the material characterisation. 26 refs. 

A Dektak siuface profilometer was used to measure the etch rates. The profiles of the etched films were observed by field emission scanning electron microscopy (FESEM). In addition, x-ray photoelectron spectroscopy PCPS) was utilized to examine the existence of possible etch products or redeposited materials, and to elucidate the etch mechanism of Co2MnSi magnetic films in a CVOa/Ar plasma. 

For the native cement exposed first to water, there was a dramatic and rapid drop in microhardness, 30-40 % in the first hour, and 55-60 % at eight hours. Compressive strength was assumed to have undergone a similar decrease, since it is linearly related to microhardness for cementitious materials (Beaudoin Feldman, 1975). Scanning electron microscopy revealed clearly the differences that occurred on soaking in water. 

A number of techniques have been employed that are capable of giving information about amorphous phases. These include infrared spectroscopy, especially the use of the attenuated total reflection (ATR) or Fourier transform (FT) techniques. They also include electron probe microanalysis, scanning electron microscopy, and nuclear magnetic resonance (NMR) spectroscopy. Nor are wet chemical methods to be neglected for they, too, form part of the armoury of methods that have been used to elucidate the chemistry and microstructure of these materials. 

Analytical studies, using scanning electron microscopy and electron microprobe techniques (see Textbox 10), revealed that the mixture used for making this particular type of ceramic material consists mainly of clay, comminuted... 

Hill, A. D., A. H. Lehman, H. Arm, and M. L. Parr (2007), Using scanning electron microscopy with energy dispersive x-ray spectroscopy to analyze archaeological materials, J. Chem. Educ. 84(5), 810-813. 

As follows from the data of scanning electron microscopy, the mean size of particles is at around 2-5 pm. The specific surface area of the amorphous material is of two orders of magnitude greater than that of... 

It is now possible to observe nanometer features on the surfaces of zeolitic materials using high-resolution scanning electron microscopy. By taking ibidem measurements in combination with atomic force microscopy we are able to illustrate the strengths and weaknesses of both techniques and judge respective resolving power. 

The structure and phase purity of the synthesized materials were determined by X-ray powder diffraction (XRD). The morphology was investigated by scanning electron microscopy (SEM). 

Lindner et al. carried out detailed studies on the use of the sol-gel procedure to obtain new materials as suitable matrices [45]. A co-condensation of Si(OR)4, Si(OR)3-spacer-Si(OR)3 and Si(OR)3-spacer-ligand resulted in new hybrid materials, the properties of which strongly depended upon the spacer and the ratio of the different components used. Most of these materials were characterised with IR, EXAFS, and EDX spectroscopy, scanning electron microscopy and solid state NMR spectroscopy. Solid state 31P NMR was used to quantify the mobility of the interphases the changes in line-... 

Scanning electron microscopy is commonly used to study the particle morphology of pharmaceutical materials. Its use is somewhat limited because the information obtained is visual and descriptive, but usually not quantitative. When the scanning electron microscope is used in conjunction with other techniques, however, it becomes a powerful characterization tool for pharmaceutical materials. 

Compression of pharmaceutical materials has also been investigated with scanning electron microscopy. Simple powder mixtures have been used to illustrate the processes that occur during compression [68], The excipients chosen... 

Goldstein JI. Scanning Electron Microscopy and X-ray Microanalysis A Textfor Biologists, Material Scientists and Geologists, Plenum Press, New York, 1981. 

Thiel, B.L. (2004). Imaging and analysis in materials science by low vacuum scanning electron microscopy. International Materials Reviews 49 109-122. 

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