Nitrous acid ether spirit

UN 1194 (DOT) FEMA 2446 Synonyms Nitrosyl ethoxide Nitrous acid ethyl ester Nitrous ether Nitrous ethyl ether Spirit of ethyl nitrite... 

Incompat Acids, acid salts, spirit nitrous ether, alkaloids salts of lead, mercury, silver. 

Physical Parameters. It is a slightly bitter, ciystalline scales or powder. 1 g dissolves in 1300 ml cold water, 82 ml boiling water, 15 ml cold ethanol, 2.8 ml boiling ethanol, 14 ml chloroform, 90 ml ether, and soluble in glycerol. It gives a pasty mass with a salicylic acid, iodine, spirit nitrous ether, chloral hydrate, and phenol. 

Combustible when exposed to heat or flame can react with oxidizing materials. To fight fire, use water, CO2, dry chemical. Potentially explosive reaction with concentrated nitric acid. Incompatible with acetanilide, alkalies, ferric salts, spirit nitrous ether, urethan. When heated to decomposition it emits acrid smoke and irritating fumes. 

Prunes, dried Sherry wine Spirit of nitrous ether Tannic acid Vanilla... 

BENZENEDIOL (108-46-3) Combustible solid (flash point 261°F/127°C cc). Dust or powder forms explosive mixture with air. Violent reaction with strong oxidizers, nitric acid. Incompatible with acetanilide, alkalis, ammonia, amino compounds, antipyrine, camphor, ferric salts, lead diacetate, menthol, spirit nitrous ether, urethane. May accumulate static electrical charges, and may cause ignition of its dust. 

Incompat Acids, alkalies, alum, ammonia water, amyl nitrite benzoates betanaphthol, phenol, calomel, chloral hydrate, copper sulfate, ferric chloride ferrous sulfate chromium trioxide (chromic acid), cinchona alkaloids, hydrocyanic acid iodides iodine Lead subacetate mercuric chloride, orthoform potassium permanganate, resorcinol, sod. bicarbonate sod. salicylate (in powder) soln arsenic and mercury iodide, spirit nitrous ether (unless prescribed with sod, bicarbonate), syrup ferrous iodide, tartar emetic tannic acid, thymol, urethane, infusions of catechu, cinchona, rose leaves and uva ursi tinctures of catechu, ferric chloride, cinchona, hamanielis iodine, kino, and rhubarb. 

Brown or greenish-brown, irregular lumps, mp 85-90. In sol in water. Freely so] in alcohol, chloroform, ether, creosote, soln of chloral hydrate, alkalies slightly sol in benzene, carbon disulfide. Incompat Of Liquid preparations Mineral acids, acacia, ferric chloride, gold chloride, perman -ganates, spirit nitrous ether, water. LDn orally in rats > 5000 mg/kg (Jenner). 

Incompot (of all salts of morphine) Alkalies, tannic acid, iodic add, potassium permanganate, borax, chlorates, ferric chloride, iodides, lead acetate, magnesia, spirit nitrous ether, mercury bichloride, gold salts. 

Salicylic acid or its salts are colored reddish even by merest traces of ferric salts. Incompaf Iron salts, spirit nitrous ether, lead acetate, iodine. 

Incompot Ferric salts, lime water, spirit nitrous ether, mineral acids, iodine, lead acetate, silver nitrate, sodium phosphate in powder. 

Spirit of glyceryl trinitrate. See Nitroglycerin Spirit of Hartshorn. See Ammonium hydroxide Spirit of nitrous ether. See Ethyl nitrite Spirit orange. See Solvent yellow 14 Spirits of salt. See Hydrochloric acid Spirits of turpentine. See Turpentine Spirits of wine. See Alcohol Spirit of trinitroglycerin. See Nitroglycerin Spirit of turpentine. See Turpentine Spiro (benzofuran-2(3H), 1 -(2) cyclohexene)-3,4 -dione, 7-chloro-2, 4,6-trimethoxy-6 -p-methyl-. See Griseofulvin Spiro [bicycio [3.1.1] heptane-2,2 -oxirane], 6,6-dimethyl-. See Epoxypinane Spiro [1,3-dioxane-5,2 (2H)-napthalene], hexahydro-2,5, 5 -trimethyl-. See Dimethyl hexahydronaphthyl dihydroxymethyl acetal Spirofior. See 3-Ethyl-2,4-dioxaspiro (5.5) undec-8-ene... 

Ethyl nitrite, CgHgOgN, Mol. Wt. 75 07. This is contained in the B.P.C. preparation of Spirit of Nitrous Ether, which is an alcoholic solution containing ethyl nitrite together with decomposition products such as acetaldehyde, nitrous, nitric and acetic acids. If possible, original bottles filled to the neck should be used for analysis as the decomposition is fairly rapid in less favourable conditions of storage, especially with free access of air such as would be occasioned by the repeated opening of a bottle to extract portions. 

Mix 15 ml of a saturated aqueous solution of potassium chlorate with 5 ml of dilute nitric acid in a 100-ml graduated flask and weigh. Add 10 ml of the spirit of nitrous ether from a pipette, shake and reweigh. Set aside in a moderately warm place for one hour and shake occasionally. Then add 20 ml of 0-1N silver nitrate, shake well and make up to volume with water. Filter, rejecting the first 20 ml of filtrate. To 50 ml of the remainder add 10 drops of iron alum solution and titrate the excess of silver nitrate with O IN potassium thiocyanate. 1 ml 0 1N AgNOa = 0 0225 g ethyl nitrite. 

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