Nitrogen blanketing system

All safety equipment and systems should be scheduled for regular inspection and test. Nitrogen blanketing systems should be inspected at least weekly. It is not sufficient to check that the nitrogen is open to the tank. The atmosphere in the tank should be tested with a portable oxygen analyzer to make sure that the oxygen concentration is below 5%. 

Communication was poor in this instance. There was no reason to tie down this conservation lid as this 100-ft (30 m) diameter tank was out of service, empty, and blinded on all process tines. Operations left the nitrogen blanketing system in service with the normal setting of about 0.5 oz/in2 gage (22 Pa). The remote shipping tank remained in that condition for several weeks. 

The RO product water tank system shown in Figure 4.9 has a capacity of 76 m. The tank is3.7mD X 7.3m SSH FRP, flat-bottom, dome-top with 50 cm man-ways in the top dome and the side shell. It is provided with side-mounted level switches and a level transmitter, a pressure rehef valve/vacuum breaker, a nitrogen blanketing system, and a HEPA filter. 

As an example, a t5q>ical basket centrifuge installation requiring a nitrogen blanketing system would need the following alarms and shutdowns ... 

Boilers should be effectively sealed and all connections blanked off to prevent air in-leakage. A nitrogen blanket is then provided to cap the system and its auxiliaries. 

The exclusion of asphaltenes as a function of temperature subsequently was approached with the aid of gel permeation chromoto-graphy (GPC) in a manner similar to that described by Drushel. Catalyst was equilibrated 4 hour at constant temperatures with a volume of resid equal to 3 times the pore volume of the catalyst. During this time, the system was nitrogen blanketed and agitated every 1/2 hour. The external liquid subsequently was drained through a screen and submitted for GPC analyses and metals content. The internal liquid was extracted from the catalyst pores first by benzene and then 50/50 methanol-benzene. After evaporation of these solvents, the internal liquid was submitted for identical analyses ... 

Nitrogen is often used to blanket prepolymers and curatives after the container has been partially used. The blanketing system, if left in place permanently, must be so engineered that the container cannot build up a level of pressure in it that renders the situation unsafe. 

The tar used for this study was obtained from a series of BSR runs. The liquids were dissolved in acetone to filter off carried-over char fines. Acetone was stripped off in a one-plate distillation system. The analyses of this mixture of BSR tar are given in Table IV. The feed was stored at — 30°C, under a nitrogen blanket to minimize degradation. 

An Electrocure radiation curing unit could cost up to 400,000 or a capital expenditure cost of 20/hr. Radiation curable systems also require more maintenance and an inert atmosphere (nitrogen blanket) to ensure efficient curing operations. 

Figure 15. Nitrogen-gas sparger and blanketing system for loading tank cars and trucks (a) inline sparger and (b) complete system.

Instrumental. The Mettler TA2000B thermal analysis system is equipped with an interface system, and Hewlett-Packard 9815 desk top calculator and 7225 plotter. Samples, weighing 5-10 mg, sealed in aluminum pans and under a nitrogen blanket, were heated in the calorimeter at a rate of 10 deg/min from -35 or 10 deg C to 180 deg C respectively, for specific heat and kinetic scans. Specific heat measurements were calibrated with alumina to an accuracy of 3%. Temperatures and enthalpies were calibrated with an Indium sample. The accuracies were .02 deg C and 2% (Indium 28.5 J/g), respectively. 

Nylon RIM systems are also nitrogen-blown but control of nitrogen content is provided by setting the pressure of the nitrogen blanket used to inert the material hold tanks. Nitrogen is quite soluble in the caprolactam monomer and so no frothing is required. 

To produce solid parts, the nitrogen blanketing on the tanks is kept at as low a pressure as possible and no foam stabilizer is used in the formulation. Some machines which require high tank pressures to fill pumping pistons or to avoid cavitation at gear pump inlets may require the operator to periodically degas the system to avoid bubbles in the parts. 

Ethylene was polymerized [A. Schindler, J. Polym. Sci Part C, 4, 81 (1963)] in n-heptane with a catalyst system consisting of diisobutylaluminum hydride (1.5 mmol/L) and titanium tetrachloride (2.5 mmol/L). The catalyst components were reacted at these concentrations at 0°C and the mixture was then aged under a nitrogen blanket for 15 min. Ethylene was fed at 770 mm Hg pressure and the temperature of the catalyst suspension maintained at 40°C. It was found that the experimental data for the rate of polymerization could be represented best by assuming a mixed first and second-order dependence of the form... 

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