Drying, intermittent

The landward marching computation of the present time-averaged model ends at the cross-shore location x = Xm where the mean water depth h is less than 1 cm. The probabilistic model by Kobayashi et could be used to predict the irregular wave runup distribution but no reliable data exists for suspended sand and bedload transport rates in the zone which is wet and dry intermittently. Consequently, the following simple procedure is adopted to deal with the zone with the bottom slope Sb > tan. The cross-shore total sediment transport rate = ( sx + 96x) at ic = Xm is denoted by q m- If 9xm is negative (offshore), qx is extrapolated linearly to estimate qx on the scarped face with Sb > tan ... 

Place 50 g. of anhydrous calcium chloride and 260 g. (323 ml.) of rectified spirit (95 per cent, ethyl alcohol) in a 1-litre narrow neck bottle, and cool the mixture to 8° or below by immersion in ice water. Introduce slowly 125 g. (155 ml.) of freshly distilled acetaldehyde, b.p. 20-22° (Section 111,65) down the sides of the bottle so that it forms a layer on the alcoholic solution. Close the bottle with a tightly fitting cork and shake vigorously for 3-4 minutes a considerable rise in temperature occurs so that the stopper must be held well down to prevent the volatilisation of the acetaldehyde. Allow the stoppered bottle to stand for 24-30 hours with intermittent shaking. (After 1-2 hours the mixture separates into two layers.) Separate the upper layer ca. 320 g.) and wash it three times with 80 ml. portions of water. Dry for several hours over 6 g. of anhydrous potassium carbonate and fractionate with an efficient column (compare Section 11,17). Collect the fraction, b.p. 101-104°, as pure acetal. The yield is 200 g. 

It may be mentioned that diazonium fluoborates containing the nitro group usually decompose suddenly and with violence upon heating, hence if o- or p-fluonitrobenzene are required, the fluoborates (in 10-20 g. quantities) should he mixed with 3-4 times their weight of pure dry sand (or barium sulphate or sodium fluoride) and heated cautiously until decomposition commences intermittent heating will be required to complete the reaction. 

A pressure filter is a plate-and-frame press which operates on an intermittent time cycle. Drier cakes are generally attainable from a filter press. Sludge drying beds are usually used for smaller sludge volumes, which drain and dry rapidly. Thein appHcation is usually restricted to the more arid climates. 

Porous bron2e and iron, a variety of plastics, carbon—graphite, wood, and mbber are widely used in dry sliding or under conditions of sparse lubrication. These materials have commonly allowed design simplifications, freedom from regular maintenance, reduced sensitivity to contamination, and good performance at low speeds and with intermittent lubrication. Although these materials are often used dry or with sparse lubrication, performance normally improves the closer the approach to full-film lubrication. 

Otner Collectors Tarry particulates and other difficult-to-handle hquids have been collected on a dry, expendable phenol formaldehyde-bonded glass-fiber mat (Goldfield, J. Air Pollut. Control A.SSOC., 20, 466 (1970)] in roll form which is advanced intermittently into a filter frame. Superficial gas velocities are 2.5 to 3.5 m/s (8.2 to 11.5 ft/s), and pressure drop is typically 41 to 46 cm (16 to 18 in) of water. CoUection efficiencies of 99 percent have been obtained on submicrometer particles. Brady [Chem. Eng. Prog., 73(8), 45 (1977)] has discussed a cleanable modification of this approach in which the gas is passed through a reticulated foam filter that is slowly rotated and solvent-cleaned. 

Automatic filters are made with either viscous-coated or dry filter media. However, the cleaning or disposal of the loaded medium is essentially continuous and automatic. In most such devices the air passes horizontally through a movable filter curtain. As the filter loads with dust, the curtain is continuously or intermittently advanced to expose clean media to the air flow and to clean or dispose of the loaded medium. Movement of the curtain can be provided by a hand crank or a motor drive. Movement of a motor-driven curtain can be actuated automatically by a differential-pressure switch connected across the filter. 

Resiheut, compressible and strong, but not impermeable. Resists medium-strength mineral acids and dilute mineral solutions if not intermittently dried. Resists oils, greases, waxes, most solvents. Damaged by alkahes. 

Phenylphosphinic acid [benzenephosphinic acid, PhPH(0)(OH)] [1779-48-2] M 142.1, m 70", 71", 83-85", 86", pK 1,75. Cryst from H2O (sol 7.7% at 25°). Purified by placing the solid in a flask covered with dry Et20, and allowed to stand for 1 day with intermittent shaking. Et20 was deeanted off and the proeess repeated. After filtration, excess Et20 was removed in vacuum. [Justus Liebigs Ann Chem 181 265 1876 Anal Chem 29 109 1957 NMR J Am Chem Soc 78 5715 1956.]... 

The flask is then fitted for steam distillation, and 700-800 ml. of distillate is collected. After addition of 55 g. of sodium chloride to the distillate, the phases are separated in a 1-1. separatory funnel. The organic layer is dried by intermittent stirring with 25 g. of anhydrous magnesium sulfate for 6-10 hours. 

Another advantage is that wet ESPs can collect sticky particles and mists, as well as highly resistive or explosive dusts. The continuous or intermittent washing with a liquid eliminates the reentrainment of particles due to rapping which dry ESPs are subject to. The humid atmosphere that results from the washing in a wet ESP enables them to collect high resistivity particles, absorb gases or cause pollutants to condense, and cools and conditions the gas stream. Liquid particles or aerosols... 

A calibration curve for the range 0.2-10 mg fluoride ion per 100 mL is constructed as follows. Add the appropriate amount of standard sodium fluoride solution, 25 mL of 2-methoxyethanol, and 10 mg of a buffer [0.1 Af in both sodium acetate and acetic (ethanoic) acid] to a 100 mL graduated flask. Dilute to volume with distilled water and add about 0.05 g of thorium chloranilate. Shake the flask intermittently for 30 minutes (the reaction in the presence of 2-methoxyethanol is about 90 per cent complete after 30 minutes and almost complete after 1 hour) and filter about 10 mL of the solution through a dry Whatman No. 42 filter paper. Measure the absorbance of the filtrate in a 1 cm cell at 540 nm (yellow-green filter) against a blank, prepared in the same manner, using a suitable spectrophotometer. Prepare a calibration curve for the concentration range 0.0-0.2 mg fluoride ion per 100 mL in the same way, but add only 10.0 mL of 2-methoxyethanol measure the absorbance of the filtrate in a 1 cm silica cell at 330 nm. 

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