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Direct water removal

For mixture.s the picture is different. Unless the mixture is to be examined by MS/MS methods, usually it will be necessary to separate it into its individual components. This separation is most often done by gas or liquid chromatography. In the latter, small quantities of emerging mixture components dissolved in elution solvent would be laborious to deal with if each component had to be first isolated by evaporation of solvent before its introduction into the mass spectrometer. In such circumstances, the direct introduction, removal of solvent, and ionization provided by electrospray is a boon and puts LC/MS on a level with GC/MS for mixture analysis. Further, GC is normally concerned with volatile, relatively low-molecular-weight compounds and is of little or no use for the many polar, water soluble, high-molecular-mass substances such as the peptides, proteins, carbohydrates, nucleotides, and similar substances found in biological systems. LC/MS with an electrospray interface is frequently used in biochemical research and medical analysis. [Pg.59]

Sephadex. Other carbohydrate matrices such as Sephadex (based on dextran) have more uniform particle sizes. Their advantages over the celluloses include faster and more reproducible flow rates and they can be used directly without removal of fines . Sephadex, which can also be obtained in a variety of ion-exchange forms (see Table 15) consists of beads of a cross-linked dextran gel which swells in water and aqueous salt solutions. The smaller the bead size, the higher the resolution that is possible but the slower the flow rate. Typical applications of Sephadex gels are the fractionation of mixtures of polypeptides, proteins, nucleic acids, polysaccharides and for desalting solutions. [Pg.23]

The Secondary LOCA sequences are related to large breaks (23/24) with small breaks and expansion joint (< 1%). Response to Secondary LOCA involves shutdown, leak control and/or isolation, water removal from the building to avoid flooding of pumps, and direct core cooling in the event of pump flooding. [Pg.421]

Commercial laundry dryers can not be easily vented to the outside in the same way that home laundry dryers are. Because of this fact, the moist air is passed through a condenser where the water will accumulate. If there is no direct water drain, the water is directed to a holding tank. The water level is monitored using a magnetic float. When the water rises to the full level, the reed sensor is activated and shuts down the dryer. Once the water is removed, the reed sensor is deactivated, enabling the dryer to operate. [Pg.135]

Evacuate danger area immediately Consult an expert Ventilation. Absorb remaining liquid in sand or inert absorbent and remove to safe place. Do NOT wash away into sewer. NEVER direct water jet on liquid. Prevent from entering confined spaces. Do NOT let this chemical enter the environment (extra personal protection gas-tight chemical protection suit including self-contained breathing apparatus). [Pg.348]

Flushing involves kneading the aqueous pigment presscake with varnish until a complete exchange has taken place between the two liquid phases. The aqueous phase is then separated and residual water removed by vacuum distillation at elevated temperature. Flushing affords a product which can be incorporated directly into a printing ink (Sec. 1.6.5.8). [Pg.544]

The use of slowly rotating rakes is beneficial in large thickeners to direct the underflow to the central outlet at the bottom of the tank. At the same time the slow motion of the rakes tends to give a gentle agitation to the sediment which facilitates its consolidation and water removal. The height requirement of the rakes must be added to that needed for the thickening zone to achieve the desired underflow concentration. [Pg.264]

Direct esterification of PHBA monomer is problematic because the rate of decarboxylation is often comparable to the rate of (co)poly-merlzation (15,16). The problem seems largely overcome by two process refinements introduced here [1] Use of p-TSA apparently catalyzes esterification and more than it catalyzes formation of the undesirable by-product, phenol. [2] "Aromatic 150" solvent helps maintain constant reaction temperature and facilitates water removal. Refluxing solvent also prevents accumulation of sublimed PHBA in the upper parts of the reactor. [Pg.345]

Precipltatora/fllterm. In the past, it was common to direct water to be treated through a bed of excelsior or a similar medium to aid coalescence of oil droplets (Fig. 6). However, the coalescing medium has a tendency to dog, and many of these devices in oil field service have had the medium removed. In such a case, these units act like vertical skimmers since oil droplets must flow counter-current to the downward flow of water through the area formerly occupied by the medium. [Pg.173]

Alternatively, the reduction may be carried out by adding the chromium (VI) compound to a mixture of 420ml of water and 80ml of concentrated hydrochloric acid and then adding S5ml of ethyl alcohol. The reduced solution is boiled as directed to remove excess alcohol and acetaldehyde (oxidation product). Either reduction procedure should be carried out in a hood. [Pg.82]

The content of resinous substances may also be determined directly by saponifying 50-100 grams of the oil with alcoholic potash in the usual way (Vol. I, p. 373), diluting with water, removing the alkaline aqueous liquid, washing the oil remaining unattacked well with hot water and weighing it by difference the content of resinous substances is determined. [Pg.310]

Processing, 84,(9), 99-106 (2005)]. This article cites downward gas velocities in the range of 10 to 37 m/s and notes gas pressure drop in the range of 6 to 20 in of water. Removals of S02 and fine particles were both close to 99 percent. The froth produced by the contactor reverses direction, flows down, and is largely disengaged in a vessel mounted below. [Pg.91]


See other pages where Direct water removal is mentioned: [Pg.31]    [Pg.433]    [Pg.31]    [Pg.433]    [Pg.386]    [Pg.322]    [Pg.454]    [Pg.474]    [Pg.1547]    [Pg.45]    [Pg.421]    [Pg.64]    [Pg.65]    [Pg.1176]    [Pg.399]    [Pg.402]    [Pg.581]    [Pg.45]    [Pg.12]    [Pg.176]    [Pg.219]    [Pg.73]    [Pg.338]    [Pg.85]    [Pg.188]    [Pg.28]    [Pg.718]    [Pg.884]    [Pg.503]    [Pg.374]    [Pg.29]    [Pg.683]    [Pg.1206]    [Pg.574]    [Pg.113]    [Pg.127]    [Pg.150]    [Pg.671]    [Pg.380]   
See also in sourсe #XX -- [ Pg.202 ]




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