Analyzer installation

Necessary roles Necessary roles in process analytics implementation can be filled by personnel from different departments, depending on the organizational setnp of the company and the complexity of the analyzer installation. A list of required expertise/necessary roles includes ... 

For the measurement of a single chemical entity, analyzers in the form of NDIR analyzers have been in use for decades for both industrial and environmental monitoring applications. These featnre one or more wavelength specific devices, usually optical filters, customized for the specific analyte, snch as CO, CO2, hydrocarbons, moisture, etc. This type of instrument is normally inexpensive (on average around 5000) and relatively easy to service, dependent on its design. This class of instrument is by far the most popular if one reviews the instrumentation market in terms of nsage and the number of analyzers installed. 

One aspect that has limited the use and introduction of process analyzers, and in particular FTIR analyzers, has been the high cost of the analyzer, and the resultant high cost per analysis point. Many process analyzer installations are financially evaluated in terms of cost per analysis or analysis point, as well as cost of ownership and the rate of payback. Typically, these costs need to be kept as low as possible... 

Occasionally attempts to justify a process analyzer are made on the basis that it will reduce the number of grab samples that need to be taken from the process to be analyzed, and therefore reduce the sample load on the QC lab. This is not usually a good justification for an on-line analyzer for two reasons (1) The reduction in lab analyses rarely offsets the cost of analyzer installation and operation (2) An on-line analyzer relies on high quality lab data for calibration, validation, and long-term model maintenance, so the reference method can never be eliminated entirely. 

The injection point of the sulfuric acid is in the pump bay, or as near as possible to water intake. The sulfuric acid pump is normally a motor-driven proportioning pump, and an electric motor is connected to a pH analyzer installed on the cooling water supply header so that the pump starts and stops, depending on the pH in the circulating water. Table 8.2 summarizes various chemical treating agents for cooling water towers. 

Dead time. Probably the best example of a measurement device that exhibits pure dead time (time delay) is the chromatograph, because the analysis is not available for some time after a sample is injected. Additional dead time results from the transportation lag within the sample system. Even continuous analyzer installations can exhibit dead time from the sample system. 

Replace, upgrade, or remove analyzers All the analyzer installations should be periodically reviewed for its operability and cost effectiveness. This should be performed with the production personnel to determine if the analyzer needs to be replaced, upgraded, or removed if it no longer serves the purpose. 

In a protocol analyzer installed on the transmitter equipment, the total time for the transference was analyzed for the transmission path between the hosts. The total bit length was also measured and the throughput was calculated, in Mbps, with the scenarios described before. The obtained throughput is compared with the base scenario and the noise effect over the channel is obtained. 

All platform production facilities must be protected with a safety system designed, analyzed, installed, tested and maintained in operating condition in accordance with API RP 14C— Safety Analysis for Production Platforms. ... 

As mentioned earlier, there are several basic types of environment in which most process analyzer installations will take place. In order to address these requirements, different levels of enclosure design and control of the internal instrument environment are required. In the subsequent subsection, these issues will be addressed. 

The calibration protocol outlined in Section II.G.4, is valid in both the laboratory and in the process environment, at least upon initial process analyzer installation. Once installed, however, the probe head is relatively inaccessible, at least for frequent checks or recalibrations. Pixel phase-stepping approaches as proposed by Mann and Vickers [227] for use in the laboratory for improved wavelength accuracy are time-consuming, costly, and add moving parts to a process analyzer system [126]. With this in mind, it is necessary to address the subject of Raman analyzer calibration from the point of view of the industrial process environment. This necessarily involves compromises with respect to the ideal calibration methods discussed previously [126,191,265]. There are several levels of compromises that can be considered, each of which involves a different level of cost, complexity, and accuracy. Ultimately, the intended process application and its associated accuracy requirements must determine the calibration approach selected. 

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