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Analysis of oligosaccharides

The application of ESI-MS/MS allows the identification and quantification of individual oligosaccharides for the diagnosis of glycoproteinoses (oligosaccharidurias) [Pg.257]

Suzuki-Sawada, J., Umeda, Y., Kondo, A., and Kato, I., Analysis of oligosaccharides by on-line high-performance liquid chromatography and ion-spray spectrometry, Anal. Biochem., 207, 203, 1992. [Pg.283]

Recent Developments in the Use of 13C-N.m.r. Spectroscopy for the Structural Analysis of Oligosaccharides of Glycoproteins... [Pg.8]

Dell, A., Morris, H.R., Easton, R., Haslam, S.M., Panico, M., Sutton-Smith, M., Reason, A.J. and Khoo, K.-H. (1999b) Structural analysis of oligosaccharides FAB-MS, ES-MS and MALDI-MS. In Ernst, B., Sinay, P. and Hart, G. (eds) Oligosaccharides in Chemistry and Biology - a Comprehensive Handbook. Wiley-VCH, Weinheim (in press). [Pg.310]

N.m.r. spectroscopy T.l.c.-m.s. analysis of oligosaccharides coupled to a lipid amine (neoglycolipids) H n.m.r. spectrum in D20 after exchange of free protons with deuterium Experiments conducted at 295 K, with acetone as the internal standard (set at 2.225 p.p.m. from 4,4-dimethyl-4-silapentane-1-sulfonate) Results compared, to within 0.005 p.p.m. (laboratory-to-la-boratory variation) of data in the literature Conformational studies by n.O.e. experiments Natural-abundance-13C analysis Chemical-shift assignment by 2D H- H and H-13C n.m.r. spectroscopy... [Pg.312]

Conformational analysis of oligosaccharides in solution by NMR is mainly based on hydrogen-hydrogen distance information obtained from the nuclear Overhauser effect (n.O.e.) ( ). Other independent NMR... [Pg.162]

Conformational Analysis of Oligosaccharides Reconciliation of Theory with Elxperiment J. P. Carvers D. MandeP, S. W. MichnickS A. Imberfy S and J. W. Brady ... [Pg.266]

Schmid, D., Behnke, B., Metzger, J., and Kuhn, R., Nano-HPLC-mass spectrometry and MEKC for the analysis of oligosaccharides from human milk, Biomedical Chromatography 16(2), 151-156, 2002. [Pg.97]

Schroeder, H. and Haslinger, E., Sequential analysis of oligosaccharide structures by selective NMR techniques. Part II. ID multistep-relayed C0SY-R0ESY, Liebigs Ann. Chem., 1, 751, 1993. [Pg.123]

Peelen GO, de Jong JG, Wevers RA (1994) HPLC analysis of oligosaccharides in urine from oligosaccharidosis patients. Clin Chem 40 914-921... [Pg.332]

Improved methods for the analysis of oligosaccharide and polysaccharide structure have revealed remarkable complexity and diversity in the oligosaccharides of glycoproteins and glycolipids. Consider the oligosaccharide chains in Figure 7-31, typical of those... [Pg.261]

However, the data available suggest that the results obtainable from mass spectrometry will considerably facilitate the structural analysis of oligosaccharides and thus permit direct investigation of the products of partial hydrolysis of polysaccharides on the oligomer level. [Pg.93]

Some important contributions to the conformational analysis of oligosaccharides have come from the determination of the structure of oligosaccharides which form complexes with protein. In this context the complex of lysozyme with chitohexaose [40] and the phosphorylase complex with maltoheptaose [41, 42] and maltopentaose [43] have been resolved to atomic resolution. [Pg.147]

Trihydroxyacetophenone (THAP) THAP can be used for the analysis of oligosaccharides and can offer improved sensitivity for detection of acidic glycopeptides over HCCA.37 Ionization with THAP can be improved with the addition of di-ammonium hydrogencitrate to limit cation adduction... [Pg.67]

C. S. Creaser, J. C. Reynolds, and D. J. Harvey, Structural analysis of oligosaccharides by atmospheric pressure matrix-assisted laser desorption/ionisation quadrupole ion trap mass spectrometry, Rapid Commun. Mass Spectrom., 16 (2002) 176-194. [Pg.129]

M. Li and J. A. Kinzer, Structural analysis of oligosaccharides by a combination of electrospray mass spectrometry and bromine isotope tagging of reducing-end sugars with 2-amino-5-bromopyridine, Rapid Commun. Mass Spectrom., 17 (2003) 1462-1466. [Pg.132]

See other pages where Analysis of oligosaccharides is mentioned: [Pg.546]    [Pg.18]    [Pg.11]    [Pg.656]    [Pg.1]    [Pg.313]    [Pg.195]    [Pg.379]    [Pg.64]    [Pg.329]    [Pg.164]    [Pg.169]    [Pg.175]    [Pg.269]    [Pg.275]    [Pg.279]    [Pg.144]    [Pg.169]    [Pg.93]    [Pg.142]    [Pg.290]    [Pg.98]    [Pg.121]    [Pg.26]    [Pg.236]    [Pg.16]   
See also in sourсe #XX -- [ Pg.257 ]



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