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Ammonia aqueous solution

Reaction of Acetoin (3-Hydroxy-2-butanone) with Ammonia. Aqueous solution of ammonium hydroxyde (20%, 100 ml) was added to acetoin (17.6 g, 0.2 mol) and the reaction mixture was stirred for 30 min at 50°C and then for 6 h at room temperature. The precipitated product was filtered off, the filtrate was neutralized with 10% hydrochloric acid, and extracted with ether (continuous overnight extraction). The extract was washed with water, dried over anhydrous sodium sulfate, and concentrated on a spinning-band distillation apparatus. The residual solution was then analyzed by GC and GC-MS. [Pg.37]

Ammonia aqueous solution (35% v/v). Widely available chemical. Used to introduce free amino groups in the epoxy-activated beads, which can be quantified by the 2,4,6-trinitrobenzenesulphonic acid (TNBS) test (see Note 3). Hazards Poison,... [Pg.45]

Perez et al. reported the bio-active monodisperse, water-soluble, and highly crystalline dextran-coated ceria NPs with pH dependent antioxidant activity, which are made through room temperature hydrolysis in ammonia aqueous solution in the presence of dextran T-10 (Perez et al., 2008). The obtained water soluble NPs contained a ratio of Ce " "/Ce + approximately 3/2, which became 2/3 after adding some H2O2. Later, the NPs could regenerate the original ratio 10 days under pH 7.4 while there is no regeneration under pH 4. [Pg.308]

Ammonia aqueous solution 10 H II. . . 2.5 TOSfiiBiiiliAftiii Nippon Goh. Soarnol... [Pg.435]

TRIMETHOXY SILANE (2487-90-3) Forms explosive mixture with air (flash point 45°F/7°C). Violent reaction with water, steam, alcohols, forming highly corrosive material. Heat, peroxides, or other catalysts may cause explosive polymerization. Violent reaction with strong oxidizers, metallic hexafluorides, ammonia. Aqueous solution incompatible with alkalis, aliphatic amines, alkanolamines, isocyanates, alkylene oxides, epichlorohydrin, halo-genated compounds, nitrogen oxides. Corrodes common metals in the presence of moisture. [Pg.1197]

Dicyanodiamide melts at 209.5° (corr.) and can be crystallized in the form of rhombic plates from water, alcohol, or a mixture of the two. It is only slightly soluble in water, moderately soluble in alcohol and in liquid ammonia. Aqueous solutions are neutral, but liquid ammonia solutions are acidic in character, and react with metallic oxides and amides to form well-defined salts. ... [Pg.44]

Lu et al. [31] synthesized alumina nanotubes via the hydrothermal technique. For a typical synthesis, AKNOsjs and camphor sulfonic acid, as surfactant, were dissolved in water. An ammonia aqueous solution was added to adjust the pH value to 5.4. A Teflon-lined stainless steel autoclave heated to 160 °C was used to grow the nanotubes for 24 h. A solid precipitate was collected by centrifugation, washed with ethanol and dried in air at room temperature followed by grinding. The product of this synthesis exhibits a one-dimensional morphology with a length of 500 nm and a diameter of 50 nm, and a boehmite phase. [Pg.66]

Hollow siUca nanoparticles can be synthesized under moderate conditions using luminescent CdSe/ZnS nanoparticles, as described by Darbandi et al. [9]. The synthesis is conducted at room temperature within reverse micelles and by way of a modified water-in-oil microemulsion system, where silica is formed from the hydrolysis of TEOS. Here, the silica acts as a host for the CdSe/ZnS nanoparticles while the latter is simultaneously dissolved. The extent of this dissolution is determined by the amount of ammonia aqueous solution used and the reaction time. In a typical synthesis, cyclohexane is added to polyethylene glycol nonylphenyl ether (the surfactant), pre-prepared luminescent CdSe/ZnS nanopartides in chloroform, and TEOS, and the mixture then stirred vigorously to form the microemulsion. After 30 min, aqueous ammonia is added to initiate the encapsulation, and the reaction is then left overnight at room temperature before the nanopartides are precipitated. By increasing the amount of ammonia used, the core particles become increasingly dissolved to the point where hollow spheres can be obtained (250 (xl ammonia solution). Similarly, an increase in the duration of the reaction will yield nanopartides with increasingly dissolved cores. [Pg.68]

Ammonia aqueous solution 10 20 7 9 0 95 Reny 1002 Mitsubishi Gas Chemical Filler 30% Glass fiber... [Pg.2471]

Ammonia aqueous solution 22 5 8 No effect Dylark 250P20 Arco Filler Specimen Medium heat grade... [Pg.3049]

Ammonia aqueous solution 25 20 0-365 9 Resistant for years Polystyrol 456M BASF Specimen Uncolored, unstressed... [Pg.3150]

Ammonia aqueous solution 10 6 No change in appearance 2.5 Soarnol Soarnol... [Pg.3346]

Ammonia aqueous solution 10 23 8 Recommen(de(d for use Halar Ausimont... [Pg.4]

Ammonia aqueous solution 20 30 8 Resistant mechanical properties are not appreciably affected Hostalen GUR Hoechst Celanese Specimen Dumbell type test specimen... [Pg.474]


See other pages where Ammonia aqueous solution is mentioned: [Pg.520]    [Pg.376]    [Pg.30]    [Pg.138]    [Pg.30]    [Pg.444]    [Pg.218]    [Pg.1049]    [Pg.45]    [Pg.971]    [Pg.27]    [Pg.98]    [Pg.284]    [Pg.622]    [Pg.125]    [Pg.18]    [Pg.185]   
See also in sourсe #XX -- [ Pg.189 ]




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Aqueous Ammonia

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