Solid state nuclear magnetic resonance morphology

Samyn, F., Bourbigot, S., Jama, C., Bellayer, S., Nazare, S., Hull, R., Castrovinci, A., and Camino, G. (2008) Crossed characterisation of polymer-layered silicate (PLS) nanocomposite morphology TEM, x-ray diffraction, rheology and solid-state nuclear magnetic resonance measurements, European Polymer Journal 44(6) 1642-1653. 

Part A Molecular Structure and Dynamics, Academic Press, 1980 L. Marton, C. Marton (Ed.) Methods of Experimental Physics Vol.16, Polymers Part B Crystal Structure and Morphology, Academic Press, 1980 L. Marton, C. Marton (Ed.) Methods of Experimental Physics Vol.16, Polymers Part C Physical Properties, Academic Press, 1980 V. J. McBrierty, K. J. Packer Cambridge Solid State Science Series, Nuclear Magnetic Resonance in Solid Polymers, Cambridge University Press, 1993... 

Similar methods are available that are based on solid-state proton nuclear magnetic resonance spectroscopy. Proton methods are less discriminating than the equivalent carbon-13 method, being based on a two-phase model of semicrystalline morphology. In their favor, they are several orders of magnitude faster than the carbon-13 method and the equipment required is much cheaper. 

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