Optical analysis test

There is the microtoming optical analysis test. In this procedure thin slices (under 30 tixri) of the plastics are cut from the product at any level and microscopically examined under polarized light transmitted through the sample. Rapid quality and failure analysis examination occurs by this technique. This technique has been used for many years in biological studies and by metallurgists to determine flaws, physical and mechanical properties. Examination can be related to stress patterns, mechanical properties, etc. 

C.A. Martin, Evaluating the utility of fiber optic analysis for dissolution testing of drug products, Dissol. TechnoL, 10(4), 37-39 (2003). 

Use Analysis (testing for ozone), artificial gem, optical glass of high refractive index. 

B.S. Zolnik, J.-L. Raton, D.J. Burgess, Application of USP apparatus 4 and in situ fiber optic analysis to microsphere release testing. Dissolution Technol. 12 (2) (2005) 4. 

Part 305. Optical laboratory test methods for electronic visual displays Part 306. Field assessment methods for electronic visual displays Part 307. Analysis and compliance test methods for electronic visual displays... 

These tests generate several Gigabytes of data that are fed into a historical database. Although most of the analysis is performed automatically, human interaction is still needed to compare current and past data. Data are stored on optical CD S s from which the historical data bank are retrieved during field inspections from a mobile unit. Each of these is equipped with a CD-jukebox linked to an analysis station. The jukebox can handle 100 CD s, enough to store all previously recorded data. A dedicated software pre-fetches the historical data and compares it on-line with the newly acquired NDT-data. It is based on fuzzy algorithms applied to signal features. 

Physical testing appHcations and methods for fibrous materials are reviewed in the Hterature (101—103) and are generally appHcable to polyester fibers. Microscopic analyses by optical or scanning electron microscopy are useful for evaluating fiber parameters including size, shape, uniformity, and surface characteristics. Computerized image analysis is often used to quantify and evaluate these parameters for quaUty control. 

The analysis of siUcon carbide involves identification, chemical analysis, and physical testing. For identification, x-ray diffraction, optical microscopy, and electron microscopy are used (136). Refinement of x-ray data by Rietveld analysis allows more precise deterrnination of polytype levels (137). 

This photoelastic stress analysis is a technique for the nondestructive determination of stress and strain components at any point in a stressed product by viewing a transparent plastic product. If not transparent, a plastic coating is used such as certain epoxy, polycarbonate, or acrylic plastics. This test method measures residual strains using an automated electro-optical system. 

An accurate determination of critical load Wcr is sometimes difficult. Several techniques, such as (1) microscopic observation (optical or SEM) during the test, (2) chemical analysis of the bottom of the scratch channel (with electron microprobes), and (3) acoustic emission, have been used to obtain the critical load. 

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