Help Routines

To set up the page layout for plotting spectra several tasks have to be performed. They include the definition of the plot region, of the spectrum components to be included in the plot (spectrum, integral, peak labels, axis, of the title, of the contents of the parameter table and any additional imported data to be added to the layout such as the formulae or molecular structure. To inspect the final layout prior to plotting. WIN-NMR offers the Preview option which shows an exact copy of your subsequent plot on the screen and allows you to perform final adjustments and rearrangements on the screen. 

Final processing and arranging the page layout may be performed in different ways. Using the appropriate quick-mode buttons is the easiest way, whereas the use of pulldown menus offers a wide variety of parameters which allow the various operations to be tailored to your specific needs. In addition, some of these operations may be performed in an automatic, but predefined way, which is ideal if a series of spectra are to be processed and plotted in the same way (see section 5.5). 

The ID WIN-NMR and the 2D WIN-NMR Help options will give you detailed information on a given topic as well as how to apply the corresponding processing options. ID WIN-NMR has seven and 2D WIN-NMR has ten main topics  

FID- and Spectrum Window Preview Window Relaxation Window Text Window Appendix 

General information Installation Buttons Panel File 

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Use of Vendors. During the validation phase of the study, vendors can be effectively employed. Often, vendors w ill provide quite detailed studies free of charge for goodwill or in hopes of a later sale. Contractors use vendor help routinely for process designs or studies. Credit is usually given in the contractor s presentation of results for any vendor participation. 

Software tools including manuals (HELP routines) describing in detail the use of ID WIN-NMR, 2D WIN-NMR and GETFILE supplied on CD-ROM. 

Processing of ID NMR Data HELP Routine Processing of 2D NMR Data HELP Routine... 

These three sections are combined in such a way that you may use all these educational tools interactively with your PC. In this way as you leam about the basics in theory, you directly apply what you have leamt in practice following the instructions given in the numerous Check its. You experience step by step the scope of the powerful software modules, their advantages and limitations and you acquire the necessary skills to become an expert in NMR data processing. It is essential at this stage to exploit and make use of the powerful HELP routines if necessary. In contrast to the introductory... 

HELP routines available with the WIN-NMR software modules give detailed... 

If you start the Help routine via Contents (ID WIN-NMR) or Help index (2D WIN-... 

If you start the Help routine in ID WIN-NMR via the cursor shape changes and you can directly select with this new mouse cursor the appropriate information about any entry in the pull-down menus, or any button or function key in the display button panel. 

Activate File Transfer and Filecopy Convert and inspect their dialog boxes. These two options have been discussed in detail in chapter 2. If necessary, use the Help routine to get more information about using these options. 

Consult the corresponding Help routine for more detailed information and for how to use these integral options. 

Use the Help routine of 2D WIN-NMR for detailed information about the various edit fields and buttons available in the Page Setup... dialog box if necessary. 

Two help routines are embedded in the system, one to provide on-line help in the use of the system, the other to provide an insight into the rationale behind adoption of the specific rules/formulae/... 

As with the system developed for tablet formulations, this system contains extensive Help routines. No formulation optimization routines are included, although a routine to develop a placebo formulation to match the active formulation is included. 

Elemental analysis also proved to be a helpful routine method for determining reaction progress and calculate resin loading, especially when bromine or fluorine tags are present. 

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