Cross-polarization magic angle spinning NMR

Lindberg, J. J. and Hortling, B. Cross Polarization — Magic Angle Spinning NMR Studies of Carbohydrates and Aromatic Polymers. Vol. 66, pp. 1—22. 

Cross Polarization — Magic Angle Spinning NMR Studies of Carbohydrates and Aromatic Polymers... 

Sherwin, C.P., Labuza, T.P., McCormick, A., and Chen, B. 2002. Cross-polarization/magic angle spinning NMR to study glucose mobility in a model intermediate-moisture foods system. J. Agric. Food Chem. 50, 7677-7683. 

Asakura, T., Kuzuhara, A., Tabeta, R., and Saito, H. (1985). Conformation characteriz-tion of Bombyx mod silk fibroin in the solid state by high-frequency 13C cross polarization-magic angle spinning NMR, x-ray diffraction, and infrared spectroscopy. Macromolecules 18, 1841-1845. 

Asakura, T., Ohgo, K., Ishida, T., Taddei, P., Monti, P., and Kishore, R. (2005). Possible implications of serine and tyrosine residues and intermolecular interactions on the appearance of silk I structure of Bombyx mod silk fibroin-derived synthetic peptides High-resolution 13C cross-polarization/magic-angle spinning NMR study. Biomacromolecules 6, 468-474. 

Figure 4. Carbon-13 cross-polarization, magic-angle spinning NMR spectra from an acrylic-melamine (A) and acrylic-urethane (B) coating. (Reproduced with permission from ref. 28. Copyright 1986 Elsevier Sequoia.)...

The use of cross-polarization/magic angle spinning NMR may well become the most powerful method to determine the structure of conjugated acid and bases in the solid state. 

Pfeffer, P. E., Hicks, K. B. and Earl, W. L. 1983. Solid state structures of keto-disacchar-ides as probed by 13C cross-polarization, magic angle spinning NMR spectroscopy. Carbohydr. Res. 11, 181-194. 

LeMay, J. D., Kelley, F. N. Structure and Ultimate Properties of Epoxy Resins. Vol. 78, pp. 113-148. Lindberg, J. J. and Hording, B. Cross Polarization — Magic Angle Spinning NMR Studies of Carbohydrates and Aromatic Polymers. Vol. 66, pp. 1-22. 

Cook, R., and Langford, C. (1999). Ramped amphtude cross polarization magic angle spinning NMR (Ramp-CP-MAS-NMR) A technique for quantitative study of the composition of solid state polymers. Polymer News 24, 6-15. 

CP-MAS cross-polarization magic-angle spinning (NMR spectroscopy)... 

Zumbulyadis N. 1983. Selective carbon excitation and the detection of spatial heterogeneity in cross-polarization magic-angle-spinning NMR. J. Magn. Reson. 59 486-494. 

Lindberg JJ, Hording B. 1985. Cross polarization-magic angle spinning NMR studies of carbohydrates and aromatic polymers. Adv. Polym. Sci. 66 1-22. 

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