Cross-flow system, direct membrane

The design of a cross-flow filter system employs an inertial filter principle that allows the permeate or filtrate to flow radially through the porous media at a relatively low face velocity compared to that of the mainstream slurry flow in the axial direction, as shown schematically in Figure 15.1.9 Particles entrained in the high-velocity axial flow field are prevented from entering the porous media by the ballistic effect of particle inertia. It has been suggested that submicron particles penetrate the filter medium and form a dynamic membrane or submicron layer, as shown in... 

The separation channel in asymmetrical flow FFF (AF4) is approximately 30 cm long, 2 cm wide, and between 100 and 500 pm thick. A carrier flow which forms a laminar flow profile streams through the channel. In contrast to the other FFF methods, there is no external force, but the carrier flow is split into two partial flows inside the channel. One partial flow is led to the channel outlet and, afterward, to the detection systems. The other partial flow, called the cross-flow, is pumped out of the channel through the bottom of the channel. In the AF4, the bottom of the separation channel is limited through a special membrane and the top is made of an impermeable plate (glass, stainless steel, etc.). The separation force, therefore, is generated internally, directly inside the channel, and not by an externally applied force. 

Two process modes, namely, dead-end and cross-flow modes, are widely used for microfiltration (14). For the dead-end mode, the entire solution is forced through the membrane. The substances to be separated are deposited on the membrane, which increases the hydraulic resistance of the deposit. The membrane needs to be renewed as soon as the filtrate flux no longer reaches the required minimum values at the maximum operation pressure. This mode is mostly used for slightly contaminated solutions, e.g., production of ultra-pure water. For the cross-flow mode, the solution flows across the membrane surface at a rate between 0.5 and 5.0 m/s, which prevents the formation of a cover layer on the membrane surface. A circulation pump produces the cross-flow velocity or the shear force needed to control the thickness of the cover layer. The system is most widely used for periodic back flushing, where part of the filtrate is forced in the opposite direction at certain intervals, and breaks up the cover layer. The normal operating pressure for this mode is 1-2 bars. 

A.2 Cross-Flow, Dead-End Configurations Microfiltration and UF systems are operated in two possible filtration modes. Figure 6.10 shows the cross-flow configuration in which the feed water is pumped tangential to the membrane. Clean water passes the membrane while the water that does not permeate is recirculated as concentrate and combined with additional feed water. To control the concentration of the sohds in the recirculation loop, a portion of the concentrate is discharged at a specific rate. In dead-end or direct filtration, all the feed water passes through the membrane. Therefore, the recovery is 100%, and a small fraction is used periodically for backwash in the system (5-15%). 

Since SIA systems are computer controlled, these can be used for additional operations intended to readily boost their sensitivity. Thus, once the sample has been propelled through the donor channel, the flow direction can be reversed to pass it again through the cell in this way, the sample is passed not once, but three times across the diffusion membrane and as a result the amount of ammonia crossing it increases. The increased sensitivity is illustrated in Figure 3.23. As can be seen, the slope of the calibration curve depends on the number of times that the sample is brought into contact with the membrane such a number is always odd as each flow reversal involves two passes across the membrane surface. In any case, more than two reversals have little further effect on the sensitivity and the analysis time is too long. 

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