P-Anisoyl Chloride

Chemical Designations - Synonyms p-Anisoyl Chloride Chemical Formula p-CHjOC HjCOCl. Observable Characteristics - Physical State (as normally shipped) Liquid Color. Yellow brown Odor. Sharp, penetrating. [Pg.23]

Anisamide, m54 Anisic acids, m57, m58, m59 Anidisines, m48, m49, m50 Anisole, m55 p-Anisoyl chloride, m60 p-Anisyl alcohol, m61 Anthranilamide, all2 Anthranilic acid, all8 Araboascorbic acid, i61 APDC, p282 Arsanilic acids, all3... [Pg.97]

A solution of 529.8 g (3.505 mole) methyl anthranilate and 294.4 g 50 weight percent NaOH (3.68 mole) in 3.6 L CH2CI2 and 1.8 L water was stirred in an ice-bath as 627.8 g (3.680 mole) p-anisoyl chloride was added at such rate that the temperature did not exceed 10°C (time required was 1.25 hr). The mixture was allowed to warm to 23°C. Acetic acid (50 mL) was added to adjust the pH to 5. The layers were separated and the organic layer was washed with 10% aqueous NaHC03 (1 times 0.8 L) and brine (1 times 0.8 L). The residual white solid was recrystallized from 7.0 L boiling material. The product was dried in vacuo at 70°C for 24 hr to yield 959.7 g (96.0%) white crystalline solid, melting point 122.5°C-124.5°C. [Pg.1431]

ANISOYL CHLORIDE or p-ANISOYL CHLORIDE (100-07-2) C8H7CIOJ Combustible solid. Decomposes at room temperature tightly closed containers may... [Pg.87]

Anisoyl chloride 4-Anisoyl chloride. See p-Anisoyl chloride p-Anisoyl chloride... [Pg.315]

Benzoyl chloride, methoxy- Benzoyl chloride, 4-methoxy-. See p-Anisoyl chloride Benzoyl chloride, 3-nitro- Benzoyl chloride, m-nitro-. See m-Nitrobenzoyl chloride N-Benzoyl-N-(3-chloro-4-fluorophenyl)-DL-alanine 1-methylethyl ester. SeeFlamprop-isopropyl... [Pg.461]

Methoxybenzoic acid. See o-Anisic acid 4-Methoxybenzoic acid. See p-Anisic acid o-Methoxybenzoic acid. See o-Anisic acid p-Methoxybenzoic acid. See p-Anisic acid 4-Methoxybenzoic acid chloride p-Methoxybenzoic acid chloride. See p-Anisoyl chloride... [Pg.2555]

Chloronitrobenzene 202-810-1 p-Nitroaniline 202-811-7 p-Nitrophenol 202-815-9 Acetanisole Xinsorb UV-A 202-816-4 p-Anisoyl chloride 202-818-5 p-Anisic acid Lexgard 688 202-819-0... [Pg.6720]

Chloroacetophenone Phenylacetyl chloride p-Toluoyl chloride C8H7CIO2 p-Anisoyl chloride Benzyl chloroformate C8H7N Indole... [Pg.7053]

Preparation by heating a mixture of 4-hydroxybenzoic acid and hydroquinone in OH nitrobenzene in the presence of boron triflu oride at 80° for 30 min (64%) [186]. N.B. In the patent, this compound was erroneously called 3, 4,5 -tri-hydroxybenzophenone (assay 5, table page 3) [186]. Preparation by Friedel-Crafts acylation of hydroquinone dimethyl ether with p-anisoyl chloride (AICI3/CS2/ 3 h at r.t.), followed by demethylation (AICI3/ Toluene/1 h at 120°) (65%). -Refer to Chem. Abstr., 44, 1271f (1950)L... [Pg.26]

Preparation by Friedel-Crafts acylation of pyrocatechol dimethyl ether with p-anisoyl-chloride (AlClj/CS / 3 h at r.t.), followed by demethylation (AlCytoluene/ 1 h at 120°) (65%). [Pg.27]

Preparation by Friedel-Crafts acylation of chlorobenzene with p-anisoyl chloride in the presence of aluminium chloride at 120° for 3 h (50-70%) [931]. [Pg.154]

Preparation by reaction of p-anisoyl chloride with p-chloro-anisole in the presence of aluminium chloride in methylene chloride at r.t. for 18 h under nitrogen (41%) [472]. [Pg.240]

Preparation by reaction of p-anisoyl chloride with resorcinol dimethyl ether,... [Pg.287]

Obtained by partial demethylation of 2,4, 5-trimethoxy-benzophenone (SM) with aluminium chloride in nitro-methane at 20° for 24 h. SM was obtained by Friedel-Crafts acylation of 1,4-dimethoxy-benzene with p-anisoyl chloride in the presence of stannic chloride in nitromethane at 20° for Ih [679],... [Pg.434]

Also obtained by Friedel-Crafts reaction between p-anisoyl chloride and anisole, followed by demethylation of the obtained product [1505]. [Pg.567]

Obtained by reaction of p-anisoyl chloride with o-bromophenylzinc iodide in the presence of Pd(PPhj) in THF at 20° for 1 h [1613]. [Pg.586]

Preparation by reaction of p-anisoyl chloride on resacetophenone with potassium carbonate in toluene (70%) [2613] or in aqueous sodium hydroxide solution (the best way) [2613],... [Pg.1016]

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