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LiChrospher 60 RP-Select

HPLC column, Merck, LiChrospher 60 RP Select B, 5 itm, 150 x 4-mm i.d. Autosampler vials, 1.8-mL Assorted laboratory glassware Autopipettes, calibrated... [Pg.1323]

CF, TB, TP, preservatives, and antioxidants HPLC-UV. Column LiChrospher 60 RP-Select B. [Pg.912]

Guard column 25x4 mm cartridge packed with LiChrospher 60 RP select B, 5 pm (Merck)... [Pg.142]

Lor analyses, two sets of HPLC conditions were used, depending on whether UV (285 nm) or MS (electrospray ionization on a triple quadrupole system) was to be used for detection. Lor MS detection, analyses were conducted using a 125 x 4 mm (5 pm) Lichrospher 60 RP-Select B column. Eluent A was 800 ml water/200ml acetonitrile/3.08 g ammonium acetate adjusted to pH 6.5 with acetic acid. Eluent B was 500 ml water/500ml acetonitrile/1.93 g ammonium acetate adjusted to pH 6.5 with acetic acid. The gradient was run at 0.5ml/min as follows from 0-25.0 min, 100% A from 25.0-35.0 min, 100% A-100% B from 35.0-45.0 min, 100% B from... [Pg.358]

Figure 10.10 Stationary phase for basic compounds. Conditions sample, adenine derivatives columns, 25cm x 4mm i.d. stationary phase left, LiChroshper 100 RP-18, 5 m (with high separation performance and good peak symmetry for neutral compounds) stationary phase right, LiChrospher 60 RP-Select B, 5 im mobile phase, 1.5mlmin water-methanol (25 75) UV detector, 260 nm. Figure 10.10 Stationary phase for basic compounds. Conditions sample, adenine derivatives columns, 25cm x 4mm i.d. stationary phase left, LiChroshper 100 RP-18, 5 m (with high separation performance and good peak symmetry for neutral compounds) stationary phase right, LiChrospher 60 RP-Select B, 5 im mobile phase, 1.5mlmin water-methanol (25 75) UV detector, 260 nm.
Figure 19.9 Analysis of explosives at a UV wavelength change of 2 nm. Conditions column, 25 cm x 4.0 mm i.d. stationary phase, LiChrospher 60 RP-Select B, 5gm mobile phase, Imimin water-acetonitrile (30 70). Peaks 1=octogen 2 = hexogen 3 tetryl 4 = trinitrotoluene 5 = nitropenta. Figure 19.9 Analysis of explosives at a UV wavelength change of 2 nm. Conditions column, 25 cm x 4.0 mm i.d. stationary phase, LiChrospher 60 RP-Select B, 5gm mobile phase, Imimin water-acetonitrile (30 70). Peaks 1=octogen 2 = hexogen 3 tetryl 4 = trinitrotoluene 5 = nitropenta.
Column 125 x 4 5 p,m Lichrospher 60 RP Select B Mobile phase MeCN 20 mM ammonium acetate 55 45 Flow rate 1 Ii jection volume 10 Detector UV 254... [Pg.149]

Column 100 x 2 5 xm LiChrospher 60-RP select B Mobile phase MeCN MeOH water 1 1 1, pH 6 Flow rate 0.1 Iqjection volume 5... [Pg.471]

Column 250 X 4 5 p,m LiChrospher 60 RP-Select B Mobile phase MeOH water acetic acid 48 45 7, pH 2.47 Flowrate 1.1 Ipjection volume 20 Detector UV 340... [Pg.1141]

Column 125 X 4 5 pm LiChrospher 60 RP-select B Mobile phase MeCN 10 mM pH 4 sodium acetate 12 88 Flowrate 0.6 Ipjection volume 50-200 Detector UV 270... [Pg.1364]

Guard column 4x45 pm Lichrospher 60 RP-select B Column 125 X 4 5 pm Lichrospher 60 RP-select B Mobile phase MeOH pH 7.0 phosphate buffer 20 80 Flow rate 1 Ipjection volume 10 Detector UV 265... [Pg.1482]

For all HPLC-analysis reversed phase C-18 or C-8 columns (LiChroCART 125-4/250-4 LiChrospher 100 RP-18 (5 pm), Merck or LiChroCART 125-4/250-4 LiChrospher 60 RP select B (5 pm), Merck) can be used with a Merck HITACHI L-4500 A Diode Array Detector. [Pg.1]


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See also in sourсe #XX -- [ Pg.325 ]




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