Hydrothermal Synthesis of Ceramics

Chapter 1 Hydrothermal Synthesis of Ceramic Oxide Powders.3... 

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Baldassari, S., Komarneni, S., Mariani, E. and Villa, C. (2005) Rapid microwave-hydrothermal synthesis of anatase form of titanium dioxide. Journal of the American Ceramic Society, 88, 3238—3240. 

Xie, Y., Yin, S., Hashimoto, T., Kimura.H. and Sato, T. (2009) Microwave-hydrothermal synthesis of nano-sized Sn2+-doped BaTi03 powdersand dielectric properties of corresponding ceramics obtained byspark plasma sintering method. Journal of Materials Science, 44, 4834—4839. 

Dawson, W.J., Hydrothermal synthesis of advanced ceramic powders. Am. Ceram. Soc. Bull., 67, 1673, 1988. 

Komameni, S., Novel microwave-hydrothermal processing for synthesis of ceramic and metal powders, in Novel Techniques in Synthesis and Processing of Advanced Materials, Singh, J., and Copley, S.M., Eds., Minerals, Metals, and Materials Society, Warrendale, PA, 103, 1995. 

Yamanaka T, Fukumori Y (1995) Molecular aspects of the electron transfer system which participates in the oxidation of iron by Thiobacillus ferrooxidans. FEMS Microbiol Rev 17 401-413 Yanagisawa K, Ovenstone J (1999) Crystallization of anatase from amorphous titania using the hydrothermal technique Effects of starting material and temperature. J Phys Chem B 103 7781-87 Yang J, Mei S, Ferreira IMF (2000) Hydrothermal synthesis of nanosized titania powders lirfluence of peptization and peptizing agents on the crystalline phases and phase transition. J Am Ceram Soc 83 1361-1368... 

Yang, J., Mei, S., and Ferreira, J.M.R, Hydrothermal synthesis of nanosized titania powders Influence of tetraalkyl ammonium hydroxides on particle characteristics, J. Am. Ceram. Soc., 84, 1696, 2001. 

ADA/DEN] Adair, J. H., Denkewicz, R. P., Arriagada, F. J., Osseo-Asare, K., Precipitation and in situ transformation in the hydrothermal synthesis of crystalline zirconium dioxide, Ceram. Trans., 1, (1987), 135-145. Cited on page 409. 

The methods of soft chemistry include sol-gel, electrochemical, hydrothermal, intercalation and ion-exchange processes. Many of these methods are employed routinely for the synthesis of ceramic materials. - There have been recent reviews of the electrochemical methods, intercalation reactions, and the sol-gel technique. The sol-gel method has been particularly effective with wide-ranging applications in ceramics, catalysts, porous solids and composites and has given rise to fine precursor chemistry. Hydrothennal synthesis has been employed for the synthesis of oxidic materials under mild conditions and most of the porous solids and open-framework structures using organic templates are prepared hydro-thermally. The advent of supramolecular chemistry has started to make an impact on synthesis, mesoporous solids being well known examples. ... 

Eckert JO, HungHouston CC, Gersten BL, Lencka MM, Riman RE (1996) Kinetics and mechanisms of hydrothermal synthesis of barium titanate. J Am Ceram Soc 79 2929-2939... 

Suchanek WL (2010) Hydrothermal synthesis of a-alumina (a-Al203) powders study of the processing variables and growth mechanisms. J Am Ceram Soc 93 399-412... 

Supercritical fluids have received considerable attention as solvents for the synthesis of ceramic or similar materials. One method applies thermal decomposition of precursors in a supercritical fluid, which is at the end of the reaction depressurized and removed from the system. After removal of the solvent, obtained inorganic material is typically in the form of micron or submicron particles. The second method uses supercritical fluid as a solvent and a reactant. In this case, the typical supercritical fluid is water, and the process is called hydrothermal synthesis. Inorganic solids obtained by the decomposition in the supercritical fluid or by the synthesis using supercritical reactant, are hsted in Tables 24.4 and Table 24.5, respectively. As it can be seen from the presented data different morphologies can be obtained on the micrometer or nanometer scale. 

Urek, S., Drofenik, M. The hydrothermal synthesis of BaTiOs fine particles from hydroxide-alkoxide precursors. J. Eur. Ceram. Soc. 18, 279-286 (1998)... 

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Pinceloup, R, Courtois, C., Vicens, J., Leriche, A., Thierry, B. Evidence of a dissolution-precipitation mechanism in hydrothermal synthesis of barium titanium powders. J. Eur. Ceram. Soc. 19, 973-977 (1999)... 

Wu, M., Long, J., Wang, G., Huang, A., Luo, Y. Hydrothermal synthesis of tetragonal barium titanate from barium hydroxide and titanium dioxide under moderate conditions. J. Am. Ceram. Soc. 82, 3254-3256 (1999)... 

Chen Z, Wei Shi E, Zheng Y-Q, Xiao B, Zhuang J-Y. Hydrothermal synthesis of nanosized C0AI2O4 on ZnAl204 seed crystallites. J Am Ceram Soc 2004 86 1058-60. 

Haiyan X, Hao W, Zhang Y, Cai H, Liang W, Mankang Z, et al. Hydrothermal synthesis of zinc oxide powders with controllable morphology. Ceram Int 2004 30 93-7. 

Dell Agli G, Mascolo G (2000) Hydrothermal synthesis of Z1O2-Y2O3 solid solutions at low temperature. J Eur Ceram Soc 20(2) 139-145... 

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