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Field emission scanning electronic

A Dektak siuface profilometer was used to measure the etch rates. The profiles of the etched films were observed by field emission scanning electron microscopy (FESEM). In addition, x-ray photoelectron spectroscopy PCPS) was utilized to examine the existence of possible etch products or redeposited materials, and to elucidate the etch mechanism of Co2MnSi magnetic films in a CVOa/Ar plasma. [Pg.378]

Figure 8. (a) Field emission scanning electron micrograph of a lead structure before the nanocrystals are introduced. The light gray... [Pg.113]

Dalgleish, D. G., Spagnuolo, P. A., and Douglas Goff, H. (2004). A possible structure of the casein micelle based on high-resolution field emission scanning electron microscopy. Int. Dairy. 14,1025-1031. [Pg.238]

MCM-41 samples have been characterized by means of powder X-ray diffraction (X Pert Philips, CuKa radiation), nitrogen adsorption measurements at 77 K (Quantachrome Autosorbl) and Field Emission Scanning Electron Microscopy (Assing FESEM Supra 25) before soaking in SBF and after different immersion times. [Pg.249]

VI. Recent Advances in Ultra-High Resolution, Low-Voltage Field Emission Scanning Electron Microscopy and Extreme FESEM in Catalysis... [Pg.217]

Typical examples of Rutherford-scattered imaging of nanoparticles of a commercially important Pd/C catalyst recorded with (a) a BSE detector in a field emission scanning electron microscope as well as (b) a STEM HAADF image of the same 5% Pd/C sample, recorded in the same instrument, are shown... [Pg.236]

Field emission devices, 17 49-50 Field emission FPDs (FEDs), 22 259 Field emission microscope (FEM), 16 503 Field emission microscopy (FEM), 24 74 Field emission scanning electron microscope (FESEM), 16 492 Field emission scanning electron... [Pg.356]

Image analysis has been used to characterize the pore structure of synthetic membrane materials. The Celgard films have also been characterized by scanning tunneling microscopy, atomic force microscopy, and field emission scanning electron microscopy. The pore size of the Celgard membranes can also be calculated from eq 5, once the MacMullin number and gurley values are known. [Pg.194]

The morphology of silver nanopartilces on the cotton surface and paint samples was observed by field emission scanning electron microscopy (FE-SEM JSM-6700F, JEOL, Japan). The size and shape of the nanoparticles in solution were determined with transmission electron microscopy (TEM) (LEO-912-OMEGA, Carl Zeiss, Germany). [Pg.171]

Fig. 8 Different views of T. foetus hydrogenosomes ( ) after field-emission scanning electron microscopy (FESEM) (a) and freeze-etching (b,c). An isolated hydrogenosome obtained from T. foetus observed by FESEM, where details of its surface can be seen, b A calcium deposit in the peripheral vesicle (asterisk) c shows that the peripheral vesicle (arrow) presents a smooth surface, distinct from the organelle body. Bars = 50 nm. (From Benchimol 2000)... Fig. 8 Different views of T. foetus hydrogenosomes ( ) after field-emission scanning electron microscopy (FESEM) (a) and freeze-etching (b,c). An isolated hydrogenosome obtained from T. foetus observed by FESEM, where details of its surface can be seen, b A calcium deposit in the peripheral vesicle (asterisk) c shows that the peripheral vesicle (arrow) presents a smooth surface, distinct from the organelle body. Bars = 50 nm. (From Benchimol 2000)...
Enhanced imaging of several dairy products has been demonstrated through the application of a relatively elaborate preparative technique in combination with a cold-field emission scanning electron microscope (FESEM) [86], The preparative methods include a metal-impregnation technique, termed tannin-ferrocyanide-osmium (TA-F-O, Figure 21), which was adapted from Hirano et al. [87]. [Pg.270]

FIGURE 3.30 Field emission scanning electron microscopy image of the submicron porous structure of methane hydrate after 2 weeks of reaction at 60 bar, 265 K. (Reproduced from Staykova, D.K., Kuhs, J. Phys. Chem. B, 107, 10299 (2003). With permission from the American Chemical Society.)... [Pg.165]

Figure 10.12. Atomic force microscope (a) and field-emission scanning electron microscope (b) images of an ordered array of 200-nm silver-coated silica spheres. (With permission from Ref. 37.)... Figure 10.12. Atomic force microscope (a) and field-emission scanning electron microscope (b) images of an ordered array of 200-nm silver-coated silica spheres. (With permission from Ref. 37.)...
I was characterized by powder X-ray diffraction (PXRD), energy dispersive analysis of X-rays (EDAX), chemical analysis, thermogravimetric analysis (TGA) and IR spectroscopy. EDAX analysis indicated the ratio of Mn S to be 3 2. The presence of fluorine was confirmed by analysis and the percentage of fluorine estimated by EDAX in a field emission scanning electron microscope was also satisfactory. Thermogravimetric analysis also confirms the stoichiometry of the compound. Bond valence sum calculations6 and the absence of electron density near fluorine in the difference Fourier map also provide evidence for the presence of fluorine. The sulfate content was found to be 30.8% compared to the expected 32% on the basis of the formula. [Pg.406]


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