Creep test

One other method used occasionally is the sudden application of a constant strain, and the monitoring of the consequent stress, which then decays away with time—this is called a stress relaxation test. The only other test we need to mention here is the application of a steady shear rate, as in the start-up of a simple viscometer —so not surprisingly this is called a start-up test. All these tests are shown in figure 2. The first two tests mentioned—creep and oscillatory—will now be dealt with at some length, since they are the most frequently used tests, while the other two — stress relaxation and start-up—will only be mentioned briefly. 

The behaviour normally seen for typical viscoelastic liquids—represented for convenience and simplicity by a Burgers model—in a creep test is shovm in figure 3. 

The answer to this problem is to tighten the level of scrutiny with which the instrument decides if steady state is achieved, and then the normal viscosity plateau is seen. 

The universal curve that describes the creep response of most structured liquids and gels is shown in figure 5, with some examples shown in figure 6. The behaviour is depicted over a very long time period, which, as ever, is best shown on a logarithmic scale. The response for most materials measured rmder normal conditions is such that we first see the immediate elastic response (the horizontal dotted line), then we see the delayed elastic response, and eventually the viscous flow predominates, and the slope approaches unity at very long times (see the second dotted tine). 

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Relaxation of the residual stresses induced by autofrettage at 720 MPa (104,400 psi) in reactor tubes k = 2.4), of AISI 4333 M6 at a uniform temperature of 300°C has been studied and it was concluded, on the basis of creep tests for 10,000 h, that after 5.7 years 60% of the original stress would remain (161). 

Creep tests are ideally suited for the measurement of long-term polymer properties in aggressive environments. Both the time to failure and the ultimate elongation in such creep tests tend to be reduced. Another test to determine plastic behavior in a corrosive atmosphere is a prestressed creep test in which the specimens are prestressed at different loads, which are lower than the creep load, before the final creep test (11). 

Creep tests require careful temperature control. Typically, a specimen is loaded in tension or compression, usually at constant load, inside a furnace which is maintained at a constant temperature, T. The extension is measured as a function of time. Figure 17.4 shows a typical set of results from such a test. Metals, polymers and ceramics all show creep curves of this general shape. 

An alloy tie bar in a chemical plant has been designed to withstand a stress, ct, of 25 MN m at 620°C. Creep tests carried out on specimens of the alloy under... 

Slides Tungsten filaments, turbine blades, lead drain pipes and organ pipes, glaciers creep-testing rigs micrographs of creep cavities. 

Type of stress. A uniaxial tensile creep test would not be expected to give the required data if the designer was concerned with torsional or compressive creep. 

Since the tensile test has disadvantages when used for plastics, creep tests have evolved as the best method of measuring the deformation behaviour of... 

Over the years there have been many attempts to simulate the behaviour of viscoelastic materials. This has been aimed at (i) facilitating analysis of the behaviour of plastic products, (ii) assisting with extrapolation and interpolation of experimental data and (iii) reducing the need for extensive, time-consuming creep tests. The most successful of the mathematical models have been based on spring and dashpot elements to represent, respectively, the elastic and viscous responses of plastic materials. Although there are no discrete molecular structures which behave like the individual elements of the models, nevertheless... 

There are several other comparable rheological experimental methods involving linear viscoelastic behavior. Among them are creep tests (constant stress), dynamic mechanical fatigue tests (forced periodic oscillation), and torsion pendulum tests (free oscillation). Viscoelastic data obtained from any of these techniques must be consistent data from the others. 

TTie strain readings of a creep test can be more accessible to a designer if they are presented as a creep modulus. In a viscoelastic material, namely plastic, the strain continues to increase with time while the stress level remains constant. Since the creep modulus equals stress divided by strain, we thus have the appearance of a changing modulus. 

Creep-test specimens may be loaded in tension or flexure (to a lesser degree in compression) in a constant temperature environment. With the load kept constant, deflection or strain is recorded at regular intervals of hours, days, weeks, months, or years. Generally, results are obtained at three or more stress levels. 

The tests are performed under carefully controlled stress (load), temperature, time, and creep (elongation) conditions. To save time, tests for different constant loads are performed simultaneously on different specimens of the same material. Creep tests may be rather extensively conducted, as for example when developing creep data prior to the design and fabrication of the first all-plastic airplane (41). The usual procedure is to plot the creep versus time curve, but other combinations are possible. 

Extensive amount of these type data has been plotted but unfortunately most of it is privately owned. Creep data available from material suppliers, college and government projects, etc. can provide guidelines. However where the product has to meet critical requirements that usually include safety of people and data from previous work does not exist, creep test have to be conducted and properly applied by the designer. 

A creep test can be carried out with an imposed stress, then after a time have its stress suddenly changed to a new value and have the test continued. This type of change in loading allows the creep curve to be predicted. The simple law referred to earlier as the Boltzmann superposition principle, hold for most materials, so that their creep curves can thus be predicted. 

Third, creep data application is generally limited to the identical material, temperature use, stress level, atmospheric conditions, and type of test (that is tensile, flexural, or compressive) with a tolerance of 10%. Only rarely do product requirement conditions coincide with those of a test or, for that matter, are creep data available for all the grades of materials that may be selected by a designer. In such cases a creep test of relatively short duration, say 1,000 hours, can be instigated, and the information be extrapolated to long-... 

Creep test data when plotted on log-log paper usually form a straight line and tend themselves to extrapolation. Tlie slope of the straight line, which indicates a decreasing modulus, depends on the nature of the material (principally its rigidity and temperature of heat deflection), the temperature of the environment in which the product is used, and the amount of stress in relation to tensile strength. 

Some charts show creep test data beyond the 1,000 h duration, and in fact under most conditions the straight line between the 100... 

If data are not available on the effects of time, temperature, and strain rate on modulus, creep tests can be performed at various stress levels as a function of temperature over a reasonable period of time. In this regard, reasonable is a relative term. For applications like rockets and missiles, data obtained over a time period of 4-5 sec to an hour provide the essential information. For structural applications, such as pipelines, data over a period of years are required. 

The tensile modulus is an important property that provides the designer with information for a comparative evaluation of plastic material and also provides a basis for predicting the short-term behavior of a loaded product. Care must be used in applying the tensile modulus data to short-term loads to be sure that the conditions of the test are comparable to those in use. The longer-term modulus is treated under the creep test (Chapter 2). 

The time segment of the creep test is common to all materials, i.e., strains are recorded until the specimen ruptures or the specimen is no longer useful because of yielding. In either case, a point of failure of the test specimen has been reached. 

In conclusion regarding creep testing, it can be stated that creep data and a stress-strain diagram indicate whether plain plastic properties can lead to practical product dimensions or whether a RP has to be substituted to keep the design within the desired proportions. For long-term product use under continuous load, plastic materials have to consider creep with much greater care than would be the case with metals. 

There are two further related sets of tests that can be used to give information on the mechanical properties of viscoelastic polymers, namely creep and stress relaxation. In a creep test, a constant load is applied to the specimen and the elongation is measured as a function of time. In a stress relaxation test, the specimen is strained quickly to a fixed amount and the stress needed to maintain this strain is also measured as a function of time. 

In creep tests, the parameter of interest is the creep compliance, J, defined as the ratio of the creep strain to the applied stress, i.e. 

Stress relaxation tests are alternative ways of measuring the same basic phenomenon in viscoelastic polymers as creep tests, Le. the time-dependent nature of their response to an applied stress. As such, they have also been of value in understanding the behaviour of these materials. The essence of stress relaxation tests is that strain increases with time for a given stress, so that if stress is decreased with time in a controlled manner ( relaxed ), a state... 

This method applies a constant force to the sample and monitors the strain (deformation) as a function of time This is called the creep test and gives the elastic and viscous properties of substances. 

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