Calypso

Charybdis Technologies. In the Calypso Reaction Block , multi-well reaetion arrays are designed for both solution and solid-phase synthesis applications. Well volumes range from 2 to 10 mL, pressures up to 207 kPa (30 psi), and temperatures from —80 to +180°C. 

TFP (tetrafluorophenol) esters55 in a 96-well filter plate, encapsulated in a Calypso frame assembly. Final compound purities were improved (13% on average) by the addition of PS-NCO. 

Typical Experimental Procedure (Plate Production). Production of an 80-member array was successfully completed using a Charybdis 96-well Teflon block, encapsulated in a Calypso reaction frame assembly. Reagents were transferred into the 96-well plate using either a Quadra 96 or Rapid Plate 96. The blocks were then heated at 65° for 3 days and the solvent evaporated in vacuo at 65°. Scavenging with PS-TsNHNH2 (6 equiv.) and PS-NCO (1 equiv.) was performed at the plate level and the resins were added using a Millipore column loader. Evaporation was performed in a Savant evaporator for 2 h. 

Information from a number of sources, including the open scientific literature, was consulted in addition to that provided by the French authorities. Reports on three independent scientific missions to the atolls that are available in the public domain were consulted—the Scientific Mission of French Polynesia (Tazieff mission) of June 1982, the New Zealand, Australia and Papua New Guinea Scientific Mission of Mururoa Atoll (Atkinson mission) of October 1983, and the Scientific Mission of the Calypso to the Site of the Nuclear Experiments at Mururoa Atoll (Cousteau mission) of June 1987. 

Fondation Cousteau, Mission Scientifique de la Calypso sur le site d experimentations nucleaires de Mururoa. Published by the Cousteau Fondation, 25 avenue Wagram, 75017-Paris, November 1988. 

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Charybdis Technologies undertook a similar approach and advanced it further in the development of the Calypso System [38]. A variety of disposable deep-well filtration plates manufactured by Polyfiltronics or reusable Multi-Well Re-... 

Calypso Vents, Taupo Zone Intfacontinental back-arc rifts... 

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