Testing methods furnace materials requirements

Many test methods for the determination of the acute toxicity of combustion products from materials and products have been developed over the last two decades and continue to be developed and/or improved. In 1983, 13 of the methods published up to that time were evaluated by Arthur D. Little, Inc. to assess the feasibility of incorporating combustion toxicity requirements for building materials and finishes into the building codes of New York State. On the basis of seven different criteria, only two methods were found acceptable. These two methods were the flow-through smoke toxicity method developed at the University of Pittsburgh and the closed-system cup furnace smoke toxicity method developed at NIST (known at that time as the National Bureau of Standards (NBS)). Standard Reference Materials and protocols (SRM 1048 and SRM 1049) were developed at NIST and are available to the users of these methods to provide assurance that they are performing the methods correctly (see Relevant Websites ... 

The mixture of starting materials is pressed into pellets and heated in a tubular carbon furnace imder high vacuum. Maximum temperatures of 1400-1900°C are required to produce the metal boride within a reasonable time. The method has been tested for borides of Ti, Zr, V, Nb, Ta and W. 

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