Solid/liquid separation, methods

There are several advantages that vacuum filtration has over other solid-liquid separation methods. Some of these advantages include ... 

In this subsection, basic design theory for preliminary sizing and specifying equipment are reviewed. Some sample design calculations are included. References cited at the end of tlie chapter can be consulted for more detailed information and design methods. For solid-liquid separation methods, the reader should refer to Liquid Filtration, 2" edition, by N. P. Cheremisinoff, Butterworth-Heinemarui Publishers (1998). 

Size (pm) Terminology Examples Solid/Liquid Separation Method... 

One of the most commonly used solid-liquid separation methods in crystallization processes is centrifugal filtration, such as continuous pusher and batchwise peeler centrifuges shown schematically in Figure 64.10. A manufacturer of centrifuges used in crystallization processes is KMPT AG [52]. In addition, Nutsche filters, frame pressure filters, and belt filters have also been used. Most of these filters have a possibility of cake washing which is important for the final purity as discussed earlier. 

Solid-liquid separation methods in direct method include washing and nonwashing. Solid-liquid separation methods in indirect method include filtering and centrifuging. 

Thus, methods are now becoming available such that process systems can be designed to manufacture crystal products of desired chemical and physical properties and characteristics under optimal conditions. In this chapter, the essential features of methods for the analysis of particulate crystal formation and subsequent solid-liquid separation operations discussed in Chapters 3 and 4 will be recapitulated. The interaction between crystallization and downstream processing will be illustrated by practical examples and problems highlighted. Procedures for industrial crystallization process analysis, synthesis and optimization will then be considered and aspects of process simulation, control and sustainable manufacture reviewed. 

The method for the recovery of tantalum and niobium was developed for use on secondary raw materials in the form of oil-contaminated sludge. Uchino and Azuma [486] suggested using solid-liquid separation of oil from the slurry prior to the recovery of tantalum and niobium from the raw material. 

The separation of solids from liquids forms an important part of almost all front-end and back-end operations in hydrometallurgy. This is due to several reasons, including removal of the gangue or unleached fraction from the leached liquor the need for clarified liquors for ion exchange, solvent extraction, precipitation or other appropriate processing and the post-precipitation or post-crystallization recovery of valuable solids. Solid-liquid separation is influenced by many factors such as the concentration of the suspended solids the particle size distribution the composition the strength and clarity of the leach liquor and the methods of precipitation used. Some important points of the common methods of solid-liquid separation have been dealt with in Chapter 2. 

The relative suitability of the common kinds of solid-liquid separation equipment is summarized in Table 11.3. Filtration is the most frequently used operation, but sedimentation as a method of pretreatment and centrifugation for difficulty filterable materials has many applications. Table 11.15 gives more detail about the kinds of filters appropriate to particular services. 

The present paper deals with fluidized bed adsorption as an integrative recovery operation. The scope of the contribution is first to describe the concept of the method and the different principles of achieving a combination of solid-liquid separation and chromatography. In the following the main system... 

The contributions of Dr. Joseph D. Henry (Alternative Solid/Liquid Separations), Dr William Eykamp (Membrane Separation Processes), Dr. T. Alan Hatton (Selection of Biochemical Separation Processes), Dr. Robert Lemlich (Adsorptive-Bubble Separation Methods), Dr. Charles G. Moyers (Crystallization from the Melt), and Dr. Michael P. Thien (Selection of Biochemical Separation Processes), who were authors for the seventh edition, are acknowledged. 

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